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1. 发明申请

US20110292566A1 CYANORESIN POLYMER FOR DIELECTRIC FILM, PROCESS OF MAKING AND ASSOCIATED ARTICLE 审中-公开
标题翻译：用于电介质膜的氰烷基聚合物，制备方法和相关文章
公开(公告)号：US20110292566A1
公开(公告)日：2011-12-01
申请号：US12787798
申请日：2010-05-26
申请人： Daniel Qi Tan , Sheldon Shafer , Farid Fouad Khouri , Patricia Chapman Irwin , Yang Cao
发明人： Daniel Qi Tan , Sheldon Shafer , Farid Fouad Khouri , Patricia Chapman Irwin , Yang Cao
IPC分类号： H01G4/06 , C08G63/91 , B32B3/00
CPC分类号： C08B11/155 , C08B31/125 , C08L29/04 , C08L33/12 , D06M13/348
摘要： A cyanoresin polymer is described, wherein about 10 percent to about 60 percent of the side chains on the polymer include a cyano group; and substantially all of the remaining polymer side chains include a hydroxyl group. A method of forming such a cyanoresin polymer is described. A capacitor having a dielectric film including such a cyanoresin polymer is also presented.
摘要翻译：描述了氰基树脂聚合物，其中聚合物上约10％至约60％的侧链包括氰基; 并且基本上所有剩余的聚合物侧链包括羟基。描述了形成这种氰基树脂聚合物的方法。还提出了具有包括这种氰基树脂聚合物的电介质膜的电容器。

2. 发明授权

US09127127B2 Polyetherimide compositions, methods of manufacture, and articles formed therefrom 有权
标题翻译：聚醚酰亚胺组合物，制造方法和由其形成的制品
公开(公告)号：US09127127B2
公开(公告)日：2015-09-08
申请号：US13649443
申请日：2012-10-11
申请人： Thomas Link Guggenheim , Roy Ray Odle , Farid Fouad Khouri
发明人： Thomas Link Guggenheim , Roy Ray Odle , Farid Fouad Khouri
IPC分类号： C08G73/10
CPC分类号： C08G73/1021 , C08G73/1046 , C08G73/1053 , C08G73/1071
摘要： A method for the manufacture of a polyetherimide composition includes catalyzing the reaction of a dianhydride and an organic diamine with a catalyst selected from guanadinium salts, pyridinium salts, imidazolium salts, tetra(C6-24)aryl ammonium salts, tetra(C7-24 arylalkylene) ammonium salts, dialkyl heterocycloaliphatic ammonium salts, bis-alkyl quaternary ammonium salts, (C7-24arylalkylene)(C1-16alkyl) phosphonium salts, (C6-24aryl)(C1-16alkyl)phosphonium salts, phosphazenium salts and combinations thereof, optionally in the presence of a solvent.
摘要翻译：制备聚醚酰亚胺组合物的方法包括用选自胍盐，吡啶鎓盐，咪唑鎓盐，四（C 6-24）芳基铵盐，四（C 7-24芳基亚烷基）烷基的催化剂催化二酐和有机二胺的反应）铵盐，二烷基杂环脂族铵盐，双烷基季铵盐，（C 7-24芳基亚烷基）（C 1-6烷基）鏻盐，（C 6-24芳基）（C 1-6烷基）鏻盐，磷氮烯基鏻盐及其组合，溶剂的存在。

3. 发明授权

US08524854B2 Chloro-substituted polyetherimides having improved relative thermal index 有权
标题翻译：具有改进的相对热指数的氯取代的聚醚酰亚胺
公开(公告)号：US08524854B2
公开(公告)日：2013-09-03
申请号：US13059691
申请日：2010-12-28
申请人： Hendrich Chiong , Thomas Link Guggenheim , Farid Fouad Khouri , Matthew L. Kuhlman , Miguel Angel Navarro de Castro , Roy Ray Odle , Brennan A. Smith
发明人： Hendrich Chiong , Thomas Link Guggenheim , Farid Fouad Khouri , Matthew L. Kuhlman , Miguel Angel Navarro de Castro , Roy Ray Odle , Brennan A. Smith
IPC分类号： C08G73/10
CPC分类号： C08G73/1046 , C08G73/1003 , C08G73/1014 , C08G73/1053 , C08G73/1067 , C08G73/1071 , C08L67/00 , C08L69/00 , C08L79/08 , C08L2666/20
摘要： A polyetherimide having an OH content that is greater than 0 and equal or less than 100 ppm; a Relative Thermal Index that is greater than or equal to 170° C.; and a chlorine content that is greater than 0 ppm is disclosed herein. A method for preparing the polyetherimide is also disclosed.
摘要翻译： OH含量大于0且等于或小于100ppm的聚醚酰亚胺; 大于或等于170℃的相对热指数; 并且本文公开了大于0ppm的氯含量。还公开了制备聚醚酰亚胺的方法。

4. 发明授权

US07772435B2 Method of forming a dry quaternary ammonium salt mixture 有权
标题翻译：形成干燥季铵盐混合物的方法
公开(公告)号：US07772435B2
公开(公告)日：2010-08-10
申请号：US11617416
申请日：2006-12-28
申请人： Thomas Link Guggenheim , Paul Edward Howson , Farid Fouad Khouri , Lioba Maria Kloppenburg , Matthew Hal Littlejohn , Jacob Lee Oberholtzer , Juan Rodriguez Ordonez , Suresh R. Sriram , David Winfield Woodruff
发明人： Thomas Link Guggenheim , Paul Edward Howson , Farid Fouad Khouri , Lioba Maria Kloppenburg , Matthew Hal Littlejohn , Jacob Lee Oberholtzer , Juan Rodriguez Ordonez , Suresh R. Sriram , David Winfield Woodruff
IPC分类号： C07C211/62 , C07C251/02 , C07D211/00 , C07D213/72
CPC分类号： C07C277/08 , C07D209/48 , C07D213/74 , C07C279/04
摘要： Disclosed herein is a method comprising: (a) adding an aqueous solution comprising a quaternary ammonium salt to an organic solvent in a vessel under an inert atmosphere, thereby forming a first mixture comprising the quaternary ammonium salt and the solvent; and (b) mixing the first mixture at a temperature and for a time sufficient to remove water and a portion of the solvent from the first mixture, wherein the mixing is performed in an inert atmosphere and the temperature is less than the decomposition temperature of the quaternary ammonium salt.
摘要翻译：本文公开了一种方法，包括：（a）在惰性气氛下，将容纳季铵盐的水溶液在容器中加入到有机溶剂中，从而形成包含季铵盐和溶剂的第一混合物; 和（b）将第一混合物在足以从第一混合物中除去水和一部分溶剂的温度和时间下混合，其中混合在惰性气氛中进行，并且温度低于所述第一混合物的分解温度季铵盐。

5. 发明授权

US5707439A Layered minerals and compositions comprising the same 失效
标题翻译：层状矿物质及其组合物
公开(公告)号：US5707439A
公开(公告)日：1998-01-13
申请号：US574012
申请日：1995-12-18
申请人： Tohru Takekoshi , Farid Fouad Khouri , John Robert Campbell , Therese Coste Jordan , Kevin Hsingtao Dai
发明人： Tohru Takekoshi , Farid Fouad Khouri , John Robert Campbell , Therese Coste Jordan , Kevin Hsingtao Dai
IPC分类号： C01B33/44 , C04B14/04 , C04B14/20 , C04B14/00
CPC分类号： C04B14/206 , C01B33/44 , C04B14/04 , C04B2103/0087
摘要： Novel silicate minerals that have undergone a cation exhange with at least one heteroaromatic cation comprising a positively charged organo-substituted heteroatom and/or at least one positively charged heteroatom not part of an aromatic ring with at least one bond having a bond order greater than one and compositions comprising the same are described.
摘要翻译：已经经历阳离子的新型硅酸盐矿物与包含带正电荷的有机取代的杂原子和/或至少一个带正电荷的杂原子的至少一个杂芳族阳离子渗透，不是具有至少一个键数大于1的芳环的一部分并描述包含该组合物的组合物。

6. 发明授权

US08592548B2 Method to prepare bis(haloimides) 有权
标题翻译：制备双（卤代酰亚胺）的方法
公开(公告)号：US08592548B2
公开(公告)日：2013-11-26
申请号：US11022907
申请日：2004-12-22
申请人： John Yupeng Gui , Norman Enoch Johnson , Thomas Link Guggenheim , David Winfield Woodruff , James Manio Silva , Farid Fouad Khouri
发明人： John Yupeng Gui , Norman Enoch Johnson , Thomas Link Guggenheim , David Winfield Woodruff , James Manio Silva , Farid Fouad Khouri
IPC分类号： C08G8/02
CPC分类号： C07D209/48 , C08G73/12
摘要： Bis(halophthalimides) are prepared in mixture in an organic liquid such as ortho-dichlorobenzene or anisole, by a reaction at a temperature of at least 150° C. between at least one diamine compound and at least one halophthalic anhydride in the presence of imidization catalyst. The reaction mixture is maintained at about 15% by weight solids content and rich in the halophthalic anhydride by constantly monitoring the reaction mixture using analytical methods such as high performance liquid chromatography. The product mixture may be directly employed in the direct preparation of polyetherimides, and similar slurries may be employed to prepare other polyether polymers.
摘要翻译：通过在至少150℃的温度下在至少一种二胺化合物和至少一种卤代邻苯二甲酸酐之间的反应中，在酰亚胺化的存在下，在有机液体如邻二氯苯或苯甲醚中混合制备双（卤代邻苯二酰亚胺）催化剂。通过使用诸如高效液相色谱法的分析方法不断监测反应混合物，将反应混合物保持在约15重量％的固体含量并富含卤代邻苯二甲酸酐。产物混合物可以直接用于直接制备聚醚酰亚胺，并且可以使用类似的浆料来制备其它聚醚聚合物。

7. 发明授权

US07981996B2 Method of making bisimides 有权
标题翻译：制备双酰亚胺的方法
公开(公告)号：US07981996B2
公开(公告)日：2011-07-19
申请号：US11600538
申请日：2006-11-16
申请人： Farid Fouad Khouri , Albert Santo Stella
发明人： Farid Fouad Khouri , Albert Santo Stella
IPC分类号： C08G8/02
CPC分类号： C07D407/12 , C07D307/89
摘要： The present invention provides a method for preparing relatively insoluble bisimides under conditions which afford high imidization reaction rates and which permit the monitoring and adjustment of reactant stoichiometry at any stage of the reaction. The bisimides provided by the present invention are prepared either by reaction of a diamine such as 4,4′-diaminodiphenylsulfone (DDS) with an anhydride, for example 3-chlorophthalic anhydride (3-ClPA) in the presence of a solvent at a pressure greater than one atmosphere and at a temperature above the normal boiling point of the solvent, or by reaction of a monoamine with a dianhydride under the same conditions. In one embodiment, the relatively insoluble product bisimides provided by the present invention have a solubility in ortho-dichlorobenzene of less than about 10 percent by weight at a temperature of about 180° C.
摘要翻译：本发明提供了在提供高酰亚胺化反应速率并允许在反应的任何阶段监测和调节反应物化学计量的条件下制备相对不溶性双酰亚胺的方法。本发明提供的双酰亚胺通过在溶剂存在下，在压力存在下，通过使诸如4,4'-二氨基二苯基砜（DDS）的二胺与酸酐例如3-氯邻苯二甲酸酐（3-ClPA）大于一个气氛，并且在高于溶剂的标准沸点的温度下，或在相同条件下通过单胺与二酐的反应。在一个实施方案中，本发明提供的相对不溶性产物双酰亚胺在约180℃的温度下在邻二氯苯中的溶解度小于约10重量％

8. 发明授权

US07928155B2 Compositions and methods for polymer composites 失效
标题翻译：聚合物复合材料的组成和方法
公开(公告)号：US07928155B2
公开(公告)日：2011-04-19
申请号：US11766850
申请日：2007-06-22
申请人： Feng Cao , Kwok Pong Chan , Erik C. Hagberg , Farid Fouad Khouri , Tara J. Mullen , Roy Ray Odle , James Mitchell White , Norimitsu Yamaguchi
发明人： Feng Cao , Kwok Pong Chan , Erik C. Hagberg , Farid Fouad Khouri , Tara J. Mullen , Roy Ray Odle , James Mitchell White , Norimitsu Yamaguchi
IPC分类号： C08J7/14 , C08K3/34 , C08K9/04 , C08L43/00 , C08L43/02
CPC分类号： C08F2/44
摘要： In one embodiment, the present invention provides a method of making a polymer-organoclay composite composition comprising (a) contacting under condensation polymerization conditions a first monomer, a second monomer, a solvent, and an organoclay composition, said organoclay composition comprising alternating inorganic silicate layers and organic layers, to provide a first polymerization reaction mixture, wherein one of said first monomer and second monomers is a diamine and the other is an dianhydride; (b) carrying out a stoichiometry verification step on the first polymerization reaction mixture; (c) optionally adding additional reactant (monomer 1, monomer 2, or chainstopper) to the first polymerization reaction mixture to provide a second polymerization reaction mixture; and (d) removing solvent from the first polymerization reaction mixture or the second polymerization reaction mixture to provide a first polymer-organoclay composite composition comprising a polymer component and an organoclay component wherein the organoclay component is at least 10% exfoliated.
摘要翻译：在一个实施方案中，本发明提供制备聚合物 - 有机粘土复合组合物的方法，其包含（a）在缩聚条件下使第一单体，第二单体，溶剂和有机粘土组合物接触，所述有机粘土组合物包含交替的无机硅酸盐层和有机层，以提供第一聚合反应混合物，其中所述第一单体和第二单体之一是二胺，另一个是二酐; （b）在第一聚合反应混合物上进行化学计量验证步骤; （c）任选地向第一聚合反应混合物中加入另外的反应物（单体1，单体2或链截止剂）以提供第二聚合反应混合物; 和（d）从第一聚合反应混合物或第二聚合反应混合物中除去溶剂以提供包含聚合物组分和有机粘土组分的第一聚合物 - 有机粘土复合组合物，其中有机粘土组分至少10％剥离。

9. 发明授权

US07714095B2 Phase transfer catalyzed method for preparation of polyetherimides 有权
标题翻译：相转移催化聚醚酰亚胺的制备方法
公开(公告)号：US07714095B2
公开(公告)日：2010-05-11
申请号：US11363681
申请日：2006-02-28
申请人： Daniel Joseph Brunelle , Havva Yagci Acar , Farid Fouad Khouri , Thomas Link Guggenheim , David Winfield Woodruff , Norman Enoch Johnson
发明人： Daniel Joseph Brunelle , Havva Yagci Acar , Farid Fouad Khouri , Thomas Link Guggenheim , David Winfield Woodruff , Norman Enoch Johnson
IPC分类号： C08G73/00 , C08G73/10 , C08G8/02 , C08G14/00
CPC分类号： C08G73/12 , C08G73/121 , C08G73/124
摘要： Polyether polymers, such as polyetherimides, are prepared by the reaction of a dihydroxy-substituted aromatic hydrocarbon alkali metal salt, such as bisphenol A disodium salt, with a bis(N-(chlorophthalimido))aromatic compound, such as 1,3- and/or 1,4-bis(N-(4-chlorophthalimido))benzene, in a solvent such as o-dichlorobenzene and in the presence of a phase transfer catalyst such as a hexaalkylguanidinium chloride. Several embodiments may be employed to improve the method. They comprise employing substantially dry reagents, employing a high solids level in solvent, beginning with an excess of bis(N-(chlorophthalimido))-aromatic compound and incrementally adding alkali metal salt, employing alkali metal salt of small particle size, and using reagents of high purity.
摘要翻译：聚醚聚合物如聚醚酰亚胺通过二羟基取代的芳族烃碱金属盐如双酚A二钠盐与双（N-（氯代邻苯二甲酰亚胺基））芳族化合物如1,3-和 /或1,4-双（N-（4-氯邻苯二甲酰亚氨基））苯，在溶剂如邻二氯苯中，并在相转移催化剂如六烷基氯化the存在下进行。可以采用几个实施例来改进该方法。它们包括使用基本上干的试剂，在溶剂中使用高固体含量，从过量的双（N-（氯代邻苯二甲酰亚胺基）） - 芳族化合物开始，并逐渐加入碱金属盐，使用小粒径的碱金属盐，并使用试剂的高纯度。

10. 发明授权

US06831123B1 Ionomeric polyester compositions containing organoclays, and method 有权
标题翻译：含有机粘土的离聚物聚酯组合物及方法
公开(公告)号：US06831123B1
公开(公告)日：2004-12-14
申请号：US09523669
申请日：2000-03-10
申请人： Bret Ja Chisholm , Farid Fouad Khouri
发明人： Bret Ja Chisholm , Farid Fouad Khouri
IPC分类号： C08J510
CPC分类号： C08K9/04 , C08L67/02 , C08L67/00 , C08L77/00
摘要： Resinous compositions are disclosed which comprise at least one ionomeric polyester and at least one organoclay. Also a method is disclosed for improving the modulus properties of a resinous composition comprising at least one organoclay, the method comprising the steps of combining the resinous composition with at least one ionomeric polyester, and intimately mixing the composition.
摘要翻译：公开了包含至少一种离聚物聚酯和至少一种有机粘土的树脂组合物。还公开了一种用于改善包含至少一种有机粘土的树脂组合物的模量性质的方法，该方法包括以下步骤：将树脂组合物与至少一种离聚物聚酯组合，并将组合物充分混合。

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