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1. 发明授权

US09840605B2 Flame-retardant copolymers of dialkyl (meth)acryloyloxyalkyl phosphate or dialkyl (meth)acryloyloxyalkyl phosphonate monomers and polymer foams based made therefrom 有权
公开(公告)号：US09840605B2
公开(公告)日：2017-12-12
申请号：US15100956
申请日：2013-12-27
申请人： DOW GLOBAL TECHNOLOGIES LLC , Yudong Qi , Yan Li , Shana P. Bunker , Stephane Costeux , Ted A. Morgan
发明人： Yudong Qi , Yan Li , Shana P. Bunker , Stephane Costeux , Ted A. Morgan
IPC分类号： C08J9/12 , C09K21/14 , C08F220/14 , C08J9/00 , C08F220/00
CPC分类号： C08J9/122 , C08F220/14 , C08F230/02 , C08J9/0061 , C08J9/12 , C08J2201/032 , C08J2203/06 , C08J2203/08 , C08J2205/042 , C08J2205/044 , C08J2325/12 , C08J2333/04 , C08J2333/10 , C08J2333/12 , C08J2343/00 , C08J2343/02 , C08J2425/12 , C08J2433/04 , C08J2433/12 , C08J2443/02 , C08L33/12 , C09K21/14 , C08L43/02
摘要： Polymer foam bodies are made from phosphorus-containing thermoplastic random copolymers of a dialkyl (meth)acryloyloxyalkyl phosph(on)ate. Foam bodies made from these copolymers exhibit increased limiting oxygen indices and surprisingly have good properties. In certain embodiments, the phosphorus-containing thermoplastic copolymer is blended with one or more other polymers and formed into nanofoams.

2. 发明申请

US20160304692A1 FLAME-RETARDANT COPOLYMERS OF DIALKYL (METH)ACRYLOYLOXYALKYL PHOSPHATE OR DIALKYL (METH)ACRYLOYLOXYALKYL PHOSPHONATE MONOMERS AND POLYMER FOAMS BASED MADE THEREFROM 有权
标题翻译：二甲基（甲基）丙烯酰氧基戊基磷酸酯或二烷基（甲基）丙烯酰氧基甲基磷酸酯单体和基于聚合物的聚合物的阻燃共聚物
公开(公告)号：US20160304692A1
公开(公告)日：2016-10-20
申请号：US15100956
申请日：2013-12-27
申请人： Yudong QI , Yan LI , Shana P. BUNKER , Stephane COSTEUX , Ted A. MORGAN , DOW GLOBAL TECHNOLOGIES LLC
发明人： Yudong Qi , Yan Li , Shana P. Bunker , Stephane Costeux , Ted A. Morgan
IPC分类号： C08J9/12 , C09K21/14 , C08J9/00 , C08F220/14
CPC分类号： C08J9/122 , C08F220/14 , C08F230/02 , C08J9/0061 , C08J9/12 , C08J2201/032 , C08J2203/06 , C08J2203/08 , C08J2205/042 , C08J2205/044 , C08J2325/12 , C08J2333/04 , C08J2333/10 , C08J2333/12 , C08J2343/00 , C08J2343/02 , C08J2425/12 , C08J2433/04 , C08J2433/12 , C08J2443/02 , C08L33/12 , C09K21/14 , C08L43/02
摘要： Polymer foam bodies are made from phosphorus-containing thermoplastic random copolymers of a dialkyl (meth)acryloyloxyalkyl phosph(on)ate. Foam bodies made from these copolymers exhibit increased limiting oxygen indices and surprisingly have good properties. In certain embodiments, the phosphorus-containing thermoplastic copolymer is blended with one or more other polymers and formed into nanofoams.
摘要翻译：聚合物泡沫体由（a）二烷基（甲基）丙烯酰氧基烷基磷酸酯的含磷热塑性无规共聚物制成。由这些共聚物制成的泡沫体显示出增加的极限氧指数，令人惊奇地具有良好的性能。在某些实施方案中，含磷热塑性共聚物与一种或多种其它聚合物共混并形成纳米电子烟。

3. 发明授权

US09187611B2 Nanoporous polymeric foam having high cell density without nanofiller 有权
标题翻译：具有高电池密度的纳米聚合物泡沫，无纳米填料
公开(公告)号：US09187611B2
公开(公告)日：2015-11-17
申请号：US13578092
申请日：2011-02-23
申请人： Stephane Costeux , Lingbo Zhu , Hyun Jeon , Shana P. Bunker , Thomas H. Kalantar
发明人： Stephane Costeux , Lingbo Zhu , Hyun Jeon , Shana P. Bunker , Thomas H. Kalantar
IPC分类号： C08J9/12 , C08J9/00
CPC分类号： C08J9/122 , C08J9/0071 , C08J2201/024 , C08J2201/032 , C08J2205/046 , C08J2333/10
摘要： A polymeric foam has a thermoplastic polymer matrix defining multiple cells, the foam characterized by: (a) the polymer matrix having greater than 50 weight-percent copolymer containing at least two different monomers at least one of which is a methacrylate monomer, each monomer having a solubility parameter lower than 20 (megaPascals)0.5 and a chemical composition where twice the mass fraction of oxygen plus the mass fraction of nitrogen, fluorine and silicon is greater than 0.2; wherein the monomers comprise at least 90 weight-percent of all monomers in the copolymer; (b) at least one of the following: (i) a nucleation site density of at least 3×1014 effective nucleation sites per cubic centimeter of foamable polymer composition; (ii) an average cell size of 300 nanometer or less; (c) a porosity percentage greater than 30%; (d) an absence of nano-sized nucleating additive; and (e) a thickness of at least one millimeter.
摘要翻译：聚合物泡沫具有限定多个细胞的热塑性聚合物基质，泡沫的特征在于：（a）聚合物基质具有大于50重量％的共聚物，其含有至少两个不同的单体，其中至少一个是甲基丙烯酸酯单体，每个单体具有溶解度参数低于20（兆帕）和化学组成，其中氧质量分数加上氮，氟和硅质量分数的两倍大于0.2; 其中所述单体包含所述共聚物中所有单体的至少90重量％（b）以下至少之一：（i）成核位点密度为每立方厘米可发泡聚合物组合物至少3×1014个有效成核位点; （ii）平均泡孔尺寸为300纳米以下; （c）孔隙率大于30％; （d）不存在纳米尺寸的成核添加剂; 和（e）至少一毫米的厚度。

4. 发明申请

US20120321873A1 NANOPOROUS POLYMERIC FOAM HAVING HIGH CELL DENSITY WITHOUT NANOFILLER 有权
标题翻译：具有无纳米纤维素的高密度聚合物的纳米聚合物泡沫
公开(公告)号：US20120321873A1
公开(公告)日：2012-12-20
申请号：US13578092
申请日：2011-02-23
申请人： Stephane Costeux , Lingbo Zhu , Hyun Jeon , Shana P. Bunker , Thomas H. Kalantar
发明人： Stephane Costeux , Lingbo Zhu , Hyun Jeon , Shana P. Bunker , Thomas H. Kalantar
IPC分类号： C08J9/02 , B29C44/08 , B29C47/00
CPC分类号： C08J9/122 , C08J9/0071 , C08J2201/024 , C08J2201/032 , C08J2205/046 , C08J2333/10
摘要： A polymeric foam has a thermoplastic polymer matrix defining multiple cells, the foam characterized by: (a) the polymer matrix having greater than 50 weight-percent copolymer containing at least two different monomers at least one of which is a methacrylate monomer, each monomer having a solubility parameter lower than 20 (megaPascals)0.5 and a chemical composition where twice the mass fraction of oxygen plus the mass fraction of nitrogen, fluorine and silicon is greater than 0.2; wherein the monomers comprise at least 90 weight-percent of all monomers in the copolymer; (b) at least one of the following: (i) a nucleation site density of at least 3×1014 effective nucleation sites per cubic centimeter of foamable polymer composition; (ii) an average cell size of 300 nanometer or less; (c) a porosity percentage greater than 30%; (d) an absence of nano-sized nucleating additive; and (e) a thickness of at least one millimeter.
摘要翻译：聚合物泡沫具有限定多个细胞的热塑性聚合物基质，泡沫的特征在于：（a）聚合物基质具有大于50重量％的共聚物，其含有至少两个不同的单体，其中至少一个是甲基丙烯酸酯单体，每个单体具有溶解度参数低于20（兆帕）和化学组成，其中氧质量分数加上氮，氟和硅质量分数的两倍大于0.2; 其中所述单体包含所述共聚物中所有单体的至少90重量％（b）以下至少之一：（i）成核位点密度为每立方厘米可发泡聚合物组合物至少3×1014个有效成核位点; （ii）平均泡孔尺寸为300纳米以下; （c）孔隙率大于30％; （d）不存在纳米尺寸的成核添加剂; 和（e）至少一毫米的厚度。

5. 发明授权

US07964663B2 Crack-resistant, flame retardant, halogen-free, cable assembly and coating composition 有权
标题翻译：耐裂纹，阻燃，无卤素，电缆组装和涂料组成
公开(公告)号：US07964663B2
公开(公告)日：2011-06-21
申请号：US12559796
申请日：2009-09-15
申请人： Yimsan Gau , Manuel F. Alsina , Paul D. Whaley , Shana P. Bunker
发明人： Yimsan Gau , Manuel F. Alsina , Paul D. Whaley , Shana P. Bunker
IPC分类号： C08L33/00 , C08K5/24
CPC分类号： C08L23/0869 , C08K3/013 , C08K3/22 , C08K5/0008 , C08L23/00 , C08L23/0846 , C08L23/0853 , C08L83/04 , H01B3/025 , H01B3/441 , H01B7/295 , C08L2666/02
摘要： Halogen-free, flame-retardant, crack-resistant, cable coatings are prepared from a composition comprising: A) 3 to 10 percent by weight of a low-melting temperature and medium to high grafted level maleic anhydride grafted polyethylene using a VLDPE base resin having density ranging from 0.86 to 0.91 g/cm3 and made with a single-site catalyst; B) 15 to 25% by weight of at least one EEA or EVA; C) 5 to 20% by weight of an α-olefin polymer; and D) 40 to 65% by weight of a flame retardant inorganic filler.
摘要翻译：无卤素，阻燃，抗裂纹，电缆涂层由以下组合物制备：A）3-10重量％的低熔点温度和中等至高接枝度的马来酸酐接枝聚乙烯，使用VLDPE基础树脂密度范围为0.86至0.91g / cm 3，并由单中心催化剂制成; B）15至25重量％的至少一种EEA或EVA; C）5〜20重量％的α-烯烃聚合物; 和D）40-65重量％的阻燃无机填料。

6. 发明申请

US20100101822A1 Stress/Thermal Cracking Resistant Cable Sheath Material 审中-公开
标题翻译：应力/耐热裂纹电缆护套材料
公开(公告)号：US20100101822A1
公开(公告)日：2010-04-29
申请号：US12529480
申请日：2008-02-20
申请人： Shana P. Bunker , Jeffrey M. Cogen , Suzanne Guerra
发明人： Shana P. Bunker , Jeffrey M. Cogen , Suzanne Guerra
IPC分类号： H01B3/30 , C08K5/101
CPC分类号： C08L51/00 , C08F255/02 , C08K3/016 , C08K3/22 , C08K3/26 , C08K3/38 , C08L23/08 , C08L23/0815 , C08L23/16 , C08L51/06 , C08L2205/02 , H01B7/295 , C08L2666/24 , C08L2666/06 , C08L2666/14 , C08L2666/04 , C08L2666/02
摘要： A composition useful as a wire or cable insulation or sheathing layer, the composition comprising (i) an inorganic flame retardant, e.g., aluminum trihydroxide (ATH), (ii) ethylene ethyl acetate (EEA) or ethylene butyl acrylate (EBA), (iii) a homogeneous polyethylene, (iv) an ethylenic resin modified with an organo-functional group, e.g., maleic anhydride (MAH) grafted polyethylene, (v) a silicone polymer, and optionally, (vi) a smoke suppressant. The insulation or sheathing layer comprising the composition of this invention exhibits good resistance to stress and/or thermal cracking.
摘要翻译：可用作电线或电缆绝缘或护套层的组合物，所述组合物包含（i）无机阻燃剂，例如三氢氧化铝（ATH），（ii）乙烯乙酸乙酯（EEA）或乙烯丙烯酸丁酯（EBA），（ iii）均匀的聚乙烯，（iv）用有机官能团改性的乙烯树脂，例如马来酸酐（MAH）接枝的聚乙烯，（v）硅氧烷聚合物，和任选的（vi）防烟剂。包含本发明组合物的绝缘层或护层显示出良好的耐应力和/或热裂纹性。

7. 发明申请

US20100069545A1 Crack-Resistant, Flame Retardant, Halogen-Free, Cable Assembly and Coating Composition 有权
标题翻译：耐破坏，阻燃，无卤素，电缆组件和涂料组成
公开(公告)号：US20100069545A1
公开(公告)日：2010-03-18
申请号：US12559796
申请日：2009-09-15
申请人： Yimsan Gau , Manuel F. Alsina , Paul D. Whaley , Shana P. Bunker
发明人： Yimsan Gau , Manuel F. Alsina , Paul D. Whaley , Shana P. Bunker
IPC分类号： C08K3/22 , C08L51/00 , C08K5/5415 , C08K5/09
CPC分类号： C08L23/0869 , C08K3/013 , C08K3/22 , C08K5/0008 , C08L23/00 , C08L23/0846 , C08L23/0853 , C08L83/04 , H01B3/025 , H01B3/441 , H01B7/295 , C08L2666/02
摘要： Halogen-free, flame-retardant, crack-resistant, cable coatings are prepared from a composition comprising: A) 3 to 10 percent by weight of a low-melting temperature and medium to high grafted level maleic anhydride grafted polyethylene using a VLDPE base resin having density ranging from 0.86 to 0.91 g/cm3 and made with a single-site catalyst; B) 15 to 25% by weight of at least one EEA or EVA; C) 5 to 20% by weight of an a-olefin polymer; and D) 40 to 65% by weight of a flame retardant inorganic filler.
摘要翻译：无卤素，阻燃，抗裂纹，电缆涂层由以下组合物制备：A）3-10重量％的低熔点温度和中等至高接枝度的马来酸酐接枝聚乙烯，使用VLDPE基础树脂密度范围为0.86至0.91g / cm 3，并由单中心催化剂制成; B）15至25重量％的至少一种EEA或EVA; C）5-20重量％的α-烯烃聚合物; 和D）40-65重量％的阻燃无机填料。

8. 发明申请

US20140200283A1 POLYMERIC NANOFOAM 审中-公开
标题翻译：聚合纳米粉体
公开(公告)号：US20140200283A1
公开(公告)日：2014-07-17
申请号：US14238746
申请日：2012-09-14
申请人： Stéphane Costeux , Shana P. Bunker , Hyun K. Jeon , Prasanna K. Jog
发明人： Stéphane Costeux , Shana P. Bunker , Hyun K. Jeon , Prasanna K. Jog
IPC分类号： C08L33/20 , C08L33/10
CPC分类号： C08L33/20 , B32B5/32 , C08J9/0061 , C08J9/122 , C08J2203/06 , C08J2333/06 , C08J2425/12 , C08J2455/02 , C08L33/10
摘要： A polymeric nanofoam has a continuous polymer phase containing at least one (meth)acrylic-free acrylonitrile-containing copolymer and at least one (meth)acrylic polymer where the concentration of (meth)acrylic polymer is in a range of 5-90 weight-percent of the total continuous polymer phase while the amount of methacrylic copolymer is 50 weight-percent or less of the total continuous polymer phase; the polymeric foam having a porosity of at least 50%, an absence of nano-sized nucleating additives and at least one of the following: (a) a number average cell size of 500 nanometers or less; and (b) an effective nucleation site density of at least 1×1014 sites per cubic centimeter of prefoamed material. The total weight of copolymerized acrylonitrile is in a range of 3-28 weight-percent based on total continuous polymer phase weight. At least one (meth)acrylic-free acrylonitrile-containing copolymer has a higher glass transition temperature than all of the (meth)acrylic polymers.
摘要翻译：聚合物纳米纤维具有包含至少一种（甲基）丙烯酸 - 丙烯腈共聚物和至少一种（甲基）丙烯酸类聚合物的连续聚合物相，其中（甲基）丙烯酸聚合物的浓度在5-90重量％的总连续聚合物相的百分比，而甲基丙烯酸共聚物的量为总连续聚合物相的50重量％或更少; 所述聚合物泡沫具有至少50％的孔隙率，不存在纳米尺寸的成核添加剂和以下至少一种：（a）500纳米或更小的数均孔数; 和（b）有效成核位点密度为每立方厘米预发泡材料至少1×1014个位点。基于总连续聚合物相重量，共聚丙烯腈的总重量在3-28重量％的范围内。至少一种（甲基）丙烯酸 - 含丙烯腈的共聚物具有比所有（甲基）丙烯酸聚合物更高的玻璃化转变温度。

9. 发明授权

US06646033B2 Pressure sensitive adhesives from plant oils 失效
标题翻译：来自植物油的压敏粘合剂
公开(公告)号：US06646033B2
公开(公告)日：2003-11-11
申请号：US10163220
申请日：2002-06-05
申请人： Richard P. Wool , Shana P. Bunker
发明人： Richard P. Wool , Shana P. Bunker
IPC分类号： C08K542
CPC分类号： C08K5/0008 , C08L33/06
摘要： A Pressure Sensitive Adhesive composition having low volatile organics content and low odor that is suitable for forming pressure sensitive adhesives containing an aqueous dispersion containing a blended mixture of: (a) a polymer obtained by the polymerization of (i) an internally plasticizing and cross-linkable long chain methyl ester having at least one double bond in said methyl ester chain; and (ii) one or more unsaturated monomers copolymerizable therewith; and (b) a surface-active agent.
摘要翻译：一种具有低挥发性有机物含量和低气味的压敏粘合剂组合物，其适用于形成含有含有以下混合混合物的混合混合物的水分散体的压敏粘合剂：（a）通过聚合获得的聚合反应获得的聚合反应（i）内部增塑和交联，在所述甲基酯链中具有至少一个双键的可连接的长链甲基酯; 和（ii）可与其共聚的一种或多种不饱和单体; 和（b）表面活性剂。

10. 发明申请

US20170002162A1 NANOCELLULAR FOAM WITH SOLID FLAME RETARDANT 有权
标题翻译：具有固体阻燃剂的纳米泡沫
公开(公告)号：US20170002162A1
公开(公告)日：2017-01-05
申请号：US15109935
申请日：2015-03-18
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： Liang Chen , Anne M. Kelly-Rowley , Shana P. Bunker , Stéphane Costeux
IPC分类号： C08J9/00 , C08J9/12
CPC分类号： C08J9/0038 , C08J3/215 , C08J3/226 , C08J9/0004 , C08J9/0061 , C08J9/122 , C08J2201/024 , C08J2201/032 , C08J2203/06 , C08J2203/08 , C08J2205/042 , C08J2205/044 , C08J2333/12 , C08J2433/12
摘要： Prepare nanofoam by (a) providing an aqueous solution of a flame retardant dissolved in an aqueous solvent, wherein the flame retardant is a solid at 23° C. and 101 kiloPascals pressure when in neat form; (b) providing a fluid polymer composition selected from a solution of polymer dissolved in a water-miscible solvent or a latex of polymer particles in a continuous aqueous phase; (c) mixing the aqueous solution of flame retardant with the fluid polymer composition to form a mixture; (d) removing water and, if present, solvent from the mixture to produce a polymeric composition having less than 74 weight-percent flame retardant based on total polymeric composition weight; (e) compound the polymeric composition with a matrix polymer to form a matrix polymer composition; and (f) foam the matrix polymer composition into nanofoam having a porosity of at least 60 percent.
摘要翻译：通过（a）提供溶解在水性溶剂中的阻燃剂的水溶液来制备纳米纤维，其中阻燃剂在23℃为固体，并且在整齐的形式下为101千帕斯卡压力; （b）提供流体聚合物组合物，其选自溶解在水混溶性溶剂中的聚合物溶液或在连续水相中的聚合物颗粒的胶乳; （c）将阻燃剂的水溶液与流体聚合物组合物混合以形成混合物; （d）从混合物中除去水和溶剂（如果存在），以产生基于总聚合物组合物重量具有小于74重量％阻燃剂的聚合物组合物; （e）将聚合物组合物与基质聚合物复合以形成基质聚合物组合物; 和（f）将基质聚合物组合物发泡成具有至少60％的孔隙率的纳米电
雾。

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