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1. 发明授权

US4596653A Demulsifying process 失效
标题翻译：破乳过程
公开(公告)号：US4596653A
公开(公告)日：1986-06-24
申请号：US661711
申请日：1984-10-17
申请人： David E. Graham , Werner A. Lidy , Patrick C. McGrath , David G. Thompson
发明人： David E. Graham , Werner A. Lidy , Patrick C. McGrath , David G. Thompson
IPC分类号： B01D17/05 , B01D17/04 , C08G77/46 , C10G33/04
CPC分类号： C08G77/46 , B01D17/047 , C10G33/04
摘要： Emulsions of oil and water are broken by treating them with a demulsifier which is a polysiloxane polyalkylene oxide copolymer in which the polyalkylene oxide segment is composed of random ethylene oxide and propylene oxide units.The demulsifier is particularly useful in breaking emulsions of water in crude oil which are normally difficult to separate and in breaking emulsions at relatively low temperatures, e.g. 30.degree. to 45.degree. C.
摘要翻译：油和水的乳液通过用聚硅氧烷聚环氧烷共聚物的破乳剂处理而破坏，其中聚环氧烷链段由无规环氧乙烷和环氧丙烷单元组成。破乳剂特别可用于破碎原油中的水的乳液，其通常难于分离，并在相对低的温度下破乳。 30〜45℃

2. 发明授权

US4902433A Equipment and method for filtration using a fabric of polyacrylonitrile fibers 失效
标题翻译：使用聚丙烯腈纤维织物的过滤设备和方法
公开(公告)号：US4902433A
公开(公告)日：1990-02-20
申请号：US93129
申请日：1987-09-02
申请人： David E. Graham , Malcolm T. McKechnie , David G. Thompson
发明人： David E. Graham , Malcolm T. McKechnie , David G. Thompson
IPC分类号： B01D39/08 , B01D39/16 , E21B43/20
CPC分类号： B01D39/083 , B01D39/1623 , E21B43/20 , B01D2239/1233 , B01D2239/1291
摘要： A backwashable filter element consists essentially of a fabric of polyacrylonitrile fibres wherein the diameter of the fibres is in the range 10 to 50 microns and the density of the element is in the range 0.05 to 0.50 g/cc. The element is suitable for use in filtering sea water, particularly for sea water injected into petroleum reservoirs to assist in the recovery of crude oil.
摘要翻译：反冲洗过滤元件基本上由聚丙烯腈纤维织物组成，其中纤维的直径在10至50微米的范围内，元件的密度在0.05至0.50g / cc的范围内。该元素适用于过滤海水，特别是用于注入石油储层的海水，以协助回收原油。

3. 发明授权

US06432355B1 Corrosion inhibition during transport of water and a hydrocarbon through a pipeline 有权
标题翻译：通过管道运输水和碳氢化合物时的腐蚀抑制
公开(公告)号：US06432355B1
公开(公告)日：2002-08-13
申请号：US09416307
申请日：1999-10-12
申请人： Kirill N. Bakeev , Jui-Chang Chuang , Thomas Winkler , Michael A. Drzewinski , David E. Graham
发明人： Kirill N. Bakeev , Jui-Chang Chuang , Thomas Winkler , Michael A. Drzewinski , David E. Graham
IPC分类号： C23F1114
CPC分类号： C10L3/06 , Y10S585/95 , Y10T137/0329 , Y10T137/0391
摘要： Described herein is a process of corrosion inhibition of a steel pipeline during transport of water and gas, or water and an oil, or mixtures thereof, therethrough, including introducing a copolymer of vinyl caprolactam and vinylpyridine into said pipeline.
摘要翻译：本文描述的是在输送水和气体或水和油或其混合物的过程中钢管道的腐蚀抑制过程，包括将乙烯基己内酰胺和乙烯基吡啶的共聚物引入所述管道中。

4. 发明授权

US06369180B1 Process for making water soluble polyvinylcaprolactam polymers 有权
标题翻译：制备水溶性聚己内酰胺聚合物的方法
公开(公告)号：US06369180B1
公开(公告)日：2002-04-09
申请号：US09642545
申请日：2000-08-18
申请人： Jenn S. Shih , Donald I. Prettypaul , John Mc Kittrick , David E. Graham
发明人： Jenn S. Shih , Donald I. Prettypaul , John Mc Kittrick , David E. Graham
IPC分类号： C08J2608
CPC分类号： C08F26/06 , C08F220/60
摘要： A process of making a homopolymer of vinyl caprolactam (VCL), and a copolymer with dimethylaminopropyl methacrylamide (DMAPMA), optionally including with one or more polymerizable monomers (X), in the composition range, by weight, VCL 99 to 30%, DMAPMA 1-70% and monomer X 0-30%, respectively, by suspension polymerization in an aqueous/alcoholic solvent medium, without requiring a protective colloid, which comprises charging vinyl caprolactam in an aqueous/alcoholic solvent mixture, wherein the weight ratio of alcohol to total monomers is ⅙ to 3, and if present, forming a solution of DMAPMA and optional monomers in water, feeding the solution into the VCL charge at a predetermined rate, periodically adding initiator to the reaction mixture, and polymerizing at about 40° to 130° C., and, if desired, neutralizing the product, to form a polymer product at about 5% to 40% solids, homogeneously dispersed in the solvent.
摘要翻译：一种制备乙烯基己内酰胺（VCL）均聚物的方法，以及任选地包含一种或多种可聚合单体（X）的二甲基氨基丙基甲基丙烯酰胺（DMAPMA）的共聚物，其组成范围为VCL 99至30％，DMAPMA 1-70％和单体X 0-30％，通过在水/醇溶剂介质中的悬浮聚合，不需要保护胶体，其包括在乙醇/醇溶剂混合物中加入乙烯基己内酰胺，其中醇的重量比至总单体为⅙至3，如果存在，则在水中形成DMAPMA和任选单体的溶液，以预定的速率将溶液进料到VCL装料中，周期性地向反应混合物中加入引发剂，并在约40° 130℃，如果需要，中和产物，形成约5％至40％固体的均匀分散在溶剂中的聚合物产物。

5. 发明授权

US06281274B1 Method for preventing or retarding the formation of gas hydrates 有权
标题翻译：防止或延缓气体水合物形成的方法
公开(公告)号：US06281274B1
公开(公告)日：2001-08-28
申请号：US09415657
申请日：1999-10-12
申请人： Kirill N. Bakeev , Jui-Chang Chuang , Thomas Winkler , Michael A. Drzewinski , David E. Graham
发明人： Kirill N. Bakeev , Jui-Chang Chuang , Thomas Winkler , Michael A. Drzewinski , David E. Graham
IPC分类号： C07C720
CPC分类号： C10L3/06 , Y10S585/95 , Y10T137/0329 , Y10T137/0391
摘要： A composition for preventing or retarding the formation of gas hydrates during the transport of a fluid comprising water and a hydrocarbon through a conduit. The composition is a copolymer of vinyl caprolactam and vinyl pyridine, and terpolymers thereof, with vinyl pyrrolidone, preferably including 70-97% by weight vinyl caprolactam. Suitably such polymers have a molecular weight in the range of 500 to 2500, and are made in a polymerization solvent, preferably a glycol ether, most preferably, 2-butoxyethanol; and also including a carrier solvent, preferably monoethylene glycol.
摘要翻译：一种用于在通过导管输送包含水和烃的流体的过程中预防或阻止气体水化物的形成的组合物。该组合物是乙烯基己内酰胺和乙烯基吡啶及其三元共聚物与乙烯基吡咯烷酮的共聚物，优选包含70-97重量％的乙烯基己内酰胺。合适地，这种聚合物的分子量在500至2500的范围内，并且在聚合溶剂中，优选二醇醚，最优选2-丁氧基乙醇制备; 并且还包括载体溶剂，优选单乙二醇。

6. 发明授权

US4345937A Herbicidal N-(haloacetyl)-N-(N'-methylenepyrrolidonyl)-2-alkoxyanilines 失效
标题翻译：除草剂N-（卤代乙酰基）-N-（N'-亚甲基吡咯烷酮基）-2-烷氧基苯胺
公开(公告)号：US4345937A
公开(公告)日：1982-08-24
申请号：US962306
申请日：1978-11-20
申请人： Louis Schneider , David E. Graham
发明人： Louis Schneider , David E. Graham
IPC分类号： A01N43/36 , C07D207/26 , C07D207/27 , C07D207/263
CPC分类号： C07D207/27 , A01N43/36
摘要： Herbicidal N-(haloacetyl-N-(N'-methylenepyrrolidonyl)-2-alkoxyanilines are provided in this invention having the formula: ##STR1## where R is alkyl of 1-6 carbon atoms, R' is hydrogen or lower alkyl of 1-3 carbon atoms, and X is halogen.The compounds of the present invention show good herbicidal activity against grassy weeds.
摘要翻译：在本发明中提供了除草的N-（卤代乙酰基-N-（N'-亚甲基吡咯烷酮基）-2-烷氧基苯胺），其具有下式：其中R是1-6个碳原子的烷基，R'是氢或1的低级烷基 -3个碳原子，X为卤素，本发明化合物对草地杂草具有良好的除草活性。

7. 发明授权

US4154594A Aquatic herbicidal diacylimide compositions 失效
标题翻译：水生除草二酰亚胺组合物
公开(公告)号：US4154594A
公开(公告)日：1979-05-15
申请号：US930372
申请日：1978-08-02
申请人： Louis Schneider , David E. Graham
发明人： Louis Schneider , David E. Graham
IPC分类号： A01N37/26 , A01N9/20
CPC分类号： A01N37/26
摘要： The invention provides broad spectrum herbicidal diacylimide compositions which include compounds having the formula: ##STR1## where R and R' are selected from alkyl, alkenyl, haloalkyl and haloalkenyl having from 1-5 carbon atoms, being the same or different groups.The compositions of this invention show excellent agricultural herbicidal activity, particularly against foxtail millet, Japanese millet, crabgrass and pigweed, and aquatic herbicidal activity against lower and higher submerged aquatic plants.The diacylimide compounds generally are prepared by reacting a suitable amide with an acyl halide. The acyl halide precursor may be prepared, if necessary, from the corresponding acid by reaction with a suitable halogenating agent, such as thionyl chloride. Similarly, a given amide may be readily prepared, for example, from the corresponding acyl halide by reaction with ammonia.
摘要翻译：本发明提供广谱除草二酰亚胺组合物，其包括具有下式的化合物：其中R和R'选自具有1-5个碳原子的烷基，烯基，卤代烷基和卤代烯基，为相同或不同的基团。

8. 发明授权

US4086364A Fungicidal 2,6-dinitrodiphenylethers 失效
标题翻译：杀真菌剂2,6-二硝基二苯醚
公开(公告)号：US4086364A
公开(公告)日：1978-04-25
申请号：US743279
申请日：1976-11-19
申请人： Louis Schneider , David E. Graham
发明人： Louis Schneider , David E. Graham
IPC分类号： A01N33/22 , A61K31/04 , C07C43/28
CPC分类号： A01N33/22
摘要： Fungicidal 2,6-dinitrodiphenylethers having the formula: ##STR1## WHERE X is halogen,Y is methyl or trifluoromethyl,R is halogen or methyl, andn is 0-3.The compounds are useful against early blight of tomatoes, bean rust, rice spot and corn rust.
摘要翻译：具有下式的杀真菌2,6-二硝基二苯基醚：其中X为卤素，Y为甲基或三氟甲基，R为卤素或甲基，N为0-3。

9. 发明授权

US4086356A Fungicidal-N-(3-halo-2,6-dinitro-4-trifluoromethylphenyl)-pyrrolidones 失效
标题翻译：杀真菌剂-N-（3-卤代-2,6-二硝基-4-三氟甲基苯基） - 吡咯烷酮
公开(公告)号：US4086356A
公开(公告)日：1978-04-25
申请号：US765904
申请日：1977-02-07
申请人： Louis Schneider , David E. Graham
发明人： Louis Schneider , David E. Graham
IPC分类号： A01N43/36 , C07D207/24 , C07D207/26 , C07D207/27 , A61K31/40
CPC分类号： C07D207/27 , A01N43/36 , C07D207/24
摘要： Fungicidal-N-(3-halo-2,6-dinitro-4-trifluoromethylphenyl)-pyrrolidones having the formula: ##STR1## where X is a halogen,Y is oxygen or sulfur, andR is H or lower alkyl, of up to 4 carbon atoms,Are prepared by reacting a 2,4-dihalo-3,5-dinitrobenzotrifluoride with an alkali metal salt of a pyrrolidone.The compounds of the invention show good fungicidal activity, particularly against rice spot and tomato blight.
摘要翻译：具有下式的杀真菌-N-（3-卤代-2,6-二硝基-4-三氟甲基苯基） - 吡咯烷酮：其中X是卤素，Y是氧或硫，R是H或低级烷基，至4个碳原子，通过用吡咯烷酮的碱金属盐反应2,4-二氢-3,5-二氮杂萘并二氮吡喃制备。

10. 发明申请

US20180134740A1 NOVEL CROSSLINKED POLYMERIC SUBSTRATES METHODS OF PREPARATION AND END USE APPLICATIONS OF THE SUBSTRATES 审中-公开
公开(公告)号：US20180134740A1
公开(公告)日：2018-05-17
申请号：US15693823
申请日：2017-09-01
申请人： Warde T. Collins , Douglas H. Adamson , David E. Graham , Robert M. Mininni
发明人： Warde T. Collins , Douglas H. Adamson , David E. Graham , Robert M. Mininni
IPC分类号： C07H1/00 , C11D3/37 , C07K1/22 , B01J39/17 , A23C1/00 , A23C9/12 , A61K8/72 , A61Q11/00 , A61Q15/00 , A61Q17/04 , A61Q19/00 , B01D15/00 , B01D15/08 , B82Y30/00 , B01J41/20 , B01J41/12 , B01J39/26 , B01J20/32 , B01J20/286 , B01J20/28 , B01J20/10 , C02F1/28 , C02F1/42 , C02F101/00 , C02F101/20 , C02F1/00
CPC分类号： C07H1/00 , A23C1/00 , A23C9/1216 , A61K8/72 , A61Q11/00 , A61Q15/00 , A61Q17/04 , A61Q19/00 , B01D15/00 , B01D15/08 , B01J20/103 , B01J20/28007 , B01J20/28057 , B01J20/286 , B01J20/3204 , B01J20/3219 , B01J20/3242 , B01J20/3263 , B01J20/327 , B01J20/3272 , B01J20/3276 , B01J20/3278 , B01J20/3282 , B01J39/17 , B01J39/26 , B01J41/12 , B01J41/20 , B01J2220/54 , B01J2220/56 , B01J2220/58 , B82Y30/00 , C02F1/001 , C02F1/285 , C02F1/42 , C02F2101/006 , C02F2101/20 , C07K1/22 , C11D3/373 , Y10T428/31663 , Y10T428/31895 , Y10T442/2861
摘要： A composition of matter wherein the composition comprises a siliceous substrate having silanols on the surface and a polymer selected from the group consisting essentially of a water soluble polymer, a water soluble copolymer, an alcohol soluble polymer, an alcohol soluble copolymer, and combinations of such polymers, wherein the polymer is chemically bonded to the siliceous substrate by a silane linking material having the general formula O3/2SiQY that is derived from an alkoxy-functional silane having the general formula (RO)3SiQX and processes for preparing the crosslinked polymer that is chemically bonded to the surface of the siliceous substrate.

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