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1. 发明授权

US10112887B2 Catalysts based on amino-sulfide ligands for hydrogenation and dehydrogenation processes 有权
公开(公告)号：US10112887B2
公开(公告)日：2018-10-30
申请号：US15286975
申请日：2016-10-06
申请人： Dmitri Goussev , Denis Spasyuk , Samantha Smith
发明人： Dmitri Goussev , Denis Spasyuk , Samantha Smith
IPC分类号： C07C67/40 , C07C323/25 , C07C5/03 , C07C209/52 , C01B3/26 , C07C5/08 , C07C45/00 , C07C29/147 , C07C41/18 , C07C67/00 , B01J31/18 , B01J31/22 , B01J31/20 , B01J31/24 , C01B3/02 , C01B3/04 , C07F15/00
摘要： The present application discloses novel amino-sulfide metal catalysts for organic chemical syntheses including hydrogenation (reduction) of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, oils and fats, resulting in alcohols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for a variety of chemicals.

2. 发明授权

US10173209B2 Complex catalysts based on amino-phosphine ligands for hydrogenation and dehydrogenation processes 有权
公开(公告)号：US10173209B2
公开(公告)日：2019-01-08
申请号：US14776947
申请日：2014-03-17
申请人： Dmitri Goussev , Denis Spasyuk
发明人： Dmitri Goussev , Denis Spasyuk
IPC分类号： C07F15/00 , C07F9/28 , B01J31/24 , C07F9/58 , C07B31/00 , C07B33/00 , C01B3/26 , B01J31/18 , B01J31/20 , C07C29/147 , C07C37/56
摘要： The present application discloses novel PWNN and PWNWP metal catalysts for organic chemical syntheses including hydrogenation (reduction) of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, enals, enones, enolates, oils and fats, resulting in alcohols, enols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for a variety of chemicals.

3. 发明申请

US20170073298A1 CATALYSTS BASED ON AMINO-SULFIDE LIGANDS FOR HYDROGENATION AND DEHYDROGENATION PROCESSES 审中-公开
标题翻译：基于氢化和脱氢方法的氨基硫化物的催化剂
公开(公告)号：US20170073298A1
公开(公告)日：2017-03-16
申请号：US15286975
申请日：2016-10-06
申请人： Dmitri Goussev , Denis Spasyuk , Samantha Smith
发明人： Dmitri Goussev , Denis Spasyuk , Samantha Smith
IPC分类号： C07C67/40 , C07F15/00 , B01J31/18 , C07C5/03 , B01J31/22 , B01J31/24
CPC分类号： C07C67/40 , B01J31/1805 , B01J31/1895 , B01J31/20 , B01J31/22 , B01J31/226 , B01J31/2295 , B01J31/2404 , B01J2231/641 , B01J2231/643 , B01J2231/645 , B01J2231/70 , B01J2231/763 , B01J2531/0238 , B01J2531/821 , B01J2531/825 , C01B3/02 , C01B3/04 , C01B3/26 , C01B2203/0277 , C01B2203/1064 , C07C5/03 , C07C5/08 , C07C29/147 , C07C41/18 , C07C45/002 , C07C67/00 , C07C209/52 , C07C323/25 , C07C2531/22 , C07C2531/24 , C07F15/0026 , C07F15/0046 , C07F15/0053 , Y02E60/364 , C07C211/45 , C07C9/06 , C07C9/15 , C07C15/073 , C07C47/06
摘要： The present application discloses novel amino-sulfide metal catalysts for organic chemical syntheses including hydrogenation (reduction) of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, oils and fats, resulting in alcohols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for a variety of chemicals.
摘要翻译：本申请公开了用于有机化学合成的新型氨基硫化物金属催化剂，包括不饱和化合物的氢化（还原）或底物脱氢。氢化底物化合物的范围包括酯，内酯，油和脂肪，产生作为反应产物的醇，二醇和三醇。目前应用的催化剂可用于在无溶剂条件下催化氢化反应。本发明的催化剂还允许氢化进行而不加入碱，并且可以代替使用主要组分的氢化物的常规还原方法。此外，本申请的催化剂可以在均匀和/或无接受条件下催化脱氢反应。因此，本文提供的催化剂可用于显着降低成本并改善各种化学品的制造方法的环境特征。

4. 发明授权

US11305268B2 Hydrogenation and dehydrogenation catalyst, and methods of making and using the same 有权
公开(公告)号：US11305268B2
公开(公告)日：2022-04-19
申请号：US16740764
申请日：2020-01-13
申请人： Dmitri Goussev , Denis Spasyuk
发明人： Dmitri Goussev , Denis Spasyuk
IPC分类号： B01J31/00 , B01J31/24 , C07F15/00 , C07F9/58 , C07B31/00 , B01J31/20 , B01J31/22 , C01B3/02 , C07C29/149 , C07C41/18 , C07C209/70 , B01J31/18
摘要： The present application discloses complexes useful as catalysts for organic chemical synthesis including hydrogenation and dehydrogenation of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, oils and fats, resulting in alcohols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for variety of chemicals.

5. 发明授权

US10583427B2 Hydrogenation and dehydrogenation catalyst, and methods of making and using the same 有权
公开(公告)号：US10583427B2
公开(公告)日：2020-03-10
申请号：US14239179
申请日：2012-08-20
申请人： Dmitri Goussev , Denis Spasyuk
发明人： Dmitri Goussev , Denis Spasyuk
IPC分类号： B01J31/00 , B01J31/24 , C07F15/00 , C07F9/58 , C07B31/00 , B01J31/20 , B01J31/22 , C01B3/02 , C07C29/149 , C07C41/18 , C07C209/70 , B01J31/18
摘要： The present application discloses complexes useful as catalysts for organic chemical synthesis including hydrogenation and dehydrogenation of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, oils and fats, resulting in alcohols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for variety of chemicals.

6. 发明申请

US20160023200A1 COMPLEX CATALYSTS BASED ON AMINO-PHOSPHINE LIGANDS FOR HYDROGENATION AND DEHYDROGENATION PROCESSES 审中-公开
标题翻译：基于用于氢化和脱氢方法的氨基磷酸化合物的复合催化剂
公开(公告)号：US20160023200A1
公开(公告)日：2016-01-28
申请号：US14776947
申请日：2014-03-17
申请人： Dmitri GOUSSEV , Denis SPASYUK
发明人： Dmitri Goussev , Denis Spasyuk
IPC分类号： B01J31/24 , B01J31/20 , C07C29/147 , C07F15/00 , C07C37/56 , B01J31/18 , C07F9/58
CPC分类号： B01J31/2461 , B01J31/1815 , B01J31/189 , B01J31/20 , B01J31/2404 , B01J2231/643 , B01J2231/763 , B01J2531/0244 , B01J2531/70 , B01J2531/821 , B01J2531/825 , B01J2531/84 , C01B3/26 , C01B2203/1047 , C01B2203/1076 , C07B31/00 , C07B33/00 , C07C29/147 , C07C37/56 , C07C2601/02 , C07F9/58 , C07F15/002 , C07F15/0046 , Y02E60/364
摘要： The present application discloses novel PWNN and PWNWP metal catalysts for organic chemical syntheses including hydrogenation (reduction) of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, enals, enones, enolates, oils and fats, resulting in alcohols, enols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for a variety of chemicals.
摘要翻译：本申请公开了用于有机化学合成的新型PWNN和PWNWP金属催化剂，包括不饱和化合物的氢化（还原）或底物脱氢。氢化底物化合物的范围包括酯，内酯，烯醛，烯酮，烯醇酯，油和脂肪，产生醇，烯醇，二醇和三醇作为反应产物。目前应用的催化剂可用于在无溶剂条件下催化氢化反应。本发明的催化剂还允许氢化进行而不加入碱，并且可以代替使用主要组分的氢化物的常规还原方法。此外，本申请的催化剂可以在均匀和/或无接受条件下催化脱氢反应。因此，本文提供的催化剂可用于显着降低成本并改善各种化学品的制造方法的环境特征。

7. 发明申请

US20150202609A1 Catalysts based on Amino-Sulfide Ligands for Hydrogenation and Dehydrogenation Processes 审中-公开
标题翻译：基于用于氢化和脱氢过程的氨基硫化物配体的催化剂
公开(公告)号：US20150202609A1
公开(公告)日：2015-07-23
申请号：US14426049
申请日：2013-09-04
申请人： Dmitri GOUSSEV , Denis SPASYUK , Samantha SMITH
发明人： Dmitri Goussev , Denis Spasyuk , Samantha Smith
IPC分类号： B01J31/22 , B01J31/20 , C01B3/02 , C07C41/18 , C07F15/00 , C07C67/00 , C07C29/147 , C07C209/52 , B01J31/24 , C01B3/04
CPC分类号： C07C67/40 , B01J31/1805 , B01J31/1895 , B01J31/20 , B01J31/22 , B01J31/226 , B01J31/2295 , B01J31/2404 , B01J2231/641 , B01J2231/643 , B01J2231/645 , B01J2231/70 , B01J2231/763 , B01J2531/0238 , B01J2531/821 , B01J2531/825 , C01B3/02 , C01B3/04 , C01B3/26 , C01B2203/0277 , C01B2203/1064 , C07C5/03 , C07C5/08 , C07C29/147 , C07C41/18 , C07C45/002 , C07C67/00 , C07C209/52 , C07C323/25 , C07C2531/22 , C07C2531/24 , C07F15/0026 , C07F15/0046 , C07F15/0053 , Y02E60/364 , C07C211/45 , C07C9/06 , C07C9/15 , C07C15/073 , C07C47/06
摘要： The present application discloses novel amino-sulfide metal catalysts for organic chemical syntheses including hydrogenation (reduction) of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, oils and fats, resulting in alcohols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for a variety of chemicals.
摘要翻译：本申请公开了用于有机化学合成的新型氨基硫化物金属催化剂，包括不饱和化合物的氢化（还原）或底物脱氢。氢化底物化合物的范围包括酯，内酯，油和脂肪，产生作为反应产物的醇，二醇和三醇。目前应用的催化剂可用于在无溶剂条件下催化氢化反应。本发明的催化剂还允许氢化进行而不加入碱，并且可以代替使用主要组分的氢化物的常规还原方法。此外，本申请的催化剂可以在均匀和/或无接受条件下催化脱氢反应。因此，本文提供的催化剂可用于显着降低成本并改善各种化学品的制造方法的环境特征。

8. 发明申请

US20140328748A1 HYDROGENATION AND DEHYDROGENATION CATALYST, AND METHODS OF MAKING AND USING THE SAME 审中-公开
标题翻译：氢化脱氢催化剂及其制备方法和使用方法
公开(公告)号：US20140328748A1
公开(公告)日：2014-11-06
申请号：US14239179
申请日：2012-08-20
申请人： Dmitri Goussev , Denis Spasyuk
发明人： Dmitri Goussev , Denis Spasyuk
IPC分类号： B01J31/24 , C07C209/70 , C07C29/149 , C07C41/18 , C01B3/02 , B01J31/22
摘要： The present application discloses complexes useful as catalysts for organic chemical synthesis including hydrogenation and dehydrogenation of unsaturated compounds or dehydrogenation of substrates. The range of hydrogenation substrate compounds includes esters, lactones, oils and fats, resulting in alcohols, diols, and triols as reaction products. The catalysts of current application can be used to catalyze a hydrogenation reaction under solvent free conditions. The present catalysts also allow the hydrogenation to proceed without added base, and it can be used in place of the conventional reduction methods employing hydrides of the main-group elements. Furthermore, the catalysts of the present application can catalyze a dehydrogenation reaction under homogenous and/or acceptorless conditions. As such, the catalysts provided herein can be useful in substantially reducing cost and improving the environmental profile of manufacturing processes for variety of chemicals.
摘要翻译：本申请公开了可用作有机化学合成催化剂的复合物，包括不饱和化合物的氢化和脱氢或底物脱氢。氢化底物化合物的范围包括酯，内酯，油和脂肪，产生作为反应产物的醇，二醇和三醇。目前应用的催化剂可用于在无溶剂条件下催化氢化反应。本发明的催化剂还允许氢化进行而不加入碱，并且可以代替使用主要组分的氢化物的常规还原方法。此外，本申请的催化剂可以在均匀和/或无接受条件下催化脱氢反应。因此，本文提供的催化剂可大大降低成本并改善各种化学品的制造方法的环境特征。

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