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1. 发明专利

JP2005132716A Plasma synthesis of metal oxide nanoparticle 审中-公开
标题翻译：金属氧化物纳米粒子的等离子体合成
公开(公告)号：JP2005132716A
公开(公告)日：2005-05-26
申请号：JP2004265979
申请日：2004-09-13
申请人： E I Du Pont De Nemours & Co , イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company
发明人： ZHANG LU
IPC分类号： A61K8/19 , A61K8/26 , A61K8/29 , B01J19/08 , B01J19/26 , B01J21/08 , B01J23/00 , B01J35/02 , B82B3/00 , C01B13/00 , C01B13/14 , C01B13/28 , C01B33/18 , C01B35/10 , C01C1/00 , C01D1/02 , C01G23/00 , C01G23/04 , C01G23/047 , C01G23/07 , C01G99/00 , C08K3/22 , A61K7/00
CPC分类号： C01G23/07 , B01J19/088 , B01J19/26 , B01J2219/0883 , B82Y30/00 , C01G23/002 , C01G23/04 , C01P2004/64 , C01P2006/12
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing particles containing metal oxides, nanoparticles in particular, which are specifically nano-size particles containing titanium dioxide.
SOLUTION: The process for synthesizing nano-size metal oxide particles in a plasma reactor comprises a process (a) where one or a plurality of reactant flows containing an oxidizing agent and a halogenated metal, a halogenated silicon, and a coarse tail controlling agent selected from a group comprising halogenated compounds of phosphorus, germanium, boron, tin, niobium, chromium, silver, gold, palladium, aluminum, and their mixtures are supplied simultaneously and a process (b) where the reactant flows and the oxidizing agent are brought into contact with plasma having a sufficient temperature to form metal oxide-containing nanoparticles having an average particle diameter of 200 nm.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种制造具有特别是含有二氧化钛的纳米尺寸颗粒的金属氧化物，特别是纳米颗粒的颗粒的方法。解决方案：在等离子体反应器中合成纳米尺寸金属氧化物颗粒的方法包括一种方法（a）其中一种或多种反应物流动含有氧化剂和卤化金属，卤化硅和粗尾同时提供选自磷，锗，硼，锡，铌，铬，银，金，钯，铝及其混合物的卤化化合物的组的控制剂，以及反应物流动的方法（b）和氧化剂与具有足够温度的等离子体接触以形成平均粒径<100nm并含有少量直径> 200nm的颗粒的含金属氧化物的纳米颗粒。版权所有（C）2005，JPO＆NCIPI

2. 发明专利

JP2005289798A Manufacturing process for titanium dioxide nanopowder 审中-公开
标题翻译：二氧化钛纳米粒子的制造工艺
公开(公告)号：JP2005289798A
公开(公告)日：2005-10-20
申请号：JP2005077668
申请日：2005-03-17
申请人： E I Du Pont De Nemours & Co , イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company
发明人： MUSICK CHARLES DAVID , REID AUSTIN H JR , ZHANG LU
IPC分类号： B82B3/00 , C01G23/04 , C01G23/07
CPC分类号： B82Y30/00 , C01G23/07 , C01P2004/51 , C01P2004/64 , C01P2006/12 , C01P2006/60 , Y10S977/773 , Y10S977/775 , Y10S977/777 , Y10S977/811
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing process for titanium dioxide nanopowder controlled in grain size.
SOLUTION: The manufacturing process for titanium dioxide nanopowder comprises: (a) reacting titanium tetrachloride and an oxygen-containing gas in the vapor phase in a flame reactor, at a specific temperature and pressure in the presence of a specified concentration of steam, a diluent gas and a nucleating agent consisting essentially of a cesium-containing substance, wherein the cesium-containing substance is present in an amount ranging from about 10 to about 5,000 parts per million, to the weight of the titanium dioxide under production, to form titanium dioxide nanopowder; and (b) recovering the titanium dioxide nanopowder having a surface area in the range of about 30 to about 300 m
2 /g and wherein about 50 volume percent of the particles have a diameter of about 80 nm or less and wherein about 90 volume percent of the particles have a diameter of about 100 nm or less.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：提供以粒度控制的二氧化钛纳米粉末的制造方法。解决方案：二氧化钛纳米粉末的制造方法包括：（a）在特定温度和压力下，在特定浓度的蒸汽存在下，在火焰反应器中，在气相中使四氯化钛与含氧气体反应，稀释气体和基本上由含铯物质组成的成核剂，其中所述含铯物质的存在量为约10至约5,000ppm，与生产中的二氧化钛的重量相对于形成二氧化钛纳米粉体; 和（b）回收表面积在约30至约300m 2 / SP / g范围内的二氧化钛纳米粉末，其中约50体积％的颗粒具有约80nm的直径或并且其中约90体积％的颗粒具有约100nm或更小的直径。版权所有（C）2006，JPO＆NCIPI

3. 发明专利

JP2005104830A Plasma synthesis of metal oxide nanoparticle 审中-公开
标题翻译：金属氧化物纳米粒子的等离子体合成
公开(公告)号：JP2005104830A
公开(公告)日：2005-04-21
申请号：JP2004265980
申请日：2004-09-13
申请人： E I Du Pont De Nemours & Co , イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーE.I.Du Pont De Nemours And Company
发明人： ZHANG LU
IPC分类号： H05H1/42 , B01J19/08 , B01J19/26 , B01J31/00 , B82B3/00 , C01B13/00 , C01B13/14 , C01B13/28 , C01B33/18 , C01B35/10 , C01C1/00 , C01D1/02 , C01G1/02 , C01G23/047 , C01G23/07 , C01G25/02 , C01G27/02 , C01G99/00 , C08F4/02 , C08F4/60
CPC分类号： B82Y30/00 , B01J19/088 , B01J19/26 , B01J2219/00094 , B01J2219/0883 , B01J2219/0894 , C01B33/18 , C01B33/183 , C01B35/1027 , C01G1/02 , C01G23/07 , C01G25/02 , C01G27/02 , C01P2004/62 , C01P2004/64 , C01P2006/12 , Y10S423/10 , Y10S977/773 , Y10S977/775 , Y10S977/777 , Y10S977/811
摘要： PROBLEM TO BE SOLVED: To provide a method of manufacturing metal oxide particles which are improved in dispersibility and particle size characteristics and have a substantially single mode particle diameter distribution.
SOLUTION: The method for synthesizing particles containing nano-sized metal oxide by a plasma process includes a process for forming the nanoparticles of metal oxide by reacting a metal halide with oxygen in a gas phase in the presence of a hydrogen source, wherein the average particle diameter is 100 nm particle diameter.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种制造金属氧化物颗粒的方法，所述金属氧化物颗粒的分散性和粒度特性得到改进，并且具有基本上单模粒径分布。解决方案：通过等离子体工艺合成含有纳米尺寸金属氧化物的颗粒的方法包括通过在氢源的存在下在气相中使金属卤化物与氧反应形成金属氧化物纳米颗粒的方法，其中平均粒径<100nm，粒子聚集体的矿石比例> 100nm粒径。版权所有（C）2005，JPO＆NCIPI

4. 发明申请

WO2007041313A3 ELECTROCHEMICAL DOUBLE LAYER CAPACITORS INCLUDING IMPROVED NANOFIBER SEPARATORS 审中-公开
标题翻译：电化学双层电容器，包括改进的纳米纤维分离器
公开(公告)号：WO2007041313A3
公开(公告)日：2007-06-21
申请号：PCT/US2006038098
申请日：2006-09-29
申请人： DU PONT , ARORA PANKAJ , FRISK SIMON , ZHANG LU
发明人： ARORA PANKAJ , FRISK SIMON , ZHANG LU
IPC分类号： H01G9/02 , H01G9/155 , H01M2/16
CPC分类号： H01G9/02 , H01G9/155 , H01G11/52 , H01M2/162 , H01M2/1626 , Y02E60/13
摘要： Electrochemical double layer capacitors are disclosed that advantageously include separators comprising at least one porous layer of nanofibers having average diameters of between about 50 nm and about 1000 nm that provide improved combinations of reduced thickness, barrier against the development of soft short-circuits and low ionic resistance as compared with known capacitor separators.
摘要翻译：公开了电化学双层电容器，其有利地包括隔板，该隔板包括至少一个平均直径在约50nm和约1000nm之间的纳米纤维多孔层，其提供改进的组合减小的厚度，阻止发生软短路和低离子与已知的电容分离器相比具有更高的电阻

5. 发明申请

WO2004056461A2 METHOD OF PRODUCING NANOPARTICLES USING A EVAPORATION-CONDENSATION PROCESS WITH A REACTION CHAMBER PLASMA REACTOR SYSTEM 审中-公开
标题翻译：使用具有反应室反应器系统的蒸发 - 凝聚方法生产纳米颗粒的方法
公开(公告)号：WO2004056461A2
公开(公告)日：2004-07-08
申请号：PCT/US0340246
申请日：2003-12-16
申请人： DU PONT , DE LA VEAUX STEPHEN CLAUDE , ZHANG LU
发明人： DE LA VEAUX STEPHEN CLAUDE , ZHANG LU
IPC分类号： B01J20060101 , B01J2/04 , B01J19/08 , B01J19/24 , B01J19/26 , B82B3/00 , C01G1/02 , C01G23/07 , B01J
CPC分类号： B01J19/088 , B01J19/26 , B01J2219/0871 , B01J2219/0883 , B01J2219/0894 , B22F9/28 , B22F2998/00 , B82Y30/00 , C01G1/00 , C01G1/02 , C01G23/07 , C01G23/075 , C01P2004/03 , C01P2004/64 , C01P2006/12 , C01P2006/64 , C22B4/005 , C22B34/1222 , C22B34/1227 , Y02P10/23 , B22F2202/13
摘要： The present invention provides a method and apparatus for the controlled synthesis of nanoparticles using a high temperature process. The reactor chamber includes a high temperature gas heated by means such as a plasma torch, and a reaction chamber. The homogenizer includes a region between the reactant inlets and the plasma (the spacer zone) to ensure that feeds from the reactant inlets are downstream of the recirculation zone induced by the high temperature gas. It also includes a region downstream of the reactant inlets that provides a nearly 1 dimensional (varying only in the axial direction) flow and concentration profile in the reaction zone to produce nanoparticles with narrow size distribution.
摘要翻译：本发明提供了一种使用高温工艺控制纳米颗粒合成的方法和装置。反应室包括通过诸如等离子体焰炬和反应室等手段加热的高温气体。均化器包括反应物入口和等离子体之间的区域（间隔区），以确保来自反应物入口的进料位于由高温气体引起的再循环区域的下游。它还包括反应物入口的下游区域，其在反应区域中提供接近1维（仅在轴向方向上变化）流动和浓度分布，以产生具有窄尺寸分布的纳米颗粒。

6. 发明申请

WO2009126605A3 AIR FILTRATION MEDIUM WITH IMPROVED DUST LOADING CAPACITY AND IMPROVED RESISTANCE TO HIGH HUMIDITY ENVIRONMENT 审中-公开
标题翻译：空气过滤介质具有改进的除尘能力和改善对高湿度环境的抵抗力
公开(公告)号：WO2009126605A3
公开(公告)日：2010-03-25
申请号：PCT/US2009039742
申请日：2009-04-07
申请人： DU PONT , CHI CHENG-HANG , LIM HYUN SUNG , ZHANG LU
发明人： CHI CHENG-HANG , LIM HYUN SUNG , ZHANG LU
IPC分类号： B01D39/16
CPC分类号： B01D39/1623
摘要： A filtration medium is disclosed for use in air filters used in heating, ventilating and air conditioning systems. The medium contains at least one nanofiber layer of fibers having diameters less than 1 µm and at least one upstream layer, the medium having sufficient holding capacity for dust particles that efficiency loss and pressure loss across the medium are minimized during use.
摘要翻译：公开了用于加热，通风和空调系统中使用的空气过滤器的过滤介质。该介质包含至少一个直径小于1μm的纤维纳米纤维层和至少一个上游层，该介质具有足够的灰尘颗粒保持能力，使得在使用过程中介质上的效率损失和压力损失最小化。

7. 发明专利

BRPI0617556A2 未知
公开(公告)号：BRPI0617556A2
公开(公告)日：2011-07-26
申请号：BRPI0617556
申请日：2006-09-29
申请人： DU PONT
发明人： ARORA PANKAJ , FRISK SIMON , ZHANG LU
IPC分类号： H01M2/16 , H01G9/00 , H01M2/14 , H01M4/26 , H01M10/0525
摘要： Alkaline batteries are disclosed that advantageously include separators comprising at least one porous layer of fine fibers having a diameter of between about 50 nm and about 3000 nm that provide improved combinations of reduced thickness, dendritic barrier against short-circuiting and low ionic resistance as compared with known battery separators.

8. 发明专利

CA2500813A1 TITANIUM DIOXIDE NANOPOWDER MANUFACTURING PROCESS 未知
公开(公告)号：CA2500813A1
公开(公告)日：2005-09-19
申请号：CA2500813
申请日：2005-03-15
申请人： DU PONT
发明人： ZHANG LU , MUSICK CHARLES DAVID , REID AUSTIN H JR
IPC分类号： B82B3/00 , C01G23/04 , C01G23/07
摘要： Titanium dioxide nanopowder is produced by a process, comprising: (a) reacting titanium tetrachloride and an oxygen containing gas in the vapor phase in a flame reactor, at a flame temperature of at least about 800.degree.C, a pressure ranging from about -35 to about 172 kPa (about -5 to about 25 psig) in the presence of (i) water vapor in an amount ranging from about 1000 to abou t 50,000 parts per million; based on the weight of titanium dioxide under production, (ii) a diluent gas in an amount greater than about 100 mole percent based on the titanium tetrachloride and oxygen containing gas and (iii) a nucleant consisting essentially of a cesium substance wherein the cesium substance is present in an amount ranging from about 10 to about 5000 parts per million, based on the weight of the titanium dioxide under production, to form titanium dioxide nanopowder, and recovering the titanium dioxide nanopowder having a surface area in the range of about 30 to about 300 m2/g and wherein about 50 volume percent of the particles have a diameter of about 80 nm or less and wherein about 90 volume percent of the particles have a diameter of about 100 nm or less.

9. 发明专利

CA2481150A1 PLASMA SYNTHESIS OF METAL OXIDE NANOPARTICLES 未知
公开(公告)号：CA2481150A1
公开(公告)日：2005-03-11
申请号：CA2481150
申请日：2004-09-10
申请人： DU PONT
发明人： ZHANG LU
IPC分类号： A61K8/19 , A61K8/26 , A61K8/29 , B01J19/08 , B01J19/26 , B01J21/08 , B01J23/00 , B01J35/02 , B82B3/00 , C01B13/00 , C01B13/14 , C01B13/28 , C01B33/18 , C01B35/10 , C01C1/00 , C01D1/02 , C01G23/00 , C01G23/04 , C01G23/047 , C01G23/07 , C01G99/00 , C08K3/22 , C09D1/00 , B22F1/00 , B01J19/00
摘要： A process for minimizing and even eliminating over-sized particles in a vapor phase synthesis of metal oxide-containing particles comprising reacting oxygen with one of more vapor streams comprising a titanium halide, a silicon halide and a compound selected from the group consisting of phosphorous, germanium, boron, tin, niobium, chromium, silver, gold, palladium aluminum, and mixtures thereof in a plug flow, plasma reactor.

10. 发明专利

CA2481152A1 PLASMA SYNTHESIS OF METAL OXIDE NANOPARTICLES 未知
公开(公告)号：CA2481152A1
公开(公告)日：2005-03-11
申请号：CA2481152
申请日：2004-09-10
申请人： DU PONT
发明人： ZHANG LU
IPC分类号： H05H1/42 , B01J19/08 , B01J19/26 , B01J31/00 , B82B3/00 , C01B13/00 , C01B13/14 , C01B13/28 , C01B33/18 , C01B35/10 , C01C1/00 , C01D1/02 , C01G1/02 , C01G23/047 , C01G23/07 , C01G25/02 , C01G27/02 , C01G99/00 , C08F4/02 , C08F4/60 , C01B13/20
摘要： The present invention is a method of increasing particle surface area and decreasing the concentration of over-sized particles. in a process for making metal oxide particles, particularly nanoparticle TiO2,in an inlet-fed, plug flow, plasma reactor by vapor phase reaction of titanium tetrachloride and oxygen in the presence of a source of hydrogen to form titanium dioxide particles.

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