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1. 发明授权

US06530974B2 Method for the separation of molecules in the gas phase by adsorption by means of agglomerated solid inorganic adsorbents with a narrow and calibrated mesopore distribution 失效
公开(公告)号：US06530974B2
公开(公告)日：2003-03-11
申请号：US09812943
申请日：2001-03-27
申请人： Dominique Plee
发明人： Dominique Plee
IPC分类号： B01D5304
CPC分类号： B01D53/02 , B01D53/0462 , B01D53/047 , B01D53/0476 , B01D2253/10 , B01D2253/106 , B01D2253/304 , B01D2253/311 , B01D2257/7022 , B01D2257/7027 , B01D2257/708 , B01D2259/40083 , B01J20/10 , B01J20/183 , B01J20/28004 , B01J20/2803 , B01J20/28069 , B01J20/28083 , B01J20/2809 , Y02A50/235 , Y10S95/902
摘要： The present invention relates to a novel family of inorganic solids with a narrow and calibrated mesopore distribution which are agglomerated with a binder; these solids can advantageously be used as adsorbents for the industrial separation of gas-phase compounds having different boiling points.

2. 发明授权

US06410815B1 Agglomerated zeolite adsorbents, process for their preparation, and their use for adsorbing paraxylene from aromatic C8 fractions 有权
$Agglomerated zeolite adsorbents, process for their preparation, and their use for adsorbing paraxylene from aromatic C8 fractions$
标题翻译：聚集的沸石吸附剂，其制备方法及其用于从芳族C 8馏分中吸附对二甲苯的用途
公开(公告)号：US06410815B1
公开(公告)日：2002-06-25
申请号：US09485907
申请日：2000-05-10
申请人： Dominique Plee , Alain Methivier
发明人： Dominique Plee , Alain Methivier
IPC分类号： C07C700
CPC分类号： C07C7/13 , B01J20/183 , B01J20/186 , Y02P20/52 , C07C15/08
摘要： The present invention relates to agglomerated zeolite adsorbents based on faujasite with an Si/Al ratio such that 1≦Si/Al≦1.15, at least 70% exchanged with barium and optionally with potassium, and on a binder, preferably a zeolitizable binder. They are obtained by agglomerating zeolite powder with a binder, followed by exchange of the zeolite ions for barium ions and activation of the adsorbents thus exchanged. These adsorbents are particularly suitable for the adsorption of the para-xylene contained in aromatic C8 hydrocarbon fractions in the liquid phase, in processes of simulated fluid-bed type.
摘要翻译：本发明涉及基于八面沸石的团聚沸石吸附剂，其Si / Al比使得1≤Si/ Al <= 1.15，与钡和任选地与钾交换至少70％，并且在粘合剂上，优选可开发的沸石它们通过将沸石粉末与粘合剂结合，然后交换钡离子的沸石离子和活化被这样交换的吸附剂而获得。这些吸附剂特别适用于吸附芳族C8烃馏分中所含的对二甲苯液相，模拟流化床型。

3. 发明授权

US5609842A Zeolitic desulfuring agents and their application in the processing of gasses containing notable CO.sub.2 proportions 失效
标题翻译：沸石脱硫剂及其在处理含有显着二氧化碳比例的气体中的应用
公开(公告)号：US5609842A
公开(公告)日：1997-03-11
申请号：US290957
申请日：1994-11-22
申请人： Albert M. Tsybulevski , Vladimir I. Mourine , Dominique Plee , Francis Mayolet
发明人： Albert M. Tsybulevski , Vladimir I. Mourine , Dominique Plee , Francis Mayolet
IPC分类号： B01D53/02 , B01J20/18 , C01B39/14 , B01J8/00
CPC分类号： B01D53/02 , B01J20/183 , Y10S95/902
摘要： It is now possible to desulfurize gases containing appreciable carbon dioxide proportions by limiting the production of carbon oxysulfide to a very low level, by treating these gases with adsorbents composed of very small, partially calcic zeolite A crystals agglomerated by clays containing low levels of iron and having reduced acidity and basicity. These clays may be obtained by phosphatization of montmorillonite, bentonite, attapulgite, or kaolin.
摘要翻译： PCT No.PCT / FR94 / 00932 Sec。 371日期：1994年11月22日 102（e）1994年11月22日日期PCT 1994年7月26日PCT公布。公开号WO96 / 03199 日期1996年2月8日现在可以通过将硫氧化碳的产生限制在非常低的水平上来对含有可观二氧化碳比例的气体进行脱硫，通过用非常小的，部分钙化的沸石A晶体吸附剂处理这些气体，所述沸石由含有铁含量低，酸度和碱度降低。这些粘土可以通过蒙脱石，膨润土，绿坡缕石或高岭土的磷酸化获得。

4. 发明授权

US5173462A Industrial adsorbents based on low-silica X zeolites, for non-cryogenic separation of air gases, and their manufacture process 失效
标题翻译：基于低硅X沸石的工业吸附剂，用于非气体分离气体及其制造方法
公开(公告)号：US5173462A
公开(公告)日：1992-12-22
申请号：US791680
申请日：1991-11-14
申请人： Dominique Plee
发明人： Dominique Plee
IPC分类号： B01D53/02 , B01J20/18 , C01B13/02 , C01B21/04
CPC分类号： B01J20/183
摘要： An industrial shaped adsorbent for the non-cryogenic separation of gases from air, comprising from 70 to 95% by weight zeolites, and, correspondingly, from 30 to 5% by weight of a clay binder,(a) said zeolites consisting essentially of mixtures of X and A zeolites having an X crystallinity greater than or equal to 95% and an A crystallinity less than or equal to 5%, a toleune standard adsorption of 23.+-.1% and an X-ray spectrum characteristic of a practically pure faujasite, and with the Si/Al ratio of the crystalline component being 1.+-.0.03, and(b) with the adsorbent having a 2Ca/Al ratio between about 80 and 99%, a nitrogen adsorption between 16 and 23.5 L/kg and a ratio of the nitrogen to the oxygen adsorption capacities under 1 bar between 3.5 and 4.5 and the process of making such adsorbents.
摘要翻译：一种用于从空气中非低温分离气体的工业成型吸附剂，其包含70至95重量％的沸石，相应地为30至5重量％的粘土粘合剂，（a）所述沸石基本上由混合物具有X结晶度大于或等于95％且A结晶度小于或等于5％的X和A沸石，洗脱标准吸附为23 +/- 1％，实际上为纯度的X射线谱特征八面沸石，结晶成分的Si / Al比为1 +/- 0.03，（b）吸附剂的2Ca / Al比为约80〜99％，氮吸附量为16〜23.5L / kg 以及在3.5至4.5之间的1巴下的氮与氧吸附能力的比率以及制备这种吸附剂的过程。

5. 发明授权

US08771627B2 Process for producing carbon nanotubes from renewable raw materials 有权
标题翻译：从可再生原料生产碳纳米管的工艺
公开(公告)号：US08771627B2
公开(公告)日：2014-07-08
申请号：US12062687
申请日：2008-04-04
申请人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , André Lozowski , Dominique Plee
发明人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , André Lozowski , Dominique Plee
IPC分类号： C01B31/02
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162
摘要： A subject of the present invention is a process for producing carbon nanotubes, the process comprising: a) the synthesis of alcohol(s) by fermentation of at least one vegetable matter and optionally the purification of the product obtained; b) the dehydration of the alcohol or alcohols obtained in a) in order to produce, in a first reactor, a mixture of alkene(s) and water and optionally the purification of the product obtained; c) the introduction, in particular the introduction into a fluidized bed, in a second reactor, of a powdery catalyst at a temperature ranging from 450 to 850° C., this catalyst comprising at least one catalytic metal supported by an inert solid substrate, the grains of catalyst having a d50 of less than 300 μm; d) bringing the alkene produced in b) into contact with the powdery catalyst of stage c), optionally in a fluidized bed, in order to form carbon nanotubes and hydrogen on the surface of said catalyst by catalytic decomposition of said alkene; e) the recovery of the carbon nanotubes produced in d). The invention also relates to nanotubes capable of being obtained according to the abovementioned process, which can be advantageously used in all the known fields of application of carbon nanotubes.
摘要翻译：本发明的主题是一种生产碳纳米管的方法，该方法包括：a）通过至少一种植物物质的发酵和任选的所得产物的纯化来合成醇; b）在a）中获得的醇或醇的脱水，以便在第一反应器中产生烯烃和水的混合物，并任选地纯化获得的产物; c）引入，特别是在第二反应器中引入粉末状催化剂在450-850℃的温度下引入流化床，该催化剂包含至少一种由惰性固体基质负载的催化金属， d50小于300μm的催化剂颗粒; d）使b）中产生的烯烃与阶段c）的粉末催化剂任选地在流化床中接触，以便通过所述烯烃的催化分解在所述催化剂的表面上形成碳纳米管和氢; e）在d）中生产的碳纳米管的回收。本发明还涉及能够根据上述方法获得的纳米管，其可有利地用于所有已知的碳纳米管应用领域。

6. 发明授权

US07799246B2 Method for synthesis of carbon nanotubes 有权
标题翻译：合成碳纳米管的方法
公开(公告)号：US07799246B2
公开(公告)日：2010-09-21
申请号：US11814811
申请日：2006-02-03
申请人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , Dominique Plee
发明人： Serge Bordere , Daniel Cochard , Eric Dutilh , Patrice Gaillard , Dominique Plee
IPC分类号： H01B1/04 , C01B31/02
CPC分类号： B01J8/24 , B01J21/04 , B01J23/745 , B01J35/006 , B01J35/023 , B01J35/10 , B01J35/1019 , B01J35/108 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C01B2202/06 , C30B7/00 , C30B7/005 , C30B29/605
摘要： The present invention relates to a process for preparing CNTs by bringing a carbon source into contact with a multivalent metal and/or metal-oxide-based catalyst deposited on an inorganic substrate having a BET specific surface area of greater than 50 m2/g. The CNTs obtained may be used as agents for improving the mechanical and electrical conductivity properties in polymeric compositions.
摘要翻译：本发明涉及通过使碳源与沉积在BET比表面积大于50m 2 / g的无机基材上的多价金属和/或金属氧化物类催化剂接触来制备CNT的方法。所获得的CNT可以用作改善聚合物组合物中机械和电导率性能的试剂。

7. 发明申请

US20100047153A1 METHOD OF MANUFACTURING CARBON FIBRES 审中-公开
标题翻译：制造碳纤维的方法
公开(公告)号：US20100047153A1
公开(公告)日：2010-02-25
申请号：US12546128
申请日：2009-08-24
申请人： Dominique Plee
发明人： Dominique Plee
IPC分类号： D01F9/12
CPC分类号： D01F9/22
摘要： The present invention relates to a method of manufacturing carbon fibres from raw materials of renewable origin, comprising: a) synthesis of acrolein from glycerol of vegetable origin; b) ammoxidation of the acrolein to obtain acrylonitrile; c) polymerization of the acrylonitrile to a homopolymer or copolymer of acrylonitrile (PAN); d) conversion of the PAN to PAN fibres; e) partial oxidation of the PAN fibres; and f) carbonization of the partially oxidized PAN fibres. It also relates to the fibres capable of being obtained according to this method, and also to the uses thereof.
摘要翻译：本发明涉及从可再生原料的原料制造碳纤维的方法，其包括：a）从植物来源的甘油合成丙烯醛; b）丙烯醛氨氧化得到丙烯腈; c）将丙烯腈聚合成丙烯腈（PAN）的均聚物或共聚物; d）将PAN转化为PAN纤维; e）PAN纤维的部分氧化; 和f）部分氧化的PAN纤维的碳化。还涉及能够根据该方法得到的纤维，以及其用途。

8. 发明申请

US20100038602A1 METHOD FOR PREPARING CARBON FIBRILS AND/OR NANOTUBES FROM A CARBON SOURCE INTEGRATED WITH THE CATALYST 审中-公开
标题翻译：从碳源与催化剂一起制备碳纤维和/或纳米碳的方法
公开(公告)号：US20100038602A1
公开(公告)日：2010-02-18
申请号：US12519995
申请日：2007-12-18
申请人： Dominique Plee
发明人： Dominique Plee
IPC分类号： H01B1/12 , B01J31/06 , D01F9/12 , C08K3/04
CPC分类号： B01J23/745 , B01J21/185 , B01J23/24 , B01J23/40 , B01J23/70 , B01J23/74 , B01J23/75 , B01J31/06 , B01J35/1014 , B01J35/1019 , B01J37/0201 , B01J37/0203 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/02 , C01B2202/06 , D01F9/127
摘要： The present invention relates to a method for preparing carbon fibrils and/or nanotubes from a carbon source integrated in the catalyst used for their preparation and a source of hydrocarbonated gas, as well as to the catalyst material and to the corresponding method. The catalyst material for preparing mono- or multi-leaved carbon fibrils and/or nanotubes includes one or more given multivalent transition metals and a hydrocarbonated solid organic substrate.
摘要翻译：本发明涉及一种用于制备碳原子纤维和/或纳米管的方法，所述碳原子纤维和/或纳米管由集成在用于其制备的催化剂中的碳源和烃化气体源以及催化剂材料以及相应的方法制备。用于制备单层或多层碳原子纤维和/或纳米管的催化剂材料包括一种或多种给定的多价过渡金属和烃化的固体有机底物。

9. 发明授权

US06652626B1 Agglomerated adsorbent, process for the production thereof and use thereof for the non-cryogenic separation of industrial gases 失效
标题翻译：聚集吸附剂，其生产方法及其用于工业气体的非低温分离的用途
公开(公告)号：US06652626B1
公开(公告)日：2003-11-25
申请号：US09118083
申请日：1998-07-17
申请人： Dominique Plee
发明人： Dominique Plee
IPC分类号： B01D53047
CPC分类号： B01D53/02 , B01D53/047 , B01D53/0476 , B01D2253/108 , B01D2253/30 , B01D2256/10 , B01D2256/16 , B01D2257/102 , B01D2257/406 , B01D2257/502 , B01D2257/504 , B01D2257/7022 , B01J20/183 , B01J20/186 , C01B3/56 , C01B13/027 , C01B21/0466 , C01B2203/0465 , C01B2203/047 , C01B2210/0046 , Y02C10/08 , Y02P20/152 , Y10S95/902
摘要： A description is given of agglomerates of faujasite X with an Si/Al ratio of 1, the inert binder of which, on the one hand, has been converted to active zeolite by conversion to zeolite in an alkaline liquor, and which have been subjected, on the other hand, to an exhaustive lithium exchange. These adsorbents develop a nitrogen adsorption capacity (1 bar/25° C.) of at least 26 cm3/g, which makes them excellent adsorbents for the non-cryogenic separation of gases from air and for the purification of hydrogen.
摘要翻译：对Si / Al比为1的八面沸石X的凝聚物进行了说明，其惰性粘合剂一方面通过在碱性液体中转化为沸石而转化为活性沸石，另一方面，进行详尽的锂离子交换。这些吸附剂产生至少26cm 3 / g的氮吸附能力（1巴/ 25℃），这使得它们对来自空气的气体的非低温分离和氢的净化具有优异的吸附剂。

10. 发明授权

US06649556B2 Process for the preparation of agglomerated zeolites X and LSX exchanged with lithium 失效
标题翻译：用于与锂交换的附聚沸石X和LSX的制备方法
公开(公告)号：US06649556B2
公开(公告)日：2003-11-18
申请号：US09897117
申请日：2001-07-03
申请人： Jean-Jacques Masini , Dominique Plee , Jean-Claude Sacleux , Jean-Louis Vidal
发明人： Jean-Jacques Masini , Dominique Plee , Jean-Claude Sacleux , Jean-Louis Vidal
IPC分类号： B01J2908
CPC分类号： B01D53/02 , B01D2253/108 , B01J20/183 , B01J20/186 , C01B39/026
摘要： Process for preparing zeolites of X type having an Si/Al atomic ratio of ≦1.5 and having exchangeable cations including lithium, trivalent and/or divalent ions, and optionally sodium, potassium, ammonium and/or hydronium ions, involves distributing starting zeolite in a series of receptacles, percolating a solution of at least one lithium compound through the series, drawing a lithium-containing bleed from first receptacle of the carrousel, and drawing off a final effluent stream from a final receptacle in the series. The effluent stream contains compounds of exchangeable cations from the starting zeolite and traces of the lithium compound(s). After a desired degree of lithium exchange has occurred in the first receptacle, the first receptacle is removed and a fresh solution of at least one lithium compound is introduced into the next receptable in the series and percolated through the series. This step can be performed for each receptacle in the series.
摘要翻译：具有Si / Al原子比<= 1.5且具有可交换阳离子，包括锂，三价和/或二价离子以及任选的钠，钾，铵和/或水合氢离子的X型沸石的方法涉及将起始沸石分配在一系列容器，渗透通过该系列的至少一种锂化合物的溶液，从转盘的第一容器中抽出含锂的液体，并从该系列中的最终容器中抽出最终的流出物流。流出物流含有起始沸石和痕量的锂化合物的可交换阳离子化合物。在第一容器中发生所需程度的锂交换之后，移除第一容器，并将至少一种锂化合物的新鲜溶液引入到下一个可接收的串联中并通过该系列进行渗滤。可以对系列中的每个插座执行此步骤。

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