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1. 发明授权

US07501024B2 Carbon nanohorn producing device and carbon nanohorn producing method 有权
标题翻译：碳纳米管生产装置和碳纳米角生产方法
公开(公告)号：US07501024B2
公开(公告)日：2009-03-10
申请号：US10556088
申请日：2004-05-19
申请人： Takeshi Azami , Daisuke Kasuya , Sumio Iijima , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka
发明人： Takeshi Azami , Daisuke Kasuya , Sumio Iijima , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka
IPC分类号： C30B25/06
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/18 , Y10T117/10 , Y10T117/1004 , Y10T117/1012
摘要： A plume (109) is generated by irradiating a side face of a graphite rod (101) with a laser beam (103) to vaporize carbon. The vaporized carbon is introduced to a carbon nanohorn recovery chamber (119) through a recovery pipe (155), and the vaporized carbon is recovered as a carbon nanohorn assembly (117). A cooling tank (150) including liquid nitrogen (151) is arranged in the recovery pipe (155). While the cooling tank (150) controls the plume (109) at a low temperature, the cooling tank (150) cools the carbon vapor when the carbon vapor passes through the recovery pipe (155). The cooled carbon vapor is recovered as the carbon nanohorn assembly (117) which is controlled in the desired shape and dimensions.
摘要翻译：通过用激光束（103）照射石墨棒（101）的侧面来汽化碳而产生羽流（109）。蒸发的碳通过回收管（155）引入到碳纳米角回收室（119）中，并且蒸发的碳作为碳纳米角组件（117）回收。包括液氮（151）的冷却箱（150）布置在回收管（155）中。当冷却箱（150）在低温下控制羽流（109）时，当碳蒸汽通过回收管（155）时，冷却罐（150）冷却碳蒸汽。冷却的碳蒸汽作为碳纳米角组件（117）回收，其被控制在所需的形状和尺寸。

2. 发明申请

US20070003468A1 Nanocarbon producing device and nanocarbon producing method 审中-公开
标题翻译：纳米碳生产装置和纳米碳生产方法
公开(公告)号：US20070003468A1
公开(公告)日：2007-01-04
申请号：US10555064
申请日：2004-04-27
申请人： Takeshi Azami , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Daisuke Kasuya , Masako Yudasaka
发明人： Takeshi Azami , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Daisuke Kasuya , Masako Yudasaka
IPC分类号： C01B31/02 , B01J19/08 , D01F9/127
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/18 , C01P2004/64 , C09C1/48 , D01F9/12
摘要： A surface of a graphite target (139), irradiated with a laser beam (103), is formed in a plane. The graphite target (139) is held by a target holding unit (153) on a target supply plate (135). A plate holding unit (137) moves the target supply plate (135) in a translational manner, which allows an irradiation position of the laser beam (103) and the surface of the graphite target (139) to be relatively moved. A transportation pipe (141) communicated with a nanocarbon collecting chamber (119) is provided toward a direction in which a plume (109) is generated, and a generated carbon nanohorn aggregates (117) is collected in the nanocarbon collecting chamber (119).
摘要翻译：在平面中形成用激光束（103）照射的石墨靶（139）的表面。石墨靶（139）由目标保持单元（153）保持在目标供给板（135）上。板保持单元（137）以平移方式移动目标供给板（135），这允许激光束（103）的照射位置和石墨靶（139）的表面相对移动。沿着生成羽流（109）的方向设置与纳米碳收集室（119）连通的输送管（141），并将生成的碳纳米角集合体（117）收集在纳米碳收集室（119）中。

3. 发明申请

US20060133979A1 Apparatus and method for manufacturing nano carbon 审中-公开
标题翻译：纳米碳制造装置及方法
公开(公告)号：US20060133979A1
公开(公告)日：2006-06-22
申请号：US10544133
申请日：2004-02-10
申请人： Takeshi Azami , Takashi Manako , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Masako Yudasaka , Daisuke Kasuya
发明人： Takeshi Azami , Takashi Manako , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Masako Yudasaka , Daisuke Kasuya
IPC分类号： C01B31/02 , B01J19/08
CPC分类号： B82Y30/00 , B01J19/121 , B01J2219/0879 , B82Y40/00 , C01B32/18
摘要： A production method and a production apparatus for stable mass production of nanocarbon are provided. In a production chamber (107), a graphite rod (101) having a cylindrical shape is fixed to a rotation apparatus (115), and is made to be capable of rotating with the length direction of the graphite rod (101) serving as an axis, and also moving to the right or the left in the length direction. The side surface of the graphite rod (101) is irradiated with a laser beam (103) from a laser light source (111), and a nanocarbon collecting chamber (119) is disposed in the direction of generation of plumes (109). On the other hand, the surface irradiated with the laser beam (103) among the side surfaces of the graphite rod (101) is speedily rotated by the rotation apparatus (115) and is flattened by a cutting tool (105). Cut dusts of the graphite rod (101) generated by the cutting tool (105) are collected into a cut graphite collecting chamber (121) and separated from the generated carbon nanohorn aggregates (117).
摘要翻译：提供了用于稳定批量生产纳米碳的生产方法和生产设备。在制造室（107）中，将具有圆筒形状的石墨棒（101）固定在旋转装置（115）上，使其能够沿石墨棒（101）的长度方向旋转，并且还在长度方向上向右或向左移动。石墨棒（101）的侧表面从激光源（111）被激光束（103）照射，并且在产生羽流（109）的方向上设置有纳米碳收集室（119）。另一方面，在石墨棒（101）的侧面中用激光（103）照射的表面通过旋转装置（115）快速旋转，并被切割工具（105）变平。由切割工具（105）产生的石墨棒（101）的切割灰尘被收集到切割的石墨收集室（121）中并与生成的碳纳米角骨料（117）分离。

4. 发明申请

US20060237301A1 Apparatus for producing nanocarbon, method for producing nanocarbon and method for collecting nanocarbon 审中-公开
标题翻译：用于生产纳米碳的装置，生产纳米碳的方法和收集纳米碳的方法
公开(公告)号：US20060237301A1
公开(公告)日：2006-10-26
申请号：US10566579
申请日：2004-08-05
申请人： Takeshi Azami , Daisuke Kasuya , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Masako Yudasaka
发明人： Takeshi Azami , Daisuke Kasuya , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Masako Yudasaka
IPC分类号： D01F9/12 , B01J19/08 , C01B31/00
CPC分类号： B82Y30/00 , B01J19/121 , B01J2219/0886 , B82Y40/00 , C01B32/16 , C01B32/18
摘要： In a nanocarbon manufacturing apparatus (183), a spray (181) is provided at a side face of a nanocarbon recovery chamber (119), and a mist (195) is sprayed on the entire nanocarbon recovery chamber (119) from the spray (181).
摘要翻译：在纳米碳制造装置（183）中，在纳米碳回收室（119）的侧面设置有喷雾（181），并且从喷雾器（11A）向整个纳米碳回收室（119）喷雾（195） 181）。

5. 发明申请

US20060147647A1 Apparatus and method for manufacturing nano carbon 审中-公开
标题翻译：纳米碳制造装置及方法
公开(公告)号：US20060147647A1
公开(公告)日：2006-07-06
申请号：US10544400
申请日：2004-02-10
申请人： Takeshi Azami , Takashi Manako , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Masako Yudasaka , Daisuke Kasuya
发明人： Takeshi Azami , Takashi Manako , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima , Masako Yudasaka , Daisuke Kasuya
IPC分类号： C08J7/04 , B05B5/025
CPC分类号： B82Y30/00 , B01J19/121 , B01J2219/0879 , B82Y40/00 , C01B32/18
摘要： Nanocarbon is produced stably in a large amount. In a production chamber (107), a graphite rod (101) having a cylindrical shape is fixed to a rotation apparatus (115) and is made capable of rotating with its axis being in the length direction of the graphite rod (101) and movable to the right or the left in the length direction. A side surface of the graphite rod (101) is irradiated with a laser beam (103) from a laser light source (111). A nanocarbon collecting chamber (119) is disposed in the direction of generation of plumes (109) so as to collect the generated carbon nanohorn aggregates 117.
摘要翻译：大量稳定地生产纳米碳。在制造室（107）中，将具有圆筒形状的石墨棒（101）固定在旋转装置（115）上并使其轴线能够在石墨棒（101）的长度方向上旋转并可移动在长度方向的右侧或左侧。石墨棒（101）的侧表面用激光束（111）照射激光束（103）。在产生羽流（109）的方向上设置纳米碳收集室（119），以收集生成的碳纳米角骨料117。

6. 发明申请

US20070025905A1 Nanocarbon-producing device 审中-公开
标题翻译：纳米碳制造装置
公开(公告)号：US20070025905A1
公开(公告)日：2007-02-01
申请号：US10560593
申请日：2004-06-22
申请人： Takeshi Azami , Tsutomu Yoshitake , Yoshimi Kubo , Daisuke Kasuya , Sumio Iijima , Masako Yudasaka
发明人： Takeshi Azami , Tsutomu Yoshitake , Yoshimi Kubo , Daisuke Kasuya , Sumio Iijima , Masako Yudasaka
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/16 , C01B32/18
摘要： In a nanocarbon-producing device (173), a plane mirror (169) and a parabolic mirror (171) are arranged in a production chamber (107). Light, emitted from a laser light source (111), transmitted through a ZnSe window (133) is reflected at the plane mirror (169) and the parabolic mirror (171), collected at the parabolic mirror (171), and then irradiated onto the surface of a graphite rod (101).
摘要翻译：在纳米碳制造装置（173）中，平面镜（169）和抛物面镜（171）布置在生产室（107）中。透射通过ZnSe窗口（133）的从激光源（111）发射的光在平面镜（169）和抛物面反射镜（171）被反射，被收集在抛物面镜（171）处，然后照射到石墨棒（101）的表面。

7. 发明授权

US08882970B2 Apparatus and method for manufacturing carbon nanohorns 有权
标题翻译：用于制造碳纳米角的装置和方法
公开(公告)号：US08882970B2
公开(公告)日：2014-11-11
申请号：US12226570
申请日：2007-04-19
申请人： Takeshi Azami , Daisuke Kasuya , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka , Sumio Iijima , Eiji Fuchita
发明人： Takeshi Azami , Daisuke Kasuya , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka , Sumio Iijima , Eiji Fuchita
IPC分类号： B01J19/12 , B82Y40/00 , B01D50/00 , B01D45/02 , B01D46/02 , B01D46/48 , B01J8/00 , B82Y30/00 , C01B31/02
CPC分类号： B01D50/002 , B01D45/02 , B01D46/02 , B01D46/48 , B01J8/006 , B01J19/121 , B01J2219/0879 , B82Y30/00 , B82Y40/00 , C01B32/18
摘要： An apparatus for manufacturing carbon nanohorns includes a production chamber configured to irradiate a solid carbon material with a laser beam to produce a product containing carbon nanohorns; and a separation mechanism configured to separate the product produced in the production chamber into a lightweight component and a heavyweight component. The heavyweight component includes carbon nanohorn aggregate with high purity, and high-purity carbon nanotubes can be obtained by collecting the heavyweight component.
摘要翻译：一种用于制造碳纳米角的装置包括：制造室，其配置成用激光束照射固体碳材料，以制造含有碳纳米角的产品; 以及分离机构，其被配置为将在所述生产室中产生的产品分离成轻质部件和重量级部件。重量级组分包括具有高纯度的碳纳米骨聚集体，并且通过收集重质组分可以获得高纯度碳纳米管。

8. 发明申请

US20070003469A1 Carbon nanohorn producing device and carbon nanohorn producing method 有权
标题翻译：碳纳米管生产装置和碳纳米角生产方法
公开(公告)号：US20070003469A1
公开(公告)日：2007-01-04
申请号：US10556088
申请日：2004-05-19
申请人： Takeshi Azami , Daisuke Kasuya , Sumio Iijima , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka
发明人： Takeshi Azami , Daisuke Kasuya , Sumio Iijima , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka
IPC分类号： C01B31/02 , C23C14/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/18 , Y10T117/10 , Y10T117/1004 , Y10T117/1012
摘要： A plume (109) is generated by irradiating a side face of a graphite rod (101) with a laser beam (103) to vaporize carbon. The vaporized carbon is introduced to a carbon nanohorn recovery chamber (119) through a recovery pipe (155), and the vaporized carbon is recovered as a carbon nanohorn assembly (117). A cooling tank (150) including liquid nitrogen (151) is arranged in the recovery pipe (155). While the cooling tank (150) controls the plume (109) at a low temperature, the cooling tank (150) cools the carbon vapor when the carbon vapor passes through the recovery pipe (155). The cooled carbon vapor is recovered as the carbon nanohorn assembly (117) which is controlled in the desired shape and dimensions.
摘要翻译：通过用激光束（103）照射石墨棒（101）的侧面来汽化碳而产生羽流（109）。蒸发的碳通过回收管（155）引入到碳纳米角回收室（119）中，并且蒸发的碳作为碳纳米角组件（117）回收。包括液氮（151）的冷却箱（150）布置在回收管（155）中。当冷却箱（150）在低温下控制羽流（109）时，当碳蒸汽通过回收管（155）时，冷却罐（150）冷却碳蒸汽。冷却的碳蒸汽作为碳纳米角组件（117）回收，其被控制在所需的形状和尺寸。

9. 发明申请

US20090301861A1 Apparatus and Method for Manufacturing Carbon Nanohorns 有权
标题翻译：碳纳米角制造装置及方法
公开(公告)号：US20090301861A1
公开(公告)日：2009-12-10
申请号：US12226570
申请日：2007-04-19
申请人： Takeshi Azami , Daisuke Kasuya , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka , Sumio Iijima , Eiji Fuchita
发明人： Takeshi Azami , Daisuke Kasuya , Tsutomu Yoshitake , Yoshimi Kubo , Masako Yudasaka , Sumio Iijima , Eiji Fuchita
IPC分类号： B01J19/08 , D01F9/12
CPC分类号： B01D50/002 , B01D45/02 , B01D46/02 , B01D46/48 , B01J8/006 , B01J19/121 , B01J2219/0879 , B82Y30/00 , B82Y40/00 , C01B32/18
摘要： An apparatus for manufacturing carbon nanohorns includes a production chamber configured to irradiate a solid carbon material with a laser beam to produce a product containing carbon nanohorns; and a separation mechanism configured to separate the product produced in the production chamber into a lightweight component and a heavyweight component. The heavyweight component includes carbon nanohorn aggregate with high purity, and high-purity carbon nanotubes can be obtained by collecting the heavyweight component.
摘要翻译：一种用于制造碳纳米角的装置包括：制造室，其配置成用激光束照射固体碳材料，以制造含有碳纳米角的产品; 以及分离机构，其被配置为将在所述制造室中产生的产品分离成轻质部件和重量级部件。重量级组分包括具有高纯度的碳纳米骨聚集体，并且通过收集重质组分可以获得高纯度碳纳米管。

10. 发明申请

US20070027029A1 Catalyst support, gas storage body and method for producing these 审中-公开
标题翻译：催化剂载体，储气体及其制备方法
公开(公告)号：US20070027029A1
公开(公告)日：2007-02-01
申请号：US10558979
申请日：2004-05-26
申请人： Daisuke Kasuya , Masako Yudasaka , Takeshi Azami , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima
发明人： Daisuke Kasuya , Masako Yudasaka , Takeshi Azami , Tsutomu Yoshitake , Yoshimi Kubo , Sumio Iijima
IPC分类号： B01J21/18
CPC分类号： B82Y30/00 , B01J20/20 , B01J20/205 , B01J21/185 , B82Y40/00 , C01B3/0021 , C01B32/18 , Y02E60/325 , Y02E60/327 , Y02E60/328 , Y02P20/129
摘要： Plural carbon nanohorn aggregates are mechanically mixed, and catalysts are supported on surfaces of the mixed carbon nanohorn aggregates. Alternatively gas is adsorbed on the surfaces of the mixed carbon nanohorn aggregates.
摘要翻译：将多个碳纳米角骨料机械混合，并将催化剂负载在混合碳纳米角骨料的表面上。或者，气体吸附在混合碳纳米角骨料的表面上。

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