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1. 发明专利

JP2011068581A Process for producing hydroxyvinylnaphthalene compound 审中-公开
标题翻译：生产羟基亚氨基萘化合物的方法
公开(公告)号：JP2011068581A
公开(公告)日：2011-04-07
申请号：JP2009219779
申请日：2009-09-24
申请人： Daicel Chemical Industries Ltd , ダイセル化学工業株式会社
发明人： FUJITA KOHEI , YOKOO TAKESHI
IPC分类号： C07C37/84 , C07C39/225
摘要： PROBLEM TO BE SOLVED: To provide a process for industrially efficiently producing high purity hydroxyvinylnaphthalene with a reduced content of impurities such as a tar content. SOLUTION: The process for producing the hydroxyvinylnaphthalene compound includes a step of subjecting a crude hydroxyvinylnaphthalene compound having a hydroxyl group and a vinyl group on the naphthalene ring to active carbon treatment in the presence of a phenolic radical scavenger at a temperature of 45°C or higher to perform purification. The active carbon treatment is preferably carried out in a mixed solvent of an alcohol and water. After the active carbon treatment, the process may have a step of isolating the hydroxyvinylnaphthalene compound by crystallizing operation. The hydroxyvinylnaphthalene compound includes 2-hydroxy-6-vinylnaphthalene. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供工业上有效生产具有降低的杂质含量如焦油含量的高纯度羟基乙烯基萘的方法。解决方案：羟基乙烯基萘化合物的制造方法包括在酚环状物清除剂的存在下，在45℃的温度下使萘环上具有羟基和乙烯基的粗羟基乙烯基萘化合物进行活性炭处理的步骤 ℃以上进行纯化。活性炭处理优选在醇和水的混合溶剂中进行。在活性炭处理之后，该方法可以具有通过结晶操作分离羟基乙烯基萘化合物的步骤。羟基乙烯基萘化合物包括2-羟基-6-乙烯基萘。版权所有（C）2011，JPO＆INPIT

2. 发明专利

JP2011105672A Method for producing 2-hydroxy-6-vinylnaphthalene 审中-公开
标题翻译： 2-羟基-6-乙烯基苯乙烯的制备方法
公开(公告)号：JP2011105672A
公开(公告)日：2011-06-02
申请号：JP2009264237
申请日：2009-11-19
申请人： Daicel Chemical Industries Ltd , ダイセル化学工業株式会社
发明人： FUJITA KOHEI , YOKOO TAKESHI
IPC分类号： C07C37/50 , C07B61/00 , C07C39/205
摘要： PROBLEM TO BE SOLVED: To provide a method for industrially efficiently producing 2-hydroxy-6-vinylnaphthalene of high purity containing little amount of impurities such as a tar component.
SOLUTION: The production method of 2-hydroxy-6-vinylnaphthalene comprises causing 2-acetoxy-6-vinylnaphthalene having a total content of impurity compounds having a molecular weight of 300-600 of at most 1 wt.% to react with a compound bearing a heteroatom to which an active hydrogen is bonded in the presence of a basic catalyst to give 2-hydroxy-6-vinylnaphthalene.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供一种工业上有效生产含有少量杂质如焦油成分的高纯度2-羟基-6-乙烯基萘的方法。解决方案：2-羟基-6-乙烯基萘的制备方法包括使具有至多1重量％的分子量为300-600的杂质化合物的总含量的2-乙酰氧基-6-乙烯基萘与在碱性催化剂的存在下，与活性氢键合的杂原子的化合物，得到2-羟基-6-乙烯基萘。版权所有（C）2011，JPO＆INPIT

3. 发明专利

JP2011032211A Method for producing alcoholic hydroxy group-containing aryl ester 有权
标题翻译：生产含酒精含羟基的ARYL ESTER的方法
公开(公告)号：JP2011032211A
公开(公告)日：2011-02-17
申请号：JP2009180118
申请日：2009-07-31
申请人： Daicel Chemical Industries Ltd , ダイセル化学工業株式会社
发明人： KITAYAMA KENJI , SUGAWARA MICHIHIRO , YOKOO TAKESHI , HANANO KIEKO
IPC分类号： C07C67/08 , C07B61/00 , C07C69/16
CPC分类号： C07C67/08 , C07C69/017 , C07C69/16
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently industrially producing in high yield at low cost in high operability an aryl ester having in the molecule an alcoholic hydroxy group. SOLUTION: The method comprises reacting a compound having in the molecule an alcoholic hydroxy group and a phenolic hydroxy group with a compound represented by formula: (a) R 1 C(=O)OCOR 2 , (b) R 1 COX, (c) R 3 NHCOX, (d) R 3 N=C=O, (e) R 4 OC(=O)X or (f) R 5 SO 2 X (wherein, R 1 and R 2 are the same as or different from each other, and are H or hydrocarbon group; R 3 , R 4 and R 5 are each a hydrocarbon group; and X is a halogen atom) in the presence of a base with a pKa of 10-15.5 to esterify only the phenolic hydroxy group among the two kinds of hydroxy groups to obtain an aryl ester having an alcoholic hydroxy group in the molecule. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：为了提供一种在高可操作性下以低成本高效率工业生产的方法，在分子中具有醇羟基的芳基酯。解决方案：该方法包括使具有醇羟基和酚羟基的分子中的化合物与下式表示的化合物反应：（a）R 1 =（C = O） SP> 2 ，（b）R 1 COX，（c）R SP 3 NHCOX，（d）R 3 SP = C = O，（e）R（SP）4 OC（= O）X或（f）R 5 SP> 1 和R 2 彼此相同或不同，为H或烃基; R 3 ，R / SP>和R 5 各自为烃基; X为卤素原子），在pKa为10-15.5的碱存在下，仅酯化两种酚型羟基的羟基，得到分子中具有醇羟基的芳基酯。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2010222267A Method for producing 2-hydroxy-6-vinylnaphthalene 审中-公开
标题翻译： 2-羟基-6-乙烯基苯乙烯的制备方法
公开(公告)号：JP2010222267A
公开(公告)日：2010-10-07
申请号：JP2009068914
申请日：2009-03-19
申请人： Daicel Chem Ind Ltd , ダイセル化学工業株式会社
发明人： KITAYAMA KENJI , SUGAWARA MICHIHIRO , YOKOO TAKESHI
IPC分类号： C07C37/01 , C07B61/00 , C07C39/19
摘要： PROBLEM TO BE SOLVED: To provide a method for producing 2-hydroxy-6-vinylnaphthalene, by which the 2-hydroxy-6-vinylnaphthalene can industrially efficiently be produced.
SOLUTION: This method for producing the 2-hydroxy-6-vinylnaphthalene is characterized by reacting a 2-substituted oxy-6-vinylnaphthalene represented by formula (1) [wherein, R is one of R
1 CO-, R
2 NHCO-, R
3 OC(=O)- and R
4 SO
2 -; R
1 is H or a hydrocarbon group; R
2 to R
4 are each a hydrocarbon group] obtained by three stage reactions and the like from 6-hydroxy-2-naphthoaldehyde with a compound having a hetero atom bound to active hydrogen.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：提供2-羟基-6-乙烯基萘的制备方法，通过该方法可以在工业上有效地制备2-羟基-6-乙烯基萘。解决方案：用于制备2-羟基-6-乙烯基萘的方法的特征在于使由式（1）表示的2-取代的氧代-6-乙烯基萘反应[其中，R是R 1， SP> CO-，R 2 NHCO-，R 3 OC（= O） - 和R 4 SO 2 - ; R 1 是H或烃基; 由具有杂原子的化合物与6-羟基-2-萘甲醛的三级反应等得到的R 2 分别为烃基，活性氢。版权所有（C）2011，JPO＆INPIT

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