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1. 发明授权

US5997715A Method of electrochemically producing epoxides 失效
标题翻译：电化学生产环氧化物的方法
公开(公告)号：US5997715A
公开(公告)日：1999-12-07
申请号：US112659
申请日：1998-07-09
申请人： David G. Roberts , Peter C. Foller , Robert H. Tang , Yingchao Zhang , James R. Franks
发明人： David G. Roberts , Peter C. Foller , Robert H. Tang , Yingchao Zhang , James R. Franks
IPC分类号： C07D301/26 , C25B3/02 , C25B3/04 , C25B3/00
CPC分类号： C07D301/14 , C07D301/26 , C25B3/04 , Y02P20/582
摘要： Describes a method of electrochemically converting .alpha.-halohydrins, e.g., 1-chloro-2-hydroxypropane and 1,3-dichloro-2-hydroxypropane, to epoxides, e.g., propylene oxide and epichlorohydrin. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and anion exchange membrane, (2) an anolyte compartment containing an anode assembly comprising an anode and a cation exchange membrane, and (3) an intermediate compartment partitioned from the catholyte and anolyte compartments by the anion and cation exchange membranes respectively. An aqueous solution of .alpha.-halohydrin is charged to the catholyte compartment, while hydrogen halide solutions are charged to the intermediate and anolyte compartments. Direct current is passed through the electrolytic cell and an aqueous solution comprising epoxide is removed from the catholyte compartment.
摘要翻译：描述了将α-卤代醇如1-氯-2-羟基丙烷和1,3-二氯-2-羟基丙烷电化学转化为环氧化物如环氧丙烷和表氯醇的方法。提供一种三室电解池，其具有（1）阴极电解室，其包含阴极组件和阴离子交换膜;（2）阳极室，其包含阳极和阳离子交换膜;以及（3）中间隔室分别由阴离子和阳极电解质隔室分隔开。将α-卤代醇的水溶液加入到阴极电解液室中，同时将卤化氢溶液加入到中间体和阳极电解液室中。直流电流通过电解槽，从阴极电解液隔室除去包含环氧化物的水溶液。

2. 发明授权

US5900133A Method of converting amine hydrohalide into free amine 失效
标题翻译：将胺氢卤化物转化为游离胺的方法
公开(公告)号：US5900133A
公开(公告)日：1999-05-04
申请号：US914600
申请日：1997-08-18
申请人： Peter C. Foller , David G. Roberts , Robert H. Tang , James R. Franks
发明人： Peter C. Foller , David G. Roberts , Robert H. Tang , James R. Franks
IPC分类号： B01D61/44 , C25B3/00 , C25B1/00 , C25B7/00 , C25B15/00
CPC分类号： C25B3/00 , B01D61/44
摘要： Describes a method of electrochemically converting amine hydrohalide, e.g., ethyleneamine hydrochloride, into free amine, e.g., free ethyleneamine. A three compartment electrolytic cell is provided having (1) a catholyte compartment containing a cathode assembly comprising a cathode and anion exchange membrane, (2) an anolyte compartment containing an anode assembly comprising an anode and a cation exchange membrane, and (3) an intermediate compartment separated from the catholyte and anolyte compartments by the anion and cation exchange membranes respectively. An aqueous solution of amine hydrohalide is charged to the catholyte compartment, while hydrogen halide solutions are charged to the intermediate and anolyte compartments. Direct current is passed through the electrolytic cell and an aqueous solution comprising free amine is removed from the catholyte compartment.
摘要翻译：描述了将胺氢卤化物（例如乙烯胺盐酸盐）电化学转化成游离胺，例如游离亚乙基胺的方法。提供一种三室电解池，其具有（1）阴极电解室，其包含阴极组件和阴离子交换膜;（2）阳极室，其包含阳极和阳离子交换膜;以及（3）中间室分别通过阴离子和阳离子交换膜与阴极电解液和阳极电解质隔室分离。将胺氢卤化物的水溶液加入到阴极电解液室中，同时将卤化氢溶液装入中间体和阳极电解液室。直流电流通过电解槽，并从阴极电解液隔室除去包含游离胺的水溶液。

3. 发明申请

US20090183455A1 LOAD BEARING ASSEMBLY 失效
标题翻译：负载轴承总成
公开(公告)号：US20090183455A1
公开(公告)日：2009-07-23
申请号：US12327042
申请日：2008-12-03
申请人： Dale E. Polk, JR. , James R. Franks
发明人： Dale E. Polk, JR. , James R. Franks
IPC分类号： B32B3/12 , E04C2/26
CPC分类号： E04C2/427 , B32B3/12 , E04C2/20 , E04C2/365 , Y10T428/24149 , Y10T428/24157
摘要： A load bearing assembly (300, 452) that includes at least one molded plastic panel (1) and/or at least one molded plastic panel assembly (3), a first support (303) and optionally a second support (306), is described. Each panel (1) of the load bearing assembly (300) includes a first external portion (17) and a second external portion (20), each having a plurality of reinforcing structures (49, 79) having sidewalls (52, 82) that define a plurality of external portion recesses (64, 98). Each support (303, 306) has a plurality of extensions (318, 339) that are received within the external portion recesses (64, 98) of the panel with which they are aligned. Receipt of the support extensions (318, 339) within the external portion recesses (64, 98) of the panel serves to attach the molded panel and the support(s) together, thereby forming the load bearing assembly (300). The invention also relates to a load bearing assembly (452) that includes a panel assembly (3) formed from a plurality of molded panels (1, 1a, 1b) having overlapping external (17, 20) and center (14) portions that interlockingly attach the panels together. Each panel assembly has a first free external portion (443) and a second free external portion (446), each having a plurality of external portion recesses (64, 98) into which are received the extensions (318, 339) of the respectively aligned supports (303, 306), thereby forming the load bearing assembly (452). The panel assemblies may be used to form at least a portion of a structure, such as a walkway, dock, wall, roof, shelf or chair.
摘要翻译：包括至少一个模制塑料板（1）和/或至少一个模制塑料板组件（3），第一支撑件（303）和任选的第二支撑件（306）的承载组件（300,452）是描述。承载组件（300）的每个面板（1）包括第一外部部分（17）和第二外部部分（20），每个外部部分（20）具有多个具有侧壁（52,82）的加强结构（52,72）限定多个外部凹部（64,98）。每个支撑件（303,306）具有多个延伸部（318,339），所述多个延伸部分（318,339）被容纳在与它们对准的面板的外部凹部（64,98）内。在面板的外部凹部（64,98）内接收支撑延伸部（318,339）用于将模制板和支撑件连接在一起，从而形成承重组件（300）。本发明还涉及一种承载组件（452），其包括由具有重叠的外部（17,20）和中心（14）部分的多个模制板（1,1a，1b）形成的面板组件（3）将面板连接在一起。每个面板组件具有第一自由外部部分（443）和第二自由外部部分（446），每个外部部分具有多个外部部分凹部（64,98），所述多个外部部分凹部（64,98）被接收到分别对准的延伸部（318,333）（303,306），由此形成承重组件（452）。面板组件可用于形成结构的至少一部分，例如人行道，码头，墙壁，屋顶，搁架或椅子。

4. 发明授权

US06265489B1 Thermosetting compositions containing carboxylic acid functional polymers prepared by atom transfer radical polymerization 失效
标题翻译：含有通过原子转移自由基聚合制备的羧酸官能聚合物的热固性组合物
公开(公告)号：US06265489B1
公开(公告)日：2001-07-24
申请号：US09375017
申请日：1999-08-16
申请人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
发明人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
IPC分类号： C08L3302
CPC分类号： C09D133/02 , C08L63/00 , C09D133/064 , C08L2666/14
摘要： A thermosetting composition comprising a co-reactable solid, particulate mixture of (a) polycarboxylic acid functional polymer, and (b) epoxide functional crosslinking agent having at least two epoxide groups, e.g., triglycidyl isocyanurate (TGIC), is described. The polycarboxylic acid functional polymer is prepared by atom transfer radical polymerization and has well defined polymer chain architecture and polydispersity index of less than 2.0. The thermosetting compositions of the present invention have utility as powder coatings compositions.
摘要翻译：描述了包含（a）多元羧酸官能聚合物和（b）具有至少两个环氧基团的环氧官能交联剂例如三缩水甘油基异氰脲酸酯（TGIC）的共反应固体，颗粒混合物的热固性组合物。聚羧酸官能聚合物通过原子转移自由基聚合制备，并且具有良好的聚合物链结构和小于2.0的多分散指数。本发明的热固性组合物可用作粉末涂料组合物。

5. 发明授权

US06482475B2 Thermosetting compositions containing hydroxy functional polymers prepared by atom transfer radical polymerization 失效
标题翻译：含有通过原子转移自由基聚合制备的羟基官能聚合物的热固性组合物
公开(公告)号：US06482475B2
公开(公告)日：2002-11-19
申请号：US09934385
申请日：2001-08-21
申请人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
发明人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
IPC分类号： C08G1862
CPC分类号： C08G18/8074 , C08F293/00 , C08F293/005 , C08F2438/01 , C08G18/6229 , C08G2150/20 , C09D153/00 , Y10T428/31504 , C08L2666/02
摘要： A thermosetting composition comprising a co-reactable solid, particulate mixture of (a) capped polyisocyanate crosslinking agent, e.g., a trimer of 1-isocyanato-3,3,5 -trimethyl-5-isocyanatomethylcyclohexane capped with e-caprolactam or 1H-2,5-dimethyl pyrazole, and (b) hydroxy functional polymer, is described. The hydroxy functional polymer is prepared by atom transfer radical polymerization and has well defined polymer chain architecture and polydispersity index of less than 2.5. The thermosetting compositions of the present invention have utility as powder coatings compositions.
摘要翻译：一种热固性组合物，其包含（a）封端的多异氰酸酯交联剂，例如用ε-己内酰胺或1H-2封端的1-异氰酸酯基-3,3,5-三甲基-5-异氰酸甲酯基环己烷的三聚体的可共反应的固体颗粒混合物，5-二甲基吡唑和（b）羟基官能聚合物。羟基官能聚合物通过原子转移自由基聚合制备，并且具有明确的聚合物链结构和小于2.5的多分散指数。本发明的热固性组合物可用作粉末涂料组合物。

6. 发明授权

US06391391B1 Coating substrate with atom transfer radical polymerized carboxyl polymer and polyepoxide 有权
公开(公告)号：US06391391B1
公开(公告)日：2002-05-21
申请号：US09855370
申请日：2001-05-15
申请人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
发明人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
IPC分类号： B05D302
摘要： A thermosetting composition comprising a co-reactable solid, particulate mixture of (a) polycarboxylic acid functional polymer, and (b) epoxide functional crosslinking agent having at least two epoxide groups, e.g., triglycidyl isocyanurate (TGIC), is described. The polycarboxylic acid functional polymer is prepared by atom transfer radical polymerization and has well defined polymer chain architecture and polydispersity index of less than 2.0. The thermosetting compositions of the present invention have utility as powder coatings compositions.

7. 发明授权

US06319988B1 Thermosetting compositions containing hydroxy functional polymers prepared by atom transfer radical polymerization 失效
标题翻译：含有通过原子转移自由基聚合制备的羟基官能聚合物的热固性组合物
公开(公告)号：US06319988B1
公开(公告)日：2001-11-20
申请号：US09375015
申请日：1999-08-16
申请人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
发明人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
IPC分类号： C08F440
CPC分类号： C08G18/8074 , C08F293/00 , C08F293/005 , C08F2438/01 , C08G18/6229 , C08G2150/20 , C09D153/00 , Y10T428/31504 , C08L2666/02
摘要： A thermosetting composition comprising a co-reactable solid, particulate mixture of (a) capped polyisocyanate crosslinking agent, e.g., a trimer of 1-isocyanato-3,3,5-trimethyl-5-isocyanatomethylcyclohexane capped with e-caprolactam or 1H-2,5-dimethyl pyrazole, and (b) hydroxy functional polymer, is described. The hydroxy functional polymer is prepared by atom transfer radical polymerization and has well defined polymer chain architecture and polydispersity index of less than 2.5. The thermosetting compositions of the present invention have utility as powder coatings compositions.
摘要翻译：一种热固性组合物，其包含（a）封端的多异氰酸酯交联剂的共可反应固体颗粒混合物，例如用ε-己内酰胺或1H-2封端的1-异氰酸酯基-3,3,5-三甲基-5-异氰酸甲酯基环己烷的三聚体，5-二甲基吡唑和（b）羟基官能聚合物。羟基官能聚合物通过原子转移自由基聚合制备，并且具有明确的聚合物链结构和小于2.5的多分散指数。本发明的热固性组合物可用作粉末涂料组合物。

8. 发明授权

US5972809A Waterborne coating compositions 失效
标题翻译：水性涂料组合物
公开(公告)号：US5972809A
公开(公告)日：1999-10-26
申请号：US16910
申请日：1998-02-02
申请人： Dennis L. Faler , James R. Franks , Roxalana L. Martin
发明人： Dennis L. Faler , James R. Franks , Roxalana L. Martin
IPC分类号： C08F283/01 , C09D151/08 , C09D167/06 , D06M15/507 , D06M15/51 , D06M23/08 , D06N3/12 , D06P1/44 , D06P1/52 , B32B27/12
CPC分类号： D06P1/5271 , C08F283/01 , C09D151/08 , C09D167/06 , D06M15/507 , D06M15/51 , D06M23/08 , D06N3/121 , D06P1/44 , Y10T442/2361
摘要： The present invention provides a waterborne coating composition which includes a polymeric film-forming resin. The polymeric film-forming resin includes a dispersion of polymeric microparticles prepared by forming, in aqueous medium, a mixture of: (a) an unsaturated, substantially hydrophobic polyester component, and (b) an ethylenically unsaturated monomer component. With various hydrophobic polyesters, the ethylenically unsaturated monomer component of the polymeric film-forming resin includes: (a) an acrylamide or methacrylamide with N-methylol or N-alkoxymethyl functionality, (b) an alpha-beta ethylenically unsaturated compound with carboxyl functionality, and (c) an alpha-beta ethylenically unsaturated compound with no additional reactive functionality. Such a waterborne coating composition has a low V.O.C., provides added stiffness, does not block, and can be applied in such a manner that it does not substantially mask the texture of the nonwoven fabrics and/or textiles over which it is applied. When the hydrophobic polyester is prepared with polycarboxylic acid and about 45 to 75 percent by weight 2,2,4-trimethyl-1,3-pentanediol, and about 0 to 23 percent by weight 2-ethyl-2-(hydroxymethyl)-1,3-propanediol, various mixtures of ethylenically unsaturated monomer(s) can be used. The percents by weight are based on total weight of the substantially hydrophobic polyester mixtures of ethylenically unsaturated monomer(s). These are particularized into microparticles by high-stress techniques followed by polymerizing the polymerizable species to form the polymeric microparticles which are stably dispersed in the aqueous medium.
摘要翻译：本发明提供一种水性涂料组合物，其包含聚合物成膜树脂。聚合物成膜树脂包括通过在水性介质中形成以下混合物制备的聚合物微粒的分散体：（a）不饱和的，基本上疏水的聚酯组分和（b）烯属不饱和单体组分的混合物。对于各种疏水聚酯，聚合物成膜树脂的烯属不饱和单体组分包括：（a）具有N-羟甲基或N-烷氧基甲基官能团的丙烯酰胺或甲基丙烯酰胺，（b）具有羧基官能团的α-β-烯属不饱和化合物，和（c）不具有额外的反应性官能团的α-β烯键式不饱和化合物。这种水性涂料组合物具有低的V.O.C.，提供增加的刚度，不阻挡，并且可以以这样的方式施加，使得其基本上不掩盖其所施加的无纺布和/或织物的织构。当疏水性聚酯用多元羧酸和约45-75％（重量）2,2,4-三甲基-1,3-戊二醇制备，和约0-23％（重量）2-乙基-2-（羟甲基）-1 可以使用3-丙二醇，各种烯属不饱和单体的混合物。重量百分数是基于烯键式不饱和单体的基本上疏水的聚酯混合物的总重量。这些通过高应力技术特别化为微粒，然后聚合可聚合物质以形成稳定分散在水性介质中的聚合物微粒。

9. 发明授权

US5212245A Thermosetting powder coating compositions containing flow modifiers 失效
标题翻译：含有流动改性剂的热固性粉末涂料组合物
公开(公告)号：US5212245A
公开(公告)日：1993-05-18
申请号：US845571
申请日：1992-03-04
申请人： James R. Franks , Paul H. Pettit, Jr.
发明人： James R. Franks , Paul H. Pettit, Jr.
IPC分类号： B05D1/36 , B05D7/24 , C08L33/06 , C09D5/03 , C09D5/46 , C09D133/04 , C09D133/06 , C09D133/12 , C09D133/14 , C09D163/00
CPC分类号： C09D163/00 , C09D133/12 , C09D5/037 , C08L33/066 , Y10S524/904 , Y10S525/934 , Y10T428/263 , Y10T428/264 , Y10T428/31678
摘要： Thermosetting powder coating compositions comprising a curable particulate resinous material and a flow control agent which is a copolymer of an alkyl acrylate or methacrylate containing from 6 to 20 carbon atoms in the alkyl group and a hydroxyalkyl acrylate or methacrylate. The flow modifiers enhance the rheology of the thermosetting powder coating composition providing for smoother coatings while at the same time not adversely affecting appearance or adhesion with associated coatings, for example, previously applied electrodeposited primers or subsequently applied topcoats.
摘要翻译：包含可固化颗粒状树脂材料的热固性粉末涂料组合物和作为烷基中含有6至20个碳原子的丙烯酸烷基酯或甲基丙烯酸烷基酯和丙烯酸酯或甲基丙烯酸羟烷基酯的共聚物的流动控制剂。流动改性剂增强热固性粉末涂料组合物的流变性，其提供更平滑的涂层，同时不会对相关涂层的外观或粘附性产生不利影响，例如先前施加的电沉积引物或随后应用的面漆。

10. 发明授权

US08091314B2 Load bearing assembly 失效
标题翻译：承重总成
公开(公告)号：US08091314B2
公开(公告)日：2012-01-10
申请号：US12327042
申请日：2008-12-03
申请人： Dale E. Polk, Jr. , James R. Franks
发明人： Dale E. Polk, Jr. , James R. Franks
IPC分类号： E04C2/00
CPC分类号： E04C2/427 , B32B3/12 , E04C2/20 , E04C2/365 , Y10T428/24149 , Y10T428/24157
摘要： A load bearing assembly (300, 452) that includes at least one molded plastic panel (1) and/or at least one molded plastic panel assembly (3), a first support (303) and optionally a second support (306), is described. Each panel (1) of the load bearing assembly (300) includes a first external portion (17) and a second external portion (20), each having a plurality of reinforcing structures (49, 79) having sidewalls (52, 82) that define a plurality of external portion recesses (64, 98).
摘要翻译：包括至少一个模制塑料板（1）和/或至少一个模制塑料板组件（3），第一支撑件（303）和任选的第二支撑件（306）的承载组件（300,452）是描述。承载组件（300）的每个面板（1）包括第一外部部分（17）和第二外部部分（20），每个外部部分（20）具有多个具有侧壁（52,82）的加强结构（52,72）限定多个外部凹部（64,98）。

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