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1. 发明申请

WO2008013510A2 GRANULATED FERTILIZER CONTAINING WATER SOLUBLE FORMS OF NITROGEN, MAGNESIUM AND SULPHUR, AND METHOD OF ITS PREPARATION 审中-公开
标题翻译：包含水可溶性氮，镁和硫的颗粒肥料及其制备方法
公开(公告)号：WO2008013510A2
公开(公告)日：2008-01-31
申请号：PCT/SK2007/050017
申请日：2007-07-25
申请人： DUSLO A.S. , LENCSES, Ladislav , KRALIK, Milan , LEHOCKY, Peter , STEFANCOVA, Radka , KERDO, Pavol , FERENCI, Michal , POLAK, Anton
发明人： LENCSES, Ladislav , KRALIK, Milan , LEHOCKY, Peter , STEFANCOVA, Radka , KERDO, Pavol , FERENCI, Michal , POLAK, Anton
CPC分类号： C01C1/18 , C01C1/24 , C01F5/40 , C05C1/00 , C05C3/00 , C05D5/00 , C05G3/0058
摘要： Granulated fertilizer, containing water soluble forms of nitrogen, magnesium and sulphur, contains 15 to 30 % by weight of nitrogen, 1 to 18 % by weight of sulphur, 2 to 10 % by weight of magnesium, expressed as magnesium oxide MgO, in the form of boussingaultite - (NH 4 ) 2 SO 4 .MgSO 4 .6H 2 O and binary salts ammonium nitrate - 2NH 4 NO 3 .(NH 4 ) 2 SO 4 and 3NH 4 NO 3 .(NH 4 ) 2 SO 4 , wherein the content of boussingaultite in the fertilizer is 40 to 45 % by weight. Magnesite is treated with concentrated nitric acid containing 30 to 80 % of HNO 3 at a temperature of 60 °C to 130 °C, under formation of reaction mixture containing magnesium nitrate, calcium nitrate, or possibly, according to the content of metallic compounds in magnesite, nitrates of iron, manganese and further metallic elements, and the remainder of undecomposed magnesite, the reaction mixture is subseguently neutralized with an alkaline agent to pH of 3 to 7.5, the neutralized reaction mixture is subseguently left to react with ammonium sulphate at a temperature of 80 to 130 °C for 20 to 80 minutes under formation of a slurry of boussingaultite (NH 4 ) 2 SO 4 -MgSO 4 .6H 2 O, containing 10 to 30 % by weight of water, which slurry is mixed with dried recycle from the preceding production in the ratio of 1 :2 to 1 :10 and it is granulated under formation of wet granulate, from which, after removing free water, the final product is obtained.
摘要翻译：包含水溶性形式的氮，镁和硫的颗粒肥料包含15至30重量％的氮，1至18重量％的硫，2至10重量％的镁，以氧化镁MgO的形式表示，其形式为bou石 - （NH4）2-SO4·MgSO4·4MgSO4。（NH 4）2 O和二元盐硝酸铵 - 2NH 4 NO 3 3（NH 4） 2（SO 4）2和3NH 4 NO 3（NH 4）2 SO 4，其中所述肥料中bou石的含量为40至45重量％。在60℃至130℃的温度下，用包含30至80％HNO 3的浓硝酸处理菱镁矿，形成含有硝酸镁，硝酸钙或可能的反应混合物的反应混合物根据菱镁矿中金属化合物的含量，铁，锰和其它金属元素的硝酸盐以及未分解的菱镁矿的剩余部分，反应混合物随后用碱性试剂随后中和至pH为3-7.5，中和的反应混合物为随后在80-130℃的温度下与硫酸铵在形成bou石（NH 4）2 SO 4的淤浆形成20至80分钟之后与硫酸铵反应，其包含10-30重量％的水，所述浆液与来自前述生产的干燥循环物混合以1：2至1：10的比例混合，并在湿颗粒形成时造粒，从中除去游离水后，将fi 最终产品。

2. 发明申请

WO2005051886A1 METHOD OF PREPARATION OF N-(1-PHENYLETHYL)-N'-PHENYL-1,4-PHENYLENEDIAMINE AND USE THEREOF 审中-公开
标题翻译：制备N-（1-苯基乙烯基）-N'-苯基-1,4-苯乙烯胺的方法及其用途
公开(公告)号：WO2005051886A1
公开(公告)日：2005-06-09
申请号：PCT/SK2004/000014
申请日：2004-11-25
申请人： DUSLO A.S. , MACAK, Ivan , UHLAR, Jan , LEHOCKY, Peter , VAGNEROVA, Hiyam , BIRO, Pavel
发明人： MACAK, Ivan , UHLAR, Jan , LEHOCKY, Peter , VAGNEROVA, Hiyam , BIRO, Pavel
IPC分类号： C07C209/26
CPC分类号： C07C209/26 , C07C211/55
摘要： N -(1-phenylethyl)- N' -phenyl-1,4-phenylenediamine of high purity is produced by a two-step synthesis, where in the first step 4-aminodiphenylamine reacts with acetophenone in the presence of an acidic catalyst. The reaction is performed to an incomplete conversion of 4-aminodiphenylamine, whereby an intermediate product of high purity is obtained, which is hydrogenated on a heterogeneous catalyst in the second step. N -(1-phenylethyl)- N' -phenyl-1,4-phenylenediamine can be used as a component of anti-degradation systems.
摘要翻译：通过两步合成制备高纯度的N-（1-苯基乙基）-N'-苯基-1,4-苯二胺，其中在第一步中，4-氨基二苯胺在酸性催化剂存在下与苯乙酮反应。反应进行到4-氨基二苯胺的不完全转化，由此得到高纯度的中间产物，其在第二步中在非均相催化剂上氢化。 N-（1-苯乙基）-N'-苯基-1,4-苯二胺可用作抗降解体系的组分。

3. 发明申请

WO2005052050A1 ANTIOXIDANT COMPOSITIONS OF OCTYLATED DIPHENYLAMINES AND METHOD OF THEIR PREPARATION 审中-公开
标题翻译：十二烷基苯胺的抗氧化剂组合物及其制备方法
公开(公告)号：WO2005052050A1
公开(公告)日：2005-06-09
申请号：PCT/SK2004/000013
申请日：2004-11-25
申请人： DUSLO A.S. , ANDRUSKOVA, Viera , UHLAR, Jan , LEHOCKY, Peter , HORAK, Jaroslav
发明人： ANDRUSKOVA, Viera , UHLAR, Jan , LEHOCKY, Peter , HORAK, Jaroslav
IPC分类号： C08K5/00
CPC分类号： C08K5/18 , C08K2201/014
摘要： Antioxidant compositions of octylated diphenylamines, containing 65 to 98% by weight of dioctyldiphenylamine, up to 29 % by weight of monooctyldiphenylamine, up to 5 % by weight of octylbutyldiphenylamine, up to 1.5 % by weight of trioctyldiphenylamine and up to 1 % by weight of diphenylamine, are prepared by alkylation of diphenylamine by diisobutylene in the presence of an acidic catalyst. They can be used as efficient stabilizers of polymeric materials, lubricants and oils, either alone or as a component of anti-degradation systems and substances based on them.
摘要翻译：辛基化二苯胺的抗氧化剂组合物，含有65-98重量％的二辛基二苯胺，至多29重量％的单辛基二苯胺，最多5重量％的辛基丁基二苯胺，至多1.5重量％的三辛基二苯胺和至多1重量％二苯胺通过在酸性催化剂的存在下通过二异丁烯烷基化二苯胺来制备。它们可以作为高分子材料，润滑剂和油的有效稳定剂，单独使用或作为抗降解体系和基于它们的物质的组分。

4. 发明授权

EP2051953B1 GRANULATED FERTILIZER CONTAINING WATER SOLUBLE FORMS OF NITROGEN, MAGNESIUM AND SULPHUR, AND METHOD OF ITS PREPARATION 有权
标题翻译：肥料颗粒使氮，镁，硫成分：水可溶性形式，以及生产方法
公开(公告)号：EP2051953B1
公开(公告)日：2010-04-28
申请号：EP07769076.6
申请日：2007-07-25
申请人： Duslo, A.S.
发明人： LENCSES, Ladislav , KRALIK, Milan , LEHOCKY, Peter , STEFANCOVA, Radka , KERDO, Pavol , FERENCI, Michal , POLAK, Anton
IPC分类号： C05C1/00 , C05C3/00 , C05D5/00 , C05D9/00
CPC分类号： C01C1/18 , C01C1/24 , C01F5/40 , C05C1/00 , C05C3/00 , C05D5/00 , C05G3/0058
摘要： Granulated fertilizer, containing water soluble forms of nitrogen, magnesium and sulphur, contains 15 to 30 % by weight of nitrogen, 1 to 18 % by weight of sulphur, 2 to 10 % by weight of magnesium, expressed as magnesium oxide MgO, in the form of boussingaultite - (NH4)2SO4.MgSO4.6H2O and binary salts ammonium nitrate - 2NH4NO3.(NH4)2SO4 and 3NH4NO3.(NH4)2SO4, wherein the content of boussingaultite in the fertilizer is 40 to 45 % by weight. Magnesite is treated with concentrated nitric acid containing 30 to 80 % of HNO3 at a temperature of 60 °C to 130 °C, under formation of reaction mixture containing magnesium nitrate, calcium nitrate, or possibly, according to the content of metallic compounds in magnesite, nitrates of iron, manganese and further metallic elements, and the remainder of undecomposed magnesite, the reaction mixture is subseguently neutralized with an alkaline agent to pH of 3 to 7.5, the neutralized reaction mixture is subseguently left to react with ammonium sulphate at a temperature of 80 to 130 °C for 20 to 80 minutes under formation of a slurry of boussingaultite (NH4)2SO4-MgSO4.6H2O, containing 10 to 30 % by weight of water, which slurry is mixed with dried recycle from the preceding production in the ratio of 1 :2 to 1 :10 and it is granulated under formation of wet granulate, from which, after removing free water, the final product is obtained.

5. 发明公开

EP1694757A1 ANTIOXIDANT COMPOSITION OF OCTYLATED DIPHENYLAMINE AND PROCESS OF PREPARATION THEREOF 有权
标题翻译：抗氧化剂用于生产辛基化二苯胺和流程
公开(公告)号：EP1694757A1
公开(公告)日：2006-08-30
申请号：EP04800460.0
申请日：2004-11-25
申请人： Duslo A.S.
发明人： ANDRUSKOVA, Viera , UHLAR, Jan , LEHOCKY, Peter , HORAK, Jaroslav
IPC分类号： C08K5/00
CPC分类号： C08K5/18 , C08K2201/014
摘要： Antioxidant compositions of octylated diphenylamines, containing 65 to 98% by weight of dioctyldiphenylamine, up to 29 % by weight of monooctyldiphenylamine, up to 5 % by weight of octylbutyldiphenylamine, up to 1.5 % by weight of trioctyldiphenylamine and up to 1 % by weight of diphenylamine, are prepared by alkylation of diphenylamine by diisobutylene in the presence of an acidic catalyst. They can be used as efficient stabilizers of polymeric materials, lubricants and oils, either alone or as a component of anti-degradation systems and substances based on them.

6. 发明公开

EP2051953A2 GRANULATED FERTILIZER CONTAINING WATER SOLUBLE FORMS OF NITROGEN, MAGNESIUM AND SULPHUR, AND METHOD OF ITS PREPARATION 有权
标题翻译：肥料颗粒使氮，镁，硫成分：水可溶性形式，以及生产方法
公开(公告)号：EP2051953A2
公开(公告)日：2009-04-29
申请号：EP07769076.6
申请日：2007-07-25
申请人： Duslo, A.S.
发明人： LENCSES, Ladislav , KRALIK, Milan , LEHOCKY, Peter , STEFANCOVA, Radka , KERDO, Pavol , FERENCI, Michal , POLAK, Anton
IPC分类号： C05C1/00 , C05C3/00 , C05D5/00 , C05D9/00
CPC分类号： C01C1/18 , C01C1/24 , C01F5/40 , C05C1/00 , C05C3/00 , C05D5/00 , C05G3/0058
摘要： Granulated fertilizer, containing water soluble forms of nitrogen, magnesium and sulphur, contains 15 to 30 % by weight of nitrogen, 1 to 18 % by weight of sulphur, 2 to 10 % by weight of magnesium, expressed as magnesium oxide MgO, in the form of boussingaultite - (NH4)2SO4.MgSO4.6H2O and binary salts ammonium nitrate - 2NH4NO3.(NH4)2SO4 and 3NH4NO3.(NH4)2SO4, wherein the content of boussingaultite in the fertilizer is 40 to 45 % by weight. Magnesite is treated with concentrated nitric acid containing 30 to 80 % of HNO3 at a temperature of 60 °C to 130 °C, under formation of reaction mixture containing magnesium nitrate, calcium nitrate, or possibly, according to the content of metallic compounds in magnesite, nitrates of iron, manganese and further metallic elements, and the remainder of undecomposed magnesite, the reaction mixture is subseguently neutralized with an alkaline agent to pH of 3 to 7.5, the neutralized reaction mixture is subseguently left to react with ammonium sulphate at a temperature of 80 to 130 °C for 20 to 80 minutes under formation of a slurry of boussingaultite (NH4)2SO4-MgSO4.6H2O, containing 10 to 30 % by weight of water, which slurry is mixed with dried recycle from the preceding production in the ratio of 1 :2 to 1 :10 and it is granulated under formation of wet granulate, from which, after removing free water, the final product is obtained.

7. 发明授权

EP1694757B1 ANTIOXIDANT COMPOSITION OF OCTYLATED DIPHENYLAMINE AND PROCESS OF PREPARATION THEREOF 有权
标题翻译：抗氧化剂用于生产辛基化二苯胺和流程
公开(公告)号：EP1694757B1
公开(公告)日：2008-01-02
申请号：EP04800460.0
申请日：2004-11-25
申请人： Duslo, a.s.
发明人： ANDRUSKOVA, Viera , UHLAR, Jan , LEHOCKY, Peter , HORAK, Jaroslav
IPC分类号： C08K5/00
CPC分类号： C08K5/18 , C08K2201/014
摘要： Antioxidant compositions of octylated diphenylamines, containing 65 to 98% by weight of dioctyldiphenylamine, up to 29 % by weight of monooctyldiphenylamine, up to 5 % by weight of octylbutyldiphenylamine, up to 1.5 % by weight of trioctyldiphenylamine and up to 1 % by weight of diphenylamine, are prepared by alkylation of diphenylamine by diisobutylene in the presence of an acidic catalyst. They can be used as efficient stabilizers of polymeric materials, lubricants and oils, either alone or as a component of anti-degradation systems and substances based on them.

8. 发明申请

WO2006068627A1 USE OF CONDENSATION PRODUCTS OF FATTY ACIDS, ALCOHOLS, PHENOLS, ALKYL PHENOLS AND AMINES WITH ETHYLENE OXIDE AND/OR PROPYLENE OXIDE AS AN ESSENTIAL OR SOLE COMPONENT OF AN ADDITIVE 审中-公开
标题翻译：使用脂肪酸，醇，酚，烷基酚和与乙烯氧化物和/或丙烯氧化物的氨基酸作为添加剂的基本成分或单一成分的冷凝产物
公开(公告)号：WO2006068627A1
公开(公告)日：2006-06-29
申请号：PCT/SK2005/000024
申请日：2005-12-15
申请人： VUCHT, a.s. , KOSAR, Karol , DURACKA, Miroslav , SUSTEK, Jan , RISKA, Miloslav , LEHOCKY, Peter , SANDTNER, Stanislav , BALKO, Jozef
发明人： KOSAR, Karol , DURACKA, Miroslav , SUSTEK, Jan , RISKA, Miloslav , LEHOCKY, Peter , SANDTNER, Stanislav , BALKO, Jozef
IPC分类号： C08K5/04
CPC分类号： C08K5/0025 , C08K5/17 , C08K9/04 , C08L21/00
摘要： The invention concerns the use of condensation products of fatty acids, alcohols, phenols, alkyl phenols and amines with ethylene oxide and/or propylene oxide, either one or a mixture of several types of these condensation products, as a main (essential) or sole component of an additive in compacting wet powders of admixtures to polymers, or an additive for admixtures to polymers in powder form. Using additives according to the present invention low dusting and in polymers well dispersing powders or granulates/pellets are obtained, dispersibility of which is better or comparable to not adjusted form of a given admixture. Additives according to the present invention are added before compaction of admixtures to polymers in an amount of 0.01 to 15 weight parts, preferably of 0.1 to 2 weight parts with respect to 100 weight parts of a given admixture to polymers. They are added in the given range also in the production of final powder forms of admixtures to polymers. Additives according to the present invention may be applied to all types of water-insoluble admixtures to polymers. They are especially suitable for rubber chemicals like, for example, vulcanization agents, vulcanization accelerators, vulcanization activators, pre-vulcanization inhibitors, antidegradants, anti-reversion agents, surfactants, fillers and the like.
摘要翻译：本发明涉及使用脂肪酸，醇，酚，烷基酚和胺与环氧乙烷和/或环氧丙烷的缩合产物，其中一种或多种类型的这些缩合产物的混合物作为主要（必需）或单体在将聚合物的混合物的湿粉末压实的添加剂的组分或用于与粉末形式的聚合物混合的添加剂。使用根据本发明的添加剂，可以获得低粉尘和在分散粉末或颗粒/丸粒的聚合物中，其分散性优于或与给定混合物的未调节形式相当。相对于100重量份给定的聚合物的混合物，加入相对于聚合物的混合物的添加剂的添加量为0.01至15重量份，优选为0.1至2重量份。它们在给定范围内也加入到聚合物的最终粉末形式的混合物中。根据本发明的添加剂可以应用于聚合物的所有类型的水不溶性混合物。它们特别适用于橡胶化学品，例如硫化剂，硫化促进剂，硫化活化剂，预硫化抑制剂，抗降解剂，抗反转剂，表面活性剂，填料等。

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