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1. 发明授权

US5229280A Process for the continuous biotechnological preparation of optical isomer S(+) of 2-(6-methoxy-2-naphthyl) propionic acid 失效
标题翻译： 2-（6-甲氧基-2-萘基）丙酸的光学异构体S（+）的连续生物制备方法
公开(公告)号：US5229280A
公开(公告)日：1993-07-20
申请号：US312976
申请日：1989-02-21
申请人： Daniele Bianchi , Pietro Cesti , Carlo Pina , Ezio Battistel
发明人： Daniele Bianchi , Pietro Cesti , Carlo Pina , Ezio Battistel
IPC分类号： C12N11/08 , C12P7/40 , C12P41/00 , C12R1/72
CPC分类号： C12N11/08 , C12P41/005 , C12P7/40 , Y10S435/921
摘要： Continuous biotechnological preparation of optical isomer S(+) of 2-(6-methoxy-2-naphthyl) propionic acid consisting in the reaction of a racemic (R,S) ester of 2-(6-methoxy-2-naphthyl) propionic acid having melting point below 50.degree. C. of formula: ##STR1## wherein R.sub.1 =a C.sub.2 -C.sub.10 alkyl, C.sub.4 -C.sub.6 cycloalkyl, phenyl, tetrahydropyranyl , tetrahydrofuranyl radicals and--(CH.sub.2 CH.sub.2 O).sub.n --R.sub.2 group, whereinn=2-15 andR.sub.2 =a C.sub.1 -C.sub.4 alkyl group, with the Lipase obtained from Candida Cylindracea, at temperatures ranging from 20.degree.-60.degree. C. and at a pH ranging from 5 to 8, by feeding said ester in a continuous way into a bioreactor containing said Lipase immobilized on a porous carrier selected from adsorbent resins of the polyacrylester type having a porosity ranging from 50 to 1000 .ANG. and a granulometry ranging from 1 to 0.01 mm.

2. 发明授权

US5302528A Process for the enzymatic separation of the optical isomers of alpha-substituted carboxylic acids using esterase from Brevibacterium imperiale 失效
标题翻译：使用来自Brevibacterium imperiale的酯酶酶分离α-取代羧酸的光学异构体的方法
公开(公告)号：US5302528A
公开(公告)日：1994-04-12
申请号：US872108
申请日：1992-04-22
申请人： Ezio Battistel , Daniele Bianchi , Pietro Cesti , Giuliana Franzosi , Roberto Tassinari , Sandro Spezia
发明人： Ezio Battistel , Daniele Bianchi , Pietro Cesti , Giuliana Franzosi , Roberto Tassinari , Sandro Spezia
IPC分类号： C12P7/40 , C12P41/00 , C12R1/01 , C12R1/07 , C12R1/13 , C12R1/265
CPC分类号： C12P7/40 , C12P41/005 , Y10S435/84
摘要： A process is described for the separation of the optical isomers of alphayl- or alpha-aryloxy- carboxylic acids by means of the stereoselective hydrolysis of racemic alkyl esters of the above acids in the presence of bacteria or their enzymes, selected from the species Brevibacterium, Bacteridium, Micrococcus, and Bacillus.
摘要翻译：描述了在细菌或其酶的存在下通过上述酸的外消旋烷基酯的立体选择性水解来分离α-芳基或α-芳氧基 - 羧酸的光学异构体的方法，所述细菌或其酶选自物种短杆菌属，细菌属，微球菌属和芽孢杆菌属。

3. 发明授权

US5332663A Process for the enzymatic preparation of 7-amino-cephalosporanic acids 失效
标题翻译： 7-氨基 - 头孢菌酸酶的制备方法
公开(公告)号：US5332663A
公开(公告)日：1994-07-26
申请号：US913041
申请日：1992-07-14
申请人： Ezio Battistel , Pietro Cesti , Giuliana Franzosi , Vilhelmus van der Goes
发明人： Ezio Battistel , Pietro Cesti , Giuliana Franzosi , Vilhelmus van der Goes
IPC分类号： C12P35/00 , C12N1/20 , C12P35/02 , C12R1/025 , C12R1/07 , C12R1/38 , C12P1/04
CPC分类号： C12R1/025 , C12P35/02 , Y10S435/832 , Y10S435/834 , Y10S435/874
摘要： 7-amino-cephalosporanic acids having the formula ##STR1## are obtained by submitting compounds having the following formula to enzymatic conversion: ##STR2## wherein R represents H, OH, O--CO--R", R" being an alkyl radical with from 1 to 4 carbon atoms, R.sup.1 represents a carboxylic group. The reaction is carried out in the presence of a microorganism selected from the Pseudomonas, Bacillus, Achromobacter genera, or in the presence of an enzyme, either free or immobilized, derived therefrom.
摘要翻译：具有下式的具有式ds的7-氨基 - 头孢菌酸进行酶促转化：其中R表示H，OH，O-CO-R“，R”是具有1至 4个碳原子，R1表示羧基。该反应是在选自假单胞菌属，芽孢杆菌属，无色杆菌属的微生物的存在下，或在由其衍生的游离或固定的酶的存在下进行的。

4. 发明授权

US6156939A Process for the hydroxylation of aromatic hydrocarbons 有权
标题翻译：芳烃羟基化方法
公开(公告)号：US6156939A
公开(公告)日：2000-12-05
申请号：US542457
申请日：2000-04-04
申请人： Rodolfo Vignola , Ezio Battistel , Daniele Bianchi , Rossella Bortolo , Roberto Tassinari
发明人： Rodolfo Vignola , Ezio Battistel , Daniele Bianchi , Rossella Bortolo , Roberto Tassinari
IPC分类号： B01J31/28 , B01J23/745 , B01J31/04 , C07B41/02 , C07B61/00 , C07C37/60 , C07C39/04 , C07C39/06 , C07C69/96 , C07C37/00
CPC分类号： B01J31/403 , B01J23/745 , B01J31/04 , B01J31/181 , B01J31/2208 , C07B41/02 , C07C37/60 , B01J2531/842 , Y02P20/52 , Y02P20/584
摘要： The invention relates to a process for the hydroxylation of aromatic hydrocarbons by direct oxidation with hydrogen peroxide. The process is carried out in the presence of a catalyst comprising:iron, administered as inorganic salt;iron ligand, consisting of carboxylic acids of ether-aromatic compounds containing nitrogen, in particular pyrazin-2-carboxylic acid and derivatives;acidifying agent, especially trifluoracetic acid, and a solvent system comprising an organic phase consisting of a substrate and acetonitrile and an aqueous phase containing the catalyst and hydrogen peroxide.
摘要翻译：本发明涉及通过用过氧化氢直接氧化来芳族烃的羟基化的方法。该方法在催化剂的存在下进行，所述催化剂包含：作为无机盐施用的铁; 铁配体，由含氮的醚 - 芳族化合物的羧酸组成，特别是吡嗪-2-羧酸及其衍生物; 酸化剂，特别是三氟乙酸，以及包含由底物和乙腈组成的有机相和含有催化剂和过氧化氢的水相的溶剂体系。

5. 发明申请

US20100069266A1 PROCESS FOR THE ENZYMATIC REMOVAL OF FILTER-CAKES PRODUCED BY WATER-BASED DRILLING AND COMPLETION FLUIDS 审中-公开
标题翻译：通过水基钻井和完井液生产的过滤器的酶除去过程
公开(公告)号：US20100069266A1
公开(公告)日：2010-03-18
申请号：US12513042
申请日：2007-10-29
申请人： Ezio Battistel , Daniele Bianchi , Sandra Cobianco , Marco Fornaroli
发明人： Ezio Battistel , Daniele Bianchi , Sandra Cobianco , Marco Fornaroli
IPC分类号： C09K8/02
CPC分类号： C09K8/52 , C09K8/524 , C09K8/582 , C12N9/2437 , C12N9/2445 , C12P19/26 , C12Y302/01021
摘要： The invention relates to a process for the solubilization of material containing scleroglucan and/or xanthan gum which comprises putting the above material in contact with an aqueous solution comprising an enzyme selected from a cellulase from Trichoderma reesei and/or a glucosidase from Aspergillus Niger.
摘要翻译：本发明涉及一种用于增溶含有硬葡聚糖和/或黄原胶的材料的方法，其包括将上述材料与包含选自里氏木霉纤维素酶和/或来自尼日尔曲霉的葡糖苷酶的酶的水溶液接触。

6. 发明授权

US06071848A Process for the hydroxylation of aromatic hydrocarbons 失效
标题翻译：芳烃羟基化方法
公开(公告)号：US06071848A
公开(公告)日：2000-06-06
申请号：US21816
申请日：1998-02-11
申请人： Rodolfo Vignola , Ezio Battistel , Daniele Bianchi , Rossella Bortolo , Roberto Tassinari
发明人： Rodolfo Vignola , Ezio Battistel , Daniele Bianchi , Rossella Bortolo , Roberto Tassinari
IPC分类号： B01J31/28 , B01J23/745 , B01J31/04 , C07B41/02 , C07B61/00 , C07C37/60 , C07C39/04 , C07C39/06 , C07C69/96 , B01J31/00
CPC分类号： B01J31/403 , B01J23/745 , B01J31/04 , B01J31/181 , B01J31/2208 , C07B41/02 , C07C37/60 , B01J2531/842 , Y02P20/52 , Y02P20/584
摘要： The invention relates to a process for the hydroxylation of aromatic hydrocarbons by direct oxidation with hydrogen peroxide. The process is carried out in the presence of a catalyst comprising:iron, administered as an inorganic salt;a carboxylic acid of an aromatic compound containing nitrogen, in particular a pyrazin-2-carboxylic acid or derivative;acidifying agent, especially trifluoracetic acid, and a solvent system comprising an organic phase consisting of a substrate and acetonitrile and an aqueous phase containing the catalyst and hydrogen peroxide.
摘要翻译：本发明涉及通过用过氧化氢直接氧化来芳族烃的羟基化的方法。该方法在催化剂的存在下进行，所述催化剂包含：作为无机盐施用的铁; 含氮的芳族化合物的羧酸，特别是吡嗪-2-羧酸或其衍生物; 酸化剂，特别是三氟乙酸，以及包含由底物和乙腈组成的有机相和含有催化剂和过氧化氢的水相的溶剂体系。

7. 发明授权

US06297391B1 Process for the synthesis of diricinoleyphosphatidylcholine 失效
标题翻译：合成二抗磷脂酰胆碱的方法
公开(公告)号：US06297391B1
公开(公告)日：2001-10-02
申请号：US09366744
申请日：1999-08-04
申请人： Giampietro Borsotti , Ezio Battistel , Francesco Cellini , Rina Iannacone
发明人： Giampietro Borsotti , Ezio Battistel , Francesco Cellini , Rina Iannacone
IPC分类号： C07C5300
CPC分类号： C12P7/6481 , C07F9/10 , Y02P20/55
摘要： Diricinoleylphosphatidylcholine (I) in an optically active form is obtained with good yields and a high purity by means of a process which comprises: a) esterifying the terminal carboxylic group of ricinoleic acid (III) with an alcohol having from 1 to 4 carbon atoms to give the corresponding ester having formula (IV); b) protecting the hydroxylic group of the ester of ricinoleic acid (IV) with a protecting group removable under bland operating conditions and isolating the ester of ricinoleic acid of which the hydroxylic group (V) is protected; c) hydrolyzing the ester of ricinoleic acid of which the hydroxylic group (V) is protected and isolating the ricinoleic acid of which the hydroxylic group (VI) is protected; d) acylating L-&agr;-glycerophosphatidylcholine (II) with an imidazolic or triazolic derivative of the compound having formula (VI) and isolating the diricinoleylphosphatidylcholine of which the hydroxylic group (VII) is protected; e) removing the protecting group from the hydroxylic group of the compound having formula (VII); and finally f) recovering and purifying the compound having formula (I) by means of chromatography.
摘要翻译：通过以下方法获得具有光学活性形式的二亚油酰基磷脂酰胆碱（I），具有良好的收率和高纯度，该方法包括：a）用具有1至4个碳原子的醇将蓖麻油酸（III）的末端羧基酯化至得到具有式（IV）的相应酯; b）用温和的操作条件下可除去的保护基保护蓖麻油酸（IV）的酯的羟基，并将其中羟基（Ⅴ）的蓖麻油酸酯保护; c）水解羟基（V）被保护的蓖麻油酸酯，并分离保护羟基（Ⅵ）的蓖麻油酸; d）用咪唑单体酰化L-α-甘油磷脂酰胆碱（II）或具有式（Ⅵ）的化合物的三唑衍生物，并分离保护羟基（Ⅶ）的二亚油酰基磷脂酰胆碱; e）从羟基中除去保护基具有式（VII）的化合物的式最后通过色谱法回收和纯化具有式（I）的化合物。

8. 发明授权

US5599698A Modified materials based on polyacrylonitrile and process for their production 失效
标题翻译：基于聚丙烯腈的改性材料及其生产工艺
公开(公告)号：US5599698A
公开(公告)日：1997-02-04
申请号：US448029
申请日：1995-05-23
申请人： Ezio Battistel , Franco Francalanci , Massimo Marinetti , Marco Morra
发明人： Ezio Battistel , Franco Francalanci , Massimo Marinetti , Marco Morra
IPC分类号： C12P13/02 , D06M16/00 , D06P3/74 , D06P3/82 , D06P5/22 , C12N9/88
CPC分类号： C12P13/02 , D06M16/003 , D06P3/74 , D06P3/8209 , D06P3/854 , D06P5/22 , Y10S435/84
摘要： The invention relates to modified materials based on polyacrylonitrile having amidic groups on their surface. The modification gives the material greater hydrophilic characteristics improving its comfort properties. In addition, it permits the polyacrylonitrile to be dyed also with acidic dyes thus making it possible for it to be used for the preparation of yarns mixed with natural fibres, such as wool for example. The process for their production involves treatment of the material with enzymes of the nitrile hydratasis class obtained from Brevibacterium imperiale.
摘要翻译：本发明涉及基于其表面具有酰胺基团的聚丙烯腈的改性材料。该改性使材料具有更好的亲水性，从而改善其舒适性。另外，它也可以用酸性染料染色聚丙烯腈，从而使其可用于制备与天然纤维例如羊毛等混合的纱线。其生产过程涉及用从Brevibacterium imperiale获得的腈水合物类的酶处理材料。

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