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1. 发明授权

US06726755B2 Ink compositions containing phthalocyanines 失效
标题翻译：含有酞菁的油墨组合物
公开(公告)号：US06726755B2
公开(公告)日：2004-04-27
申请号：US10072210
申请日：2002-02-08
申请人： Donald R. Titterington , Michael B. Meinhardt , Jeffrey H. Banning , James D. Mayo , James M. Duff , Roger E. Gaynor , Harold R. Frame
发明人： Donald R. Titterington , Michael B. Meinhardt , Jeffrey H. Banning , James D. Mayo , James M. Duff , Roger E. Gaynor , Harold R. Frame
IPC分类号： C09D1112
CPC分类号： C09D11/34
摘要： Disclosed is a phase change ink composition comprising a phase change ink carrier and a colorant compound of the formula wherein M is an atom or group of atoms capable of bonding to the central cavity of a phthalocyanine molecule, wherein axial ligands optionally can be attached to M. Also disclosed are printing processes using the phase change inks.
摘要翻译：公开了一种相变油墨组合物，其包含相变油墨载体和糠醛的着色剂化合物M是能够结合到酞菁分子的中心腔的原子或原子团，其中轴向配体任选地可以连接到M. 还公开了使用相变油墨的印刷方法。

2. 发明授权

US06476219B1 Methods for preparing phthalocyanine compositions 失效
标题翻译：制备酞菁组合物的方法
公开(公告)号：US06476219B1
公开(公告)日：2002-11-05
申请号：US10072237
申请日：2002-02-08
申请人： James M. Duff , James D. Mayo , Roger E. Gaynor , Jeffrey H. Banning , Michael B. Meinhardt , Randall R. Bridgeman , Nan-Xing Hu , Carol A. Jennings , Marko D. Saban , Paul F. Smith , Hadi K. Mahabadi
发明人： James M. Duff , James D. Mayo , Roger E. Gaynor , Jeffrey H. Banning , Michael B. Meinhardt , Randall R. Bridgeman , Nan-Xing Hu , Carol A. Jennings , Marko D. Saban , Paul F. Smith , Hadi K. Mahabadi
IPC分类号： C07D48722
CPC分类号： C07D487/22
摘要： Disclosed is a process for preparing a colorant of the formula wherein M is an atom or group of atoms capable of bonding to the central cavity of a phthalocyanine molecule, wherein axial ligands optionally can be attached to M, which comprises (a) reacting 3-n-pentadecylphenol with 4-nitrophthalonitrile in the presence of a base to form an alkylarylether adduct of phthalonitrile; and (b) reacting the alkylarylether adduct of phthalonitrile with either (i) a metal compound, or (ii) an ammonia-releasing compound in the presence of an alkanolamine solvent, or (iii) mixtures of (i) and (ii), to form the colorant.
摘要翻译：公开了一种制备绢云母的着色剂的方法M是能够结合到酞菁分子的中心腔的原子或原子团，其中轴向配体任选地可以连接到M上，其包括（a）使3-n 十六烷基酚与4-硝基邻苯二甲腈在碱的存在下反应形成邻苯二甲腈的烷基芳基醚加成物; 和（b）使邻苯二甲腈的烷基醚加成物与（i）金属化合物或（ii）氨释放化合物在烷醇胺溶剂存在下反应，或（iii）（i）和（ii）的混合物，以形成着色剂。

3. 发明授权

US06576748B1 Method for making dimeric azo pyridone colorants 失效
标题翻译：制备二聚偶氮吡啶酮着色剂的方法
公开(公告)号：US06576748B1
公开(公告)日：2003-06-10
申请号：US10185828
申请日：2002-06-27
申请人： Rina Carlini , James D. Mayo , James M. Duff , Jeffrey H. Banning , Paul F. Smith , George Liebermann , Roger E. Gaynor
发明人： Rina Carlini , James D. Mayo , James M. Duff , Jeffrey H. Banning , Paul F. Smith , George Liebermann , Roger E. Gaynor
IPC分类号： C09B3312
CPC分类号： C09B33/12 , C09B35/031 , Y10S534/02
摘要： Disclosed is a process for preparing a diazopyridone compound either (A) of the formula or (B) of the formula which comprises diazotizing a dianiline and coupling it with a pyridone or diazotizing an aniline and coupling it with a dipyridone.
摘要翻译：公开了一种制备二叠氮基吡啶酮化合物的方法，式（B）的化合物（A）包括重氮化二苯胺并将其与吡啶酮偶联或重氮化苯胺并将其与二吡啶酮偶联。

4. 发明授权

US06576747B1 Processes for preparing dianthranilate compounds and diazopyridone colorants 失效
标题翻译：制备二邻氨基苯甲酸酯化合物和重氮吡啶酮着色剂的方法
公开(公告)号：US06576747B1
公开(公告)日：2003-06-10
申请号：US10185261
申请日：2002-06-27
申请人： Rina Carlini , James M. Duff , Stephen G. Robinson , George Liebermann , Roger E. Gaynor , Tania Pereira , Jeffrey H. Banning , James D. Mayo
发明人： Rina Carlini , James M. Duff , Stephen G. Robinson , George Liebermann , Roger E. Gaynor , Tania Pereira , Jeffrey H. Banning , James D. Mayo
IPC分类号： C09B35031
CPC分类号： C09B35/031 , C07C227/18 , C07C227/22 , C07C229/56 , C07D213/85 , Y10S534/02
摘要： Disclosed is a process for preparing dianthranilate compounds which comprises (a) admixing reactants as follows: (1) a diol of the formula R1(OH)2, wherein R1 is an alkylene group having at least about 20 carbon atoms, and wherein the —OH groups are primary or secondary, (2) isatoic anhydride, present in an amount of at least, about 2 moles of isatoic anhydride per every one mole of diol, (3) a catalyst which is 1,4-diazabicyclo [2.2.2]octane, N,N,N′,N′-tetramethylethylene diamine, or a mixture thereof, said catalyst being present in an amount of at least about 0.2 mole of catalyst per every one mole of diol, and (4) a solvent; and (b) heating the mixture thus formed to form a dianthranilate compound of the formula Also disclosed is a process for preparing diazopyridone colorants which comprises (I) preparing a dianthranilate compound by the aforementioned method, (II) reacting the dianthranilate compound with nitrosylsulfuric acid to form a diazonium salt, and (III) reacting the, diazonium salt with a pyridone compound to form a diazopyridone compound.
摘要翻译：公开了一种制备二氨基甲酸盐化合物的方法，其包括（a）如下混合反应物：（1）式R 1（OH）2的二醇，其中R 1是具有至少约20个碳原子的亚烷基， OH基团是伯或仲，（2）丙酸酐，每1摩尔二醇存在量至少约2摩尔丙烯酸酐，（3）作为1,4-二氮杂双环[2.2.2 ]辛烷，N，N，N'，N'-四甲基乙二胺或其混合物，所述催化剂的存在量为每一摩尔二醇至少约0.2摩尔催化剂，和（4）溶剂; 和（b）加热由此形成的混合物以形成下式的二邻氨基苯甲酸酯化合物。另外公开的是一种制备重氮吡啶酮着色剂的方法，其包括（I）通过上述方法制备二氨基甲酸酯化合物，（II）使二邻氨基苯甲酸酯化合物与亚硝酰基磺酸反应形成重氮盐，和（III）使重氮盐与吡啶酮化合物反应形成二叠氮基吡啶酮化合物。

5. 发明授权

US06472523B1 Phthalocyanine compositions 失效
标题翻译：酞菁组合物
公开(公告)号：US06472523B1
公开(公告)日：2002-10-29
申请号：US10072241
申请日：2002-02-08
申请人： Jeffrey H. Banning , Nan-Xing Hu , James D. Mayo , James M. Duff , Roger E. Gaynor , Rosa M. Duque , Nam S. Ro
发明人： Jeffrey H. Banning , Nan-Xing Hu , James D. Mayo , James M. Duff , Roger E. Gaynor , Rosa M. Duque , Nam S. Ro
IPC分类号： C07D48722
CPC分类号： C07D487/22 , C09B47/0675
摘要： Disclosed are compounds of the formula wherein M is an atom or group of atoms capable of bonding to the central cavity of a phthalocyanine molecule, wherein axial ligands optionally can be attached to M.
摘要翻译：公开的是糠醛的化合物M是能够结合到酞菁分子的中心腔的原子或原子团，其中轴向配体任选地可以连接到M.

6. 发明授权

US06663703B1 Phase change inks containing dimeric azo pyridone colorants 失效
标题翻译：相变油墨含有二聚偶氮吡啶酮着色剂
公开(公告)号：US06663703B1
公开(公告)日：2003-12-16
申请号：US10184269
申请日：2002-06-27
申请人： Bo Wu , Rina Carlini , Jeffrey H. Banning , James M. Duff , James D. Mayo , Jule W. Thomas, Jr. , Paul F. Smith , Michael B. Meinhardt
发明人： Bo Wu , Rina Carlini , Jeffrey H. Banning , James M. Duff , James D. Mayo , Jule W. Thomas, Jr. , Paul F. Smith , Michael B. Meinhardt
IPC分类号： C09D1100
CPC分类号： C09D11/34 , C09D11/328
摘要： Disclosed is a phase change ink composition comprising a phase change ink carrier and a colorant compound of the formula
摘要翻译：公开了一种相变油墨组合物，其包含相变油墨载体和下式的着色剂化合物

7. 发明授权

US06755902B2 Phase change inks containing azo pyridone colorants 失效
标题翻译：相变油墨含有偶氮吡啶酮着色剂
公开(公告)号：US06755902B2
公开(公告)日：2004-06-29
申请号：US10185264
申请日：2002-06-27
申请人： Jeffrey H. Banning , Bo Wu , James D. Mayo , James M. Duff , Rina Carlini , Jule W. Thomas, Jr. , Paul F. Smith
发明人： Jeffrey H. Banning , Bo Wu , James D. Mayo , James M. Duff , Rina Carlini , Jule W. Thomas, Jr. , Paul F. Smith
IPC分类号： C09D1100
CPC分类号： C09D11/34
摘要： Disclosed is a phase change ink composition comprising a phase change ink carrier and a colorant compound of the formula
摘要翻译：公开了一种相变油墨组合物，其包含相变油墨载体和下式的着色剂化合物

8. 发明授权

US06646111B1 Dimeric azo pyridone colorants 失效
标题翻译：二聚偶氮吡啶酮着色剂
公开(公告)号：US06646111B1
公开(公告)日：2003-11-11
申请号：US10186023
申请日：2002-06-27
申请人： Rina Carlini , James M. Duff , Jeffrey H. Banning , Bo Wu , James D. Mayo
发明人： Rina Carlini , James M. Duff , Jeffrey H. Banning , Bo Wu , James D. Mayo
IPC分类号： C09B3312
CPC分类号： C09B33/12 , Y10S534/02
摘要： Disclosed are compounds of the formula The compounds are useful as colorants, particularly in applications such as phase change inks.
摘要翻译：公开了下式的化合物该化合物可用作着色剂，特别是在诸如相变油墨的应用中。

9. 发明授权

US06696552B2 Process for preparing substituted pyridone compounds 有权
标题翻译：取代吡啶酮化合物的制备方法
公开(公告)号：US06696552B2
公开(公告)日：2004-02-24
申请号：US10185597
申请日：2002-06-27
申请人： James D. Mayo , James M. Duff , Rina Carlini , Roger E. Gaynor , George Liebermann
发明人： James D. Mayo , James M. Duff , Rina Carlini , Roger E. Gaynor , George Liebermann
IPC分类号： C09B4100
CPC分类号： C07D213/69 , C07D213/85 , Y10S534/02
摘要： A process which comprises admixing in the absence of a solvent an amine of the formula R1—NH2 and a first ester of the formula wherein R2 is an electron withdrawing group and R3 is an alkyl group; heating the mixture containing the amine and the first ester to form an intermediate compound of the formula admixing the intermediate compound with a base and a second ester of the formula said second ester being present in a molar excess relative to the intermediate compound, said base being present in a molar excess relative to the intermediate compound, and heating the mixture to form a pyridone compound of the formula or a salt thereof. Also disclosed is a process for preparing diazopyridone colorants which comprises preparing a pyridone compound by the above process and reacting the pyridone compound with a diazonium salt to form a diazopyridone compound.
摘要翻译：包括在不存在溶剂的情况下混合式R 1 -NH 2的胺和式R 2的第一酯的方法是吸电子基团，并且R 3是烷基; 加热含有胺和第一酯的混合物以形成中间体化合物，该中间体化合物将中间体化合物与碱和第二酯的第二酯相对于中间体化合物以摩尔过量存在，所述碱存在于相对于中间体化合物的摩尔过量，并加热该混合物以形成式的吡啶酮化合物或其盐。还公开了制备重氮吡啶酮着色剂的方法，其包括通过上述方法制备吡啶酮化合物并使吡啶酮化合物与重氮盐反应以形成重氮吡啶酮化合物。

10. 发明授权

US06673139B1 Phase change inks containing dimeric azo pyridone colorants 失效
标题翻译：相变油墨含有二聚偶氮吡啶酮着色剂
公开(公告)号：US06673139B1
公开(公告)日：2004-01-06
申请号：US10184266
申请日：2002-06-27
申请人： Bo Wu , Rina Carlini , James M. Duff , Jeffrey H. Banning , James D. Mayo
发明人： Bo Wu , Rina Carlini , James M. Duff , Jeffrey H. Banning , James D. Mayo
IPC分类号： C09D1100
CPC分类号： C09D11/34
摘要： Disclosed is a phase change ink composition comprising a phase change ink carrier and a colorant compound of the formula
摘要翻译：公开了一种相变油墨组合物，其包含相变油墨载体和下式的着色剂化合物

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