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1. 发明授权

US06790904B2 Liquid coating of film-forming resin and particles chemically modified to lower surface tension 有权
标题翻译：化学改性的成膜树脂和颗粒的液体涂层降低表面张力
公开(公告)号：US06790904B2
公开(公告)日：2004-09-14
申请号：US10160888
申请日：2002-06-03
申请人： Daniela White , James B. O'Dwyer , Michael A. Mayo , Laura E. Poindexter , John R. Schneider , Michael L. White , Richard J. Sadvary , Shiryn Tyebjee , Joseph M. Carney , Lawrence G. Anderson , Dennis A. Simpson , Thomas R. Hockswender
发明人： Daniela White , James B. O'Dwyer , Michael A. Mayo , Laura E. Poindexter , John R. Schneider , Michael L. White , Richard J. Sadvary , Shiryn Tyebjee , Joseph M. Carney , Lawrence G. Anderson , Dennis A. Simpson , Thomas R. Hockswender
IPC分类号： C08K322
CPC分类号： C09D7/69 , C08K3/22 , C08K3/28 , C08K3/36 , C08K9/06 , C09D7/62 , C09D7/67 , C09D7/68 , Y10T428/31511
摘要： Liquid coating compositions having improved mar and scratch resistance are disclosed. The coatings generally comprise one or more particles that have been modified to render the particles more surface active. The improved resistance is achieved without affecting the appearance or mechanical performance of the coatings. Methods for using the coatings, and the substrates coated therewith, are also disclosed.
摘要翻译：公开了具有改善的耐擦伤和耐划伤性的液体涂料组合物。涂料通常包含一种或多种已被改性以使颗粒更具表面活性的颗粒。在不影响涂层的外观或机械性能的情况下实现改进的电阻。还公开了使用涂层的方法及其涂覆的基材。

2. 发明授权

US07141618B2 Coating compositions with modified particles and methods of using the same 有权
公开(公告)号：US07141618B2
公开(公告)日：2006-11-28
申请号：US10161509
申请日：2002-06-03
申请人： John R. Schneider , Daniela White , Anthony M. Chasser , James B. O'Dwyer , Thomas R. Hockswender
发明人： John R. Schneider , Daniela White , Anthony M. Chasser , James B. O'Dwyer , Thomas R. Hockswender
IPC分类号： C08K9/06 , C08K3/00
CPC分类号： C09D5/033 , Y10S524/904 , Y10S525/931 , Y10S525/934
摘要： Powder coating compositions having improved mar and scratch resistance are disclosed. The coatings generally comprise one or more particles that have been modified to render the particles more surface active. The improved resistance is achieved without affecting the appearance or mechanical performance of the coatings. Methods for using the coatings, and the substrates coated therewith, are also disclosed.

3. 发明授权

US06306965B1 Thermosetting compositions containing carbamate-functional polylmers prepared using atom transfer radical polymerization 失效
标题翻译：含有使用原子转移自由基聚合制备的氨基甲酸酯官能聚合物的热固性组合物
公开(公告)号：US06306965B1
公开(公告)日：2001-10-23
申请号：US09375020
申请日：1999-08-16
申请人： Lawrence G. Anderson , James B. O'Dwyer , Dennis A. Simpson , Daniela White
发明人： Lawrence G. Anderson , James B. O'Dwyer , Dennis A. Simpson , Daniela White
IPC分类号： C08F830
CPC分类号： C08F220/36 , C08G18/3831 , C09D201/025
摘要： A thermosetting composition is provided comprising: (a) a crosslinking agent having at least two functional groups that are reactive with carbamates; and (b) a non-gelled, carbamate functional polymer prepared by atom transfer radical polymerization, in the presence of an initiator having at least one radically transferable group. The polymer contains at least one of the following polymer chain structures: —{(M)p—(G)q}x— or —{(G)q—(M)p}x— wherein M is a residue, that is free of carbamate functionality, of at least one ethylenically unsaturated radically polymerizable monomer; G is a residue, that has carbamate functionality, of at least one ethylenically unsaturated radically polymerizable monomer; p and q represent average numbers of residues occurring in a block of residues in each polymer chain structure; and p, q, and x are each independently selected for each structure such that the carbamate functional polymer has a number average molecular weight of at least 250. Also provided by the present invention are methods of coating a substrate using compositions of the present invention and substrates coated by such methods, as well as color-plus-clear composite coatings.
摘要翻译：提供一种热固性组合物，其包括：（a）具有至少两个与氨基甲酸酯反应的官能团的交联剂; 和（b）在具有至少一个可自由基转移基团的引发剂的存在下通过原子转移自由基聚合制备的非胶凝的氨基甲酸酯官能聚合物。所述聚合物含有至少一种以下聚合物链结构：或其中M是不含氨基甲酸酯官能团的至少一种烯属不饱和自由基聚合单体的残基; G是具有氨基甲酸酯官能团的至少一种烯属不饱和自由基聚合单体的残基; p和q表示在每个聚合物链结构的残基块中发生的残基的平均数目; 对于每种结构，p，q和x各自独立地选择，使得氨基甲酸酯官能聚合物的数均分子量至少为250.本发明还提供了使用本发明的组合物涂覆底物的方法和通过这些方法涂覆的基材，以及彩色 - 透明复合涂层。

4. 发明授权

US06517905B2 Thermosetting compositions containing hydroxyl-functional polymers prepared using atom transfer radical polymerization 失效
标题翻译：含有使用原子转移自由基聚合制备的羟基官能聚合物的热固性组合物
公开(公告)号：US06517905B2
公开(公告)日：2003-02-11
申请号：US09964964
申请日：2001-09-27
申请人： Daniela White , James B. O'Dwyer , Dennis A. Simpson
发明人： Daniela White , James B. O'Dwyer , Dennis A. Simpson
IPC分类号： C08F440
CPC分类号： C08L53/00 , C08F293/00 , C08F293/005 , C08F2438/01 , C08G18/6229 , C09D153/00 , Y10T428/31504 , Y10T428/31855 , C08L2666/02
摘要： A thermosetting composition that includes: (a) a crosslinking agent having at least two functional groups reactive with hydroxyl groups; and (b) a non-gelled, hydroxyl functional polymer prepared by atom transfer radical polymerization. The polymer contains at least one of the following polymer chain structures: —{(M)p—(G)q}x— or —{(G)q—(M)p}x— wherein M is a residue, that is free of hydroxyl functionality, of at least one monomer; G is a residue, that has hydroxyl functionality, of at least one monomer; p and q represent average numbers of residues occurring in a block of residues in each polymer chain structure; and p, q, and x are each independently selected for each structure such that the hydroxyl functional polymer has a number average molecular weight of at least 250. Also provided are methods of coating a substrate using compositions of the present invention and substrates coated by such methods, as well as color-plus-clear composite coatings.
摘要翻译：一种热固性组合物，其包括：（a）具有至少两个与羟基反应的官能团的交联剂; 和（b）通过原子转移自由基聚合制备的非胶凝的羟基官能聚合物。该聚合物含有至少一种以下聚合物链结构：或其中M是至少一种单体不含羟基官能团的残基; G是具有至少一个单体的羟基官能团的残基; p和q表示在每个聚合物链结构的残基块中发生的残基的平均数目; 对于每种结构，p，q和x各自独立地选择，使得羟基官能聚合物的数均分子量为至少250.还提供了使用本发明的组合物涂覆底物的方法和由其涂覆的底物方法，以及彩色+透明复合涂层。

5. 发明授权

US06319987B1 Thermosetting compositions containing hydroxyl-functional polymers prepared using atom transfer radical polymerization 有权
标题翻译：含有使用原子转移自由基聚合制备的羟基官能聚合物的热固性组合物
公开(公告)号：US06319987B1
公开(公告)日：2001-11-20
申请号：US09375019
申请日：1999-08-16
申请人： Daniela White , James B. O'Dwyer , Dennis A. Simpson
发明人： Daniela White , James B. O'Dwyer , Dennis A. Simpson
IPC分类号： C08L5300
CPC分类号： C08L53/00 , C08F293/00 , C08F293/005 , C08F2438/01 , C08G18/6229 , C09D153/00 , Y10T428/31504 , Y10T428/31855 , C08L2666/02
摘要： A thermosetting composition is provided comprising: (a) a crosslinking agent having at least two functional groups that are reactive with hydroxyl groups; and (b) a non-gelled, hydroxyl functional polymer prepared by atom transfer radical polymerization, in the presence of an initiator having at least one radically transferable group. The polymer contains at least one of the following polymer chain structures: —{(M)p—(G)q}x— or —{(G)q—(M)p}x— wherein M is a residue, that is free of hydroxyl functionality, of at least one ethylenically unsaturated radically polymerizable monomer; G is a residue, that has hydroxyl functionality, of at least one ethylenically unsaturated radically polymerizable monomer; p and q represent average numbers of residues occurring in a block of residues in each polymer chain structure; and p, q, and x are each independently selected for each structure such that the hydroxyl functional polymer has a number average molecular weight of at least 250.
摘要翻译：提供一种热固性组合物，其包括：（a）具有至少两个与羟基反应的官能团的交联剂; 和（b）在具有至少一个可自由基转移基团的引发剂的存在下通过原子转移自由基聚合制备的非胶凝的羟基官能聚合物。聚合物含有至少一种以下聚合物链结构：或其中M是至少一种烯属不饱和自由基聚合单体的残基，其不含羟基官能团; G是具有至少一个烯属不饱和自由基聚合性单体的羟基官能团的残基; p和q表示在每个聚合物链结构的残基块中发生的残基的平均数目; 对于每种结构，p，q和x各自独立地选择，使得羟基官能聚合物的数均分子量至少为250。

6. 发明授权

US06485788B1 Thermosetting compositions containing epoxy-functional polymers prepared using atom transfer radical 失效
标题翻译：含有使用原子转移自由基聚合制备的环氧官能聚合物的热固性组合物
公开(公告)号：US06485788B1
公开(公告)日：2002-11-26
申请号：US09934384
申请日：2001-08-21
申请人： Simion Coca , Dennis A. Simpson , James B. O'Dwyer , Kurt G. Olson
发明人： Simion Coca , Dennis A. Simpson , James B. O'Dwyer , Kurt G. Olson
IPC分类号： C08G5932
CPC分类号： C08L53/00 , C08F8/26 , C08F293/005 , C08F2438/01 , C08G59/3209 , C08K5/0025 , C09D153/00 , Y10T428/31511 , C08L33/12 , C08L2666/02
摘要： A thermosetting composition is provided comprising: (a) a crosslinking agent having at least two functional groups that are reactive with epoxides; and (b) a non-gelled, epoxy functional polymer prepared by atom transfer radical polymerization, in the presence of an initiator having at least one radically transferable group. The polymer contains at least one of the following polymer chain structures: —{(M)p—(G)q}x— or —{(G)q—(M)p}x— wherein M is a residue, that is free of epoxy functionality, of at least one ethylenically unsaturated radically polymerizable monomer; G is a residue, that has epoxy functionality, of at least one ethylenically unsaturated radically polymerizable monomer; p and q represent average numbers of residues occurring in a block of residues in each polymer chain structure; and p, q, and x are each independently selected for each structure such that the epoxy functional polymer has a number average molecular weight of at least 250. Also provided by the present invention are methods of coating a substrate using compositions of the present invention and substrates coated by such methods, as well as color-plus-clear composite coatings.
摘要翻译：提供一种热固性组合物，其包括：（a）具有至少两个与环氧化物反应的官能团的交联剂; 和（b）在具有至少一个可自由基转移基团的引发剂的存在下通过原子转移自由基聚合制备的非胶凝的环氧官能聚合物。聚合物含有至少一种以下聚合物链结构：或其中M是不含环氧官能团的至少一种烯属不饱和自由基聚合单体的残基; G是具有至少一个烯属不饱和自由基聚合单体的具有环氧官能度的残基; p和q表示在每个聚合物链结构的残基块中发生的残基的平均数目; 对于每种结构，p，q和x各自独立地选择，使得环氧官能聚合物的数均分子量至少为250.本发明还提供了使用本发明的组合物涂覆底物的方法和通过这些方法涂覆的基材，以及彩色 - 透明复合涂层。

7. 发明授权

US06319967B1 Thermosetting compositions containing epoxy-functional polymers prepared using atom transfer radical polymerization 有权
标题翻译：含有使用原子转移自由基聚合制备的环氧官能聚合物的热固性组合物
公开(公告)号：US06319967B1
公开(公告)日：2001-11-20
申请号：US09375021
申请日：1999-08-16
申请人： Simion Coca , Dennis A. Simpson , James B. O'Dwyer , Kurt G. Olson
发明人： Simion Coca , Dennis A. Simpson , James B. O'Dwyer , Kurt G. Olson
IPC分类号： C08G5932
CPC分类号： C08L53/00 , C08F8/26 , C08F293/005 , C08F2438/01 , C08G59/3209 , C08K5/0025 , C09D153/00 , Y10T428/31511 , C08L33/12 , C08L2666/02
摘要： A thermosetting composition is provided comprising: (a) a crosslinking agent having at least two functional groups that are reactive with epoxides; and (b) a non-gelled, epoxy functional polymer prepared by atom transfer radical polymerization, in the presence of an initiator having at least one radically transferable group. The polymer contains at least one of the following polymer chain structures: —{(M)p—(G)q}x—or —{(G)q—(M)p}x— wherein M is a residue, that is free of epoxy functionality, of at least one ethylenically unsaturated radically polymerizable monomer; G is a residue, that has epoxy functionality, of at least one ethylenically unsaturated radically polymerizable monomer; p and q represent average numbers of residues occurring in a block of residues in each polymer chain structure; and p, q, and x are each independently selected for each structure such that the epoxy functional polymer has a number average molecular weight of at least 250. Also provided by the present invention are methods of coating a substrate using compositions of the present invention and substrates coated by such methods, as well as color-plus-clear composite coatings.
摘要翻译：提供一种热固性组合物，其包括：（a）具有至少两个与环氧化物反应的官能团的交联剂; 和（b）在具有至少一个可自由基转移基团的引发剂的存在下通过原子转移自由基聚合制备的非胶凝的环氧官能聚合物。聚合物含有至少一种以下聚合物链结构：其中M是至少一种烯属不饱和可自由基聚合单体的残基，不含环氧官能团; G是具有至少一个烯属不饱和自由基聚合单体的具有环氧官能度的残基; p和q表示在每个聚合物链结构的残基块中发生的残基的平均数目; 对于每种结构，p，q和x各自独立地选择，使得环氧官能聚合物的数均分子量至少为250.本发明还提供了使用本发明的组合物涂覆底物的方法和通过这些方法涂覆的基材，以及彩色 - 透明复合涂层。

8. 发明授权

US06462125B1 Pigment dispersions containing dispersants prepared by controlled radical polymerization having hydrophilic and hydrophobic segments 失效
标题翻译：含有通过具有亲水和疏水链段的受控自由基聚合制备的分散剂的颜料分散体
公开(公告)号：US06462125B1
公开(公告)日：2002-10-08
申请号：US09464946
申请日：1999-12-16
申请人： Daniela White , Simion Coca , James B. O'Dwyer
发明人： Daniela White , Simion Coca , James B. O'Dwyer
IPC分类号： C08J3100
CPC分类号： C09D17/001 , C09B67/009
摘要： A pigment dispersion that includes a pigment, an aqueous carrier, and a pigment dispersant. The pigment dispersant is prepared by atom transfer radical polymerization initiated and has the polymer chain structure: &phgr;—(G)p—(E)a—T where G is a residue of at least One ethylenically unsaturated monomer; E is a hydrophilic residue of at least one ethylenically unsaturated monomer; &phgr; is a hydrophobic residue of or derived from an initiator; T is or is derived from a radically transferable group from the initiator, p and s represent average numbers of residues occurring in a block of residues; p and s are each individually selected such that said pigment dispersant has a number average molecular weight of at least 250.
摘要翻译：包含颜料，水性载体和颜料分散剂的颜料分散体。颜料分散剂通过引发原子转移自由基聚合制备，并具有聚合物链结构：其中G是至少一个烯属不饱和单体的残基; E是至少一种烯属不饱和单体的亲水性残基; phi是引发剂的疏水残基或衍生自引发剂; T是衍生自起始基团的可自由转移的基团，p和s代表在残基块中发生的残基的平均数; p和s各自单独选择，使得所述颜料分散剂的数均分子量为至少250。

9. 发明授权

US06265489B1 Thermosetting compositions containing carboxylic acid functional polymers prepared by atom transfer radical polymerization 失效
标题翻译：含有通过原子转移自由基聚合制备的羧酸官能聚合物的热固性组合物
公开(公告)号：US06265489B1
公开(公告)日：2001-07-24
申请号：US09375017
申请日：1999-08-16
申请人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
发明人： Karen A. Barkac , Simion Coca , James R. Franks , Kurt A. Humbert , Paul H. Lamers , Roxalana L. Martin , James B. O'Dwyer , Kurt G. Olson , Daniela White
IPC分类号： C08L3302
CPC分类号： C09D133/02 , C08L63/00 , C09D133/064 , C08L2666/14
摘要： A thermosetting composition comprising a co-reactable solid, particulate mixture of (a) polycarboxylic acid functional polymer, and (b) epoxide functional crosslinking agent having at least two epoxide groups, e.g., triglycidyl isocyanurate (TGIC), is described. The polycarboxylic acid functional polymer is prepared by atom transfer radical polymerization and has well defined polymer chain architecture and polydispersity index of less than 2.0. The thermosetting compositions of the present invention have utility as powder coatings compositions.
摘要翻译：描述了包含（a）多元羧酸官能聚合物和（b）具有至少两个环氧基团的环氧官能交联剂例如三缩水甘油基异氰脲酸酯（TGIC）的共反应固体，颗粒混合物的热固性组合物。聚羧酸官能聚合物通过原子转移自由基聚合制备，并且具有良好的聚合物链结构和小于2.0的多分散指数。本发明的热固性组合物可用作粉末涂料组合物。

10. 发明授权

US06875832B2 Synthesis of vinyl polymers by controlled radical polymerization 失效
标题翻译：通过控制自由基聚合合成乙烯基聚合物
公开(公告)号：US06875832B2
公开(公告)日：2005-04-05
申请号：US10116239
申请日：2002-04-04
申请人： Daniela White , James B. O'Dwyer
发明人： Daniela White , James B. O'Dwyer
IPC分类号： C08F2/32 , C08F2/38 , C08F4/00 , C08F293/00 , C08F4/04
CPC分类号： C08F4/00 , C08F2/32 , C08F293/005
摘要： A controlled free radical polymerization process, which includes the steps of: adding a monofunctional iniferter compound to an oxygen-free solvent; heating the solution to a temperature sufficient to allow the iniferter compound to form two carbon centered radical residues; adding a first monomer composition comprising one or more monomers to the solution containing the radical containing residues; polymerizing the first monomer composition to form a quasi-living polymer; and optionally polymerizing a second monomer composition comprising one or more monomers, which are different than the first monomer composition. The resulting non-random copolymer having the general formula: φ-[—Ap—Bs—]t-φ where A and B are different compositions of ethylenically unsaturated monomers; p is an integer from 1 to 1,000; s is an integer from 0 to 1,000; t is an integer from 1 to 100; and φ is a residue from the iniferter.
摘要翻译：一种受控的自由基聚合方法，其包括以下步骤：将单官能异构体化合物加入到无氧溶剂中; 将溶液加热至足以允许引发剂化合物形成两个碳中心自由基残基的温度; 将含有一种或多种单体的第一单体组合物加入到含有基团的残基的溶液中; 聚合第一单体组合物以形成准活性聚合物; 并且任选地聚合包含与第一单体组合物不同的一种或多种单体的第二单体组合物。所得的具有以下通式的非无规共聚物：其中A和B是烯属不饱和单体的不同组成; p是1至1,000的整数; s是0到1,000之间的整数; t为1〜100的整数; phi是来自引物的残基。

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