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1. 发明申请

WO2021128126A1 ALPHA-OLEFIN INTERPOLYMERS WITH IMPROVED MOLECULAR DESIGN FOR PHOTOVOLTAIC ENCAPSULANTS 审中-公开
公开(公告)号：WO2021128126A1
公开(公告)日：2021-07-01
申请号：PCT/CN2019/128574
申请日：2019-12-26
申请人： DOW GLOBAL TECHNOLOGIES LLC , WU, Gaoxiang , HABERSBERGER, Brian M. , DELORBE, Johnathan E. , KARJALA, Thomas W. , SUN, Yabin , CONG, Rongjuan
发明人： WU, Gaoxiang , HABERSBERGER, Brian M. , DELORBE, Johnathan E. , KARJALA, Thomas W. , SUN, Yabin , CONG, Rongjuan
IPC分类号： C08L23/20 , C08F210/14 , C08K5/14 , C08K5/54 , H01L31/042 , C08F210/16 , C08F4/659 , C08F4/65908 , C08F4/65912 , C08J2323/08 , C08J5/18 , C08K5/0025 , C08K5/34924 , C08K5/5425 , H01L31/0481
摘要： A composition comprising an ethylene/alpha-olefin interpolymer that comprises the following properties: a) a total unsaturation/1000C ≥ 0.30; b) a molecular weight distribution (MWD) ≤ 3.0; c) a TGIC broadness parameter B 1/4 ≤ 8.0. A solution polymerization process to prepare an ethylene/alpha-olefin/interpolymer; said process comprising polymerizing, in one reactor, at a reactor temperature ≥ 150℃, a reaction mixture comprising ethylene, an alpha-olefin, a solvent, and a metal complex as described herein. A method to determine the TGIC broadness parameter B 1/x of a polymer composition comprising one or more olefin-based polymers.

2. 发明申请

WO2021133640A1 ALPHA-OLEFIN INTERPOLYMERS WITH IMPROVED MOLECULAR DESIGN FOR PHOTOVOLTAIC ENCAPSULANTS 审中-公开
公开(公告)号：WO2021133640A1
公开(公告)日：2021-07-01
申请号：PCT/US2020/065761
申请日：2020-12-17
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： WU, Gaoxiang , HABERSBERGER, Brian M. , DELORBE, Johnathan E. , KARJALA, Thomas W. , SUN, Yabin , CONG, Rongjuan
IPC分类号： C08F210/16 , C08J5/18 , H01L31/00 , C08F4/659 , C08F4/65908 , C08F4/65912 , C08J2323/08 , C08K5/0025 , C08K5/14 , C08K5/34924 , C08K5/5425 , H01L31/0481
摘要： A composition comprising an ethylene/alpha-olefin interpolymer that comprises the following properties: a) a total unsaturation/1000C ≥ 0.30; b) a molecular weight distribution (MWD) ≤ 3.0; c) a TGIC broadness parameter B1/4 ≤ 8.0. A solution polymerization process to prepare an ethylene/alpha-olefin/interpolymer; said process comprising polymerizing, in one reactor, at a reactor temperature ≥ 150°C, a reaction mixture comprising ethylene, an alpha-olefin, a solvent, and a metal complex as described herein. A method to determine the TGIC broadness parameter B1/x of a polymer composition comprising one or more olefin-based polymers.

3. 发明申请

WO2016028957A1 NUCLEATION WITH A BLOCK COMPOSITE NUCLEATOR 审中-公开
标题翻译：具有块状复合核的核
公开(公告)号：WO2016028957A1
公开(公告)日：2016-02-25
申请号：PCT/US2015/046002
申请日：2015-08-20
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： JIN, Yi , WALTON, Kim L. , HUGHES, Morgan M. , KARJALA, Thomas W. , CHOPIN III, Lamy J. , LEE, Dean , CONG, Rongjuan
IPC分类号： C08L23/14
CPC分类号： C08L23/16 , C08L23/142 , C08L2205/025 , C08L2205/035 , C08L2205/24 , C08L53/00
摘要： A composition includes (A) 30-95 wt% of a random or homogeneous propylene-based interpolymer having: (i) a comonomer content of at least one of C 2 and C 4-10 α-olefins of 7 wt% to 49 wt% based on the total weight of the propylene-based interpolymer, (ii) a density of 0.90 g/cc or less, and (iii) an MFR of 1 g/10 min or greater (230°C/2.16 kg); and (B) 5-70 wt% of a block composite nucleator comprising: (1) a first polymer that includes polypropylene; (2) a second polymer that includes an alpha-olefin based polymer, the alpha-olefin being selected from at least one of a C 2 and C 4-10 α-olefins, and (3) a block copolymer having a first segment and a second segment, the first segment of the block copolymer having the same composition as the first polymer in the block composite nucleator and the second segment of the block copolymer having the same composition as the second polymer of the block composite nucleator.
摘要翻译：组合物包括（A）30-95重量％的无规或均相丙烯基互聚物，其具有：（i）C 2和C 4 -10α-烯烃中的至少一种的共聚单体含量为7重量％至49重量％（ii）密度为0.90g / cc以下，（iii）MFR为1g / 10分钟以上（230℃/ 2.16kg）的丙烯系共聚体的总重量; 和（B）5-70重量％的嵌段复合成核剂，其包含：（1）包含聚丙烯的第一聚合物; （2）包含α-烯烃基聚合物的第二聚合物，所述α-烯烃选自C 2和C 4 -10α-烯烃中的至少一种，和（3）具有第一链段和第二链段的嵌段共聚物嵌段共聚物的第一段具有与嵌段复合成核剂中的第一聚合物相同的组成，第二嵌段共聚物的嵌段共聚物的第二嵌段具有与嵌段复合成核剂的第二聚合物相同的组成。

4. 发明申请

WO2013096573A1 ETHYLENE/ALPHA-OLEFIN/NONCONJUGATED POLYENE INTERPOLYMERS AND PROCESSES TO FORM THE SAME 审中-公开
标题翻译：乙烯/丙烯腈/非共轭多烯聚合物嵌段共聚物及其形成方法
公开(公告)号：WO2013096573A1
公开(公告)日：2013-06-27
申请号：PCT/US2012/070859
申请日：2012-12-20
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： LIPISHAN, Colin , KARJALA, Thomas W. , SMITH, Michael L. , SPENCER, Liam P. , KLOSIN, Jerzy
IPC分类号： C08F210/18
CPC分类号： C08F210/18 , C08F4/65908 , C08F4/65912 , C08F4/64193 , C08F2/06 , C08F210/16 , C08F236/20 , C08F2500/03 , C08F2500/17 , C08F2500/25
摘要： The invention provides a solution polymerization process to form an ethylene/α-olefin/nonconjugated polyene interpolymer, said process comprising polymerizing ethylene, an α-olefin, and a nonconjugated polyene in at least one reactor in the presence of a catalyst selected from Formula I, as described herein; and wherein the polymerization is conducted in a continuous process; and wherein the interpolymer has a rheology ratio (V0.1/V100 at 19°C) greater than, or equal to, 20.
摘要翻译：本发明提供了形成乙烯/α-烯烃/非共轭多烯互聚物的溶液聚合方法，所述方法包括在选自式I的催化剂存在下，在至少一个反应器中聚合乙烯，α-烯烃和非共轭多烯，如本文所述; 并且其中所述聚合在连续方法中进行; 并且其中所述互聚物具有大于或等于20的流变比（在19℃下为V0.1 / V100）。

5. 发明申请

WO2016154188A1 Process of Adding a Chain Shuttling Agent 审中-公开
标题翻译：添加链式穿梭剂的方法
公开(公告)号：WO2016154188A1
公开(公告)日：2016-09-29
申请号：PCT/US2016/023553
申请日：2016-03-22
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： KARJALA, Thomas W. , FAILS, Brandon , VELDMAN, Jacob , HYPOLITE, Curvel , CRIM, James, B. , CASTELLUCCIO, Anthony, J. , SLUIJTS, Ludovicus, JC , JAIN, Pradeep
IPC分类号： C08F210/16 , C08F297/08 , C08F2/00
CPC分类号： C08F2/38 , C08F2/001 , C08F210/06 , C08F210/16 , C08F297/08 , C08F297/083
摘要： A process to form a block copolymer comprising two or more regions or segments of differentiated polymer composition or properties, including feeding a first mixture that includes a chain shuttling agent, a solvent, the one or more monomers, and optionally hydrogen into a first reactor or reactor zone, feeding a second mixture that includes at least one olefin polymerization catalyst and at least one cocatalyst into the first reactor or reactor zone, contacting the first mixture and the second mixture under polymerization conditions in the first reactor or reactor zone to form a reaction mixture that is characterized by the formation of polymer chains from the monomers, allowing polymerization to occur in the first reactor or reactor zone and/or a second reactor or reactor zone to form polymer chains that are differentiated from the polymer chains, such that the resultant polymer has two or more chemically or physically distinguishable blocks.
摘要翻译：形成嵌段共聚物的方法，其包含两个或多个分化聚合物组合物或性质的区域或区段，包括将包含链穿梭剂，溶剂，一种或多种单体和任选的氢的第一混合物进料至第一反应器或将包含至少一种烯烃聚合催化剂和至少一种助催化剂的第二混合物进料到第一反应器或反应器区中，在第一反应器或反应器区中在聚合条件下使第一混合物和第二混合物接触以形成反应区其特征在于从单体形成聚合物链，允许聚合在第一反应器或反应器区和/或第二反应器或反应器区中发生，以形成与聚合物链不同的聚合物链，使得所得物聚合物具有两个或多个化学或物理上可区分的嵌段。

6. 发明申请

WO2016109264A1 PROCESS TO FORM ETHYLENE/ALPHA-OLEFIN INTERPOLYMERS 审中-公开
标题翻译：形成乙烯/丙烯酰胺嵌段共聚物的方法
公开(公告)号：WO2016109264A1
公开(公告)日：2016-07-07
申请号：PCT/US2015/066848
申请日：2015-12-18
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： KARJALA, Thomas W. , RUBALCABA, Jorge , MADENJIAN, Edward O. , HYPOLITE, Curvel , JAIN, Pradeep
IPC分类号： C08F2/00 , C08L23/08
CPC分类号： C08L23/0815 , B01J19/18 , B01J19/2455 , C08L2205/025 , C08L2308/00 , C08F210/18 , C08F2/001 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/03 , C08F2500/17 , C08F2/06
摘要： The invention provides a process to form a "first composition comprising a first ethylene/α-olefin interpolymer and a second ethylene/α-olefin interpolymer," said process comprising polymerizing a first mixture comprising ethylene, an α-olefin, and optionally a polyene, in a stirred tank reactor to form a first ethylene/α-olefin interpolymer, and transferring at least some of the first ethylene/α-olefin interpolymer to a loop reactor, and polymerizing, therein, a second mixture comprising ethylene, an alpha-olefin, and optionally a polyene, in the presence of the first ethylene/α-olefin interpolymer, to form the "first composition comprising the first ethylene/α-olefin interpolymer and the second ethylene/α-olefin interpolymer." The invention also provides a polymerization reactor configuration comprising at least the following: a stirred tank reactor followed by a loop reactor.
摘要翻译：本发明提供了一种形成“第一组合物的方法，该组合物包含第一乙烯/α-烯烃互聚物和第二乙烯/α-烯烃互聚物”，所述方法包括聚合包含乙烯，α-烯烃和任选的多烯在搅拌釜反应器中形成第一乙烯/α-烯烃互聚物，并将至少一些第一乙烯/α-烯烃互聚物转移到环管反应器中，并在其中聚合第二混合物，其包含乙烯，烯烃和任选的多烯，在第一种乙烯/α-烯烃互聚物的存在下，形成“包含第一乙烯/α-烯烃互聚物和第二乙烯/α-烯烃互聚物的第一组合物”。本发明还提供了至少包括以下的聚合反应器构型：搅拌釜反应器，随后是环流反应器。

7. 发明公开

EP4081560A1 ALPHA-OLEFIN INTERPOLYMERS WITH IMPROVED MOLECULAR DESIGN FOR PHOTOVOLTAIC ENCAPSULANTS 审中-实审
公开(公告)号：EP4081560A1
公开(公告)日：2022-11-02
申请号：EP20848817.1
申请日：2020-12-17
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： WU, Gaoxiang , HABERSBERGER, Brian M. , DELORBE, Johnathan E. , KARJALA, Thomas W. , SUN, Yabin , CONG, Rongjuan
IPC分类号： C08F210/16 , C08J5/18 , H01L31/00 , C08F4/659

8. 发明授权

EP3274382B1 PROCESS OF ADDING A CHAIN SHUTTLING AGENT 有权
公开(公告)号：EP3274382B1
公开(公告)日：2019-10-30
申请号：EP16714155.5
申请日：2016-03-22
申请人： Dow Global Technologies LLC
发明人： KARJALA, Thomas W. , FAILS, Brandon , VELDMAN, Jacob , HYPOLITE, Curvel , CRIM, James, B. , CASTELLUCCIO, Anthony, J. , SLUIJTS, Ludovicus, JC , JAIN, Pradeep
IPC分类号： C08F210/16 , C08F297/08 , C08F2/00 , C08F2/38

9. 发明授权

EP3240808B1 PROCESS TO FORM ETHYLENE/ALPHA-OLEFIN INTERPOLYMERS 有权
公开(公告)号：EP3240808B1
公开(公告)日：2020-05-13
申请号：EP15831102.7
申请日：2015-12-18
申请人： Dow Global Technologies LLC
发明人： KARJALA, Thomas W. , RUBALCABA, Jorge , MADENJIAN, Edward O. , HYPOLITE, Curvel , JAIN, Pradeep
IPC分类号： C08F2/00 , C08L23/08

10. 发明公开

EP3240808A1 PROCESS TO FORM ETHYLENE/ALPHA-OLEFIN INTERPOLYMERS 有权
公开(公告)号：EP3240808A1
公开(公告)日：2017-11-08
申请号：EP15831102.7
申请日：2015-12-18
申请人： Dow Global Technologies LLC
发明人： KARJALA, Thomas W. , RUBALCABA, Jorge , MADENJIAN, Edward O. , HYPOLITE, Curvel , JAIN, Pradeep
IPC分类号： C08F2/00 , C08L23/08
摘要： The invention provides a process to form a “first composition comprising a first ethylene/α-olefin interpolymer and a second ethylene/α-olefin interpolymer,” said process comprising polymerizing a first mixture comprising ethylene, an α-olefin, and optionally a polyene, in a stirred tank reactor to form a first ethylene/α-olefin interpolymer, and transferring at least some of the first ethylene/α-olefin interpolymer to a loop reactor, and polymerizing, therein, a second mixture comprising ethylene, an alpha-olefin, and optionally a polyene, in the presence of the first ethylene/α-olefin interpolymer, to form the “first composition comprising the first ethylene/α-olefin interpolymer and the second ethylene/α-olefin interpolymer.” The invention also provides a polymerization reactor configuration comprising at least the following: a stirred tank reactor followed by a loop reactor.

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