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1. 发明申请

WO2011011142A3 METHOD AND MATERIALS FOR REVERSE PATTERNING 审中-公开
标题翻译：反向图案的方法和材料
公开(公告)号：WO2011011142A3
公开(公告)日：2011-04-21
申请号：PCT/US2010039415
申请日：2010-06-22
申请人： DOW CORNING , BRADFORD MICHAEL L , MOYER ERIC SCOTT , TAKEUCHI KASUMI , WANG SHENG , YEAKLE CRAIG
发明人： BRADFORD MICHAEL L , MOYER ERIC SCOTT , TAKEUCHI KASUMI , WANG SHENG , YEAKLE CRAIG
IPC分类号： C08G77/18 , C08L83/04 , C09D183/04 , G03F7/075 , G03F7/20
CPC分类号： C08G77/18 , C08L83/04 , C09D183/04 , H01L21/02137 , H01L21/02282 , H01L21/0337
摘要： A silsesquioxane resin is applied on top of the patterned photo-resist and cured to produce a cured silsesquioxane resin on top of the pattern surface. Subsequently, an aqueous base stripper or a reactive ion etch recipe containing CF4 is used to "etch back" the silicon resin to the top of the photoresist material, exposing the entire top surface of the photoresist. Then, a second reactive ion etch recipe containing O2 to etch away the photoresist. The result is a silicon resin film with via holes with the size and shape of the post that were patterned into the photoresist. Optionally, the new pattern can be transferred into the underlying layer(s).
摘要翻译：将一倍半硅氧烷树脂施加在图案化的光致抗蚀剂的顶部并固化，以在图案表面的顶部上产生固化的倍半硅氧烷树脂。随后，使用包含CF 4的水性碱性剥离剂或反应性离子蚀刻配方将硅树脂“回蚀”到光致抗蚀剂材料的顶部，暴露光致抗蚀剂的整个顶表面。然后，第二反应离子蚀刻配方含有O 2以蚀刻掉光致抗蚀剂。结果是具有图案化为光致抗蚀剂的柱的尺寸和形状的通孔的硅树脂膜。可选地，新图案可以被转移到下层中。

2. 发明申请

WO2005054371A3 ADDITION-CURABLE ORGANOPOLYSILOXANE RESIN COMPOSITION AND AN OPTICAL MATERIAL 审中-公开
标题翻译：可加固化的有机聚硅氧烷树脂组合物和光学材料
公开(公告)号：WO2005054371A3
公开(公告)日：2005-08-11
申请号：PCT/JP2004018093
申请日：2004-11-29
申请人： DOW CORNING TORAY SILICONE , DOW CORNING ASIA LTD , YOSHITAKE MAKOTO , NAKANISHI KOJI , NAKASHIMA HISATAKA , KOBAYASHI HIDEKI , MURAKAMI MASASHI , TAKEUCHI KASUMI
发明人： YOSHITAKE MAKOTO , NAKANISHI KOJI , NAKASHIMA HISATAKA , KOBAYASHI HIDEKI , MURAKAMI MASASHI , TAKEUCHI KASUMI
IPC分类号： G02B1/04 , C08L83/04 , C08L83/05 , C08L83/07
CPC分类号： C08L83/04 , C08G77/045 , C08G77/12 , C08G77/20 , C08G77/70 , C08L83/00
摘要： An addition-curable organopolysiloxane resin composition having, in a state of cued body, a hardness of 60 to 100 at 25 degree C and 40 to 100 at 150 degree C as measued in accordance with the provisions of ASTM D2240-86, said composition comprising: (A) 100 parts by weight of an organopolysiloxane resin comprised of at least alkenyl groups and phenyl groups; (B) 10 to 50 parts by weight of an organooligosiloxane comprised of at least alkeyl groups and phenyl groups; (C) 20 to 100 parts by weight of an organohydrogenoligosiloxane or organohydrogenpolysiloxane; and (D) an addition-reaction catalyst in a catalytic quantity; an optical material that is comprised of a cured body producted from aforementioned components (A), (B), and (C) and posseses the aforementioned characteristics.
摘要翻译：根据ASTM D2240-86的规定测量，加热固化的有机聚硅氧烷树脂组合物具有在固体状态下在25℃和150℃下硬度为60至100，所述组合物包含：（A）100重量份由至少烯基和苯基组成的有机聚硅氧烷树脂; （B）10-50重量份至少包含烯基和苯基的有机低聚硅氧烷; （C）20至100重量份的有机氢低聚硅氧烷或有机氢聚硅氧烷; 和（D）催化量的加成反应催化剂; （A），（B）和（C）制造的具有上述特征的固化体构成的光学材料。

3. 发明申请

WO2005062080A3 ADDITION-CURABLE ORGANOPOLYSILOXANE RESIN COMPOSITION 审中-公开
标题翻译：添加可固化的有机硅氧烷树脂组合物
公开(公告)号：WO2005062080A3
公开(公告)日：2006-03-02
申请号：PCT/JP2004019469
申请日：2004-12-17
申请人： DOW CORNING TORAY CO LTD , YOSHITAKE MAKOTO , NAKANISHI KOJI , MURAKAMI MASASHI , TAKEUCHI KASUMI
发明人： YOSHITAKE MAKOTO , NAKANISHI KOJI , MURAKAMI MASASHI , TAKEUCHI KASUMI
IPC分类号： C08L83/04 , C08L83/05 , C08L83/07 , G02B1/04
CPC分类号： G02B1/04 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/70 , C08L83/04 , C08L83/00
摘要： Addition-curable organopolysiloxane resin composition comprising an organopolysiloxane resin that contains at least alkenyl, hydroxyl, and phenyl directly bonded to silicon of which at least 30 mole% is phenyl; an organohydrogenoligosiloxane or organohydrogenpolysiloxane that contains at least phenyl directly bonded to silicon of which at least 20 mole% is phenyl; and an addition reaction-curing catalyst.
摘要翻译：包含有机聚硅氧烷树脂的可加成固化的有机聚硅氧烷树脂组合物，其至少含有至少30摩尔％为苯基的硅的键合，羟基和苯基; 至少包含至少20摩尔％的苯的直接键合至苯基的有机氢氢化二硅氧烷或有机氢聚硅氧烷; 和加成反应固化催化剂。

4. 发明专利

JP2005171069A Active energy ray-curable organopolysiloxane resin composition, optical transmission member and method for producing the optical transmission member 有权
标题翻译：活性能量可变光固化有机硅氧烷树脂组合物，光传输部件及其制造光传输部件的方法
公开(公告)号：JP2005171069A
公开(公告)日：2005-06-30
申请号：JP2003412452
申请日：2003-12-10
申请人： Dow Corning Asia Ltd , Dow Corning Corp , Dow Corning Toray Silicone Co Ltd , ダウコーニングアジア株式会社 , ダウコーニングコーポレーション , 東レ・ダウコーニング・シリコーン株式会社
发明人： WATANABE TOSHINORI , OGAWA TAKUYA , TAKEUCHI KASUMI , YOSHITAKE MAKOTO , GLOVER O SHEDRIC , TOMALIA MARY KAY
IPC分类号： G02B6/12 , C08G77/14 , C08K5/00 , C08L83/06 , C09D183/06 , G02B6/13
CPC分类号： C08L83/06 , C08L2666/28
摘要： PROBLEM TO BE SOLVED: To provide an active energy ray-curable organopolysiloxane resin composition quickly curable by active energy ray irradiation and giving a cured product that is excellent in form retention and solvent resistance, high in light transmittance over communication wavelength band and slight in the change of its light transmittance and refractive index even if exposed to high temperatures. SOLUTION: The active energy ray-curable organopolysiloxane resin composition comprises (A) 100 pts. wt. of an epoxy group-containing organopolysiloxane resin represented by the siloxane unit formula: (R 1 R 2 R 3 SiO 1/2 ) a (R 4 R 5 SiO 2/2 ) b (R 6 SiO 3/2 ) c (SiO 4/2 ) d ( wherein, R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are each an organic group selected from 1-6C monovalent aliphatic hydrocarbon group, 6-10C monovalent aromatic hydrocarbon group and epoxy group-containing monovalent hydrocarbon group; the siloxane units each having the epoxy group-containing monovalent hydrocarbon group accounts for 2-50 mol%; 15 mol% or greater of the total organic group is the monovalent aromatic hydrocarbon groups; (a+b+c+d)=1, 0≤a COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供通过活性能量射线照射快速固化的活性能量射线固化型有机聚硅氧烷树脂组合物，得到形状保持性和耐溶剂性优异的固化物，通信波长带的透光率高，即使暴露在高温下，其透光率和折射率的变化也会轻微。解决方案：活性能量射线固化型有机聚硅氧烷树脂组合物包含（A）100个。重量。由硅氧烷单元式表示的含环氧基的有机聚硅氧烷树脂：（R 1 SP＆lt; SP＆gt; 2＆lt; SP＆gt; 3＆lt; SP＆gt; ）一（R 4 - [R 5 的SiO 2/2 ） b'/ SB>（R 6 的SiO 3/2 ） C （SIO 4/2 ）ð< / SB>（其中，R 1 ，R 2 ，R 3， 5＆lt; SP＆gt;和＆lt; SP＆gt; 6＆lt; SP＆gt;各自是选自1-6C一价脂族烃基，6-10C一价芳族烃基和含环氧基的一价烃基的有机基团;每个硅氧烷单元含有环氧基的一价烃基占2-50摩尔％;总有机基团的15摩尔％以上为一价芳香族烃基;（a + b + c + d）= 1,0

5. 发明专利

JP2005162859A Addition reaction curing type organopolysiloxane resin composition and optical member 审中-公开
标题翻译：添加反应固化型有机聚硅氧烷树脂组合物和光学成员
公开(公告)号：JP2005162859A
公开(公告)日：2005-06-23
申请号：JP2003402810
申请日：2003-12-02
申请人： Dow Corning Asia Ltd , Dow Corning Toray Silicone Co Ltd , ダウコーニングアジア株式会社 , 東レ・ダウコーニング・シリコーン株式会社
发明人： YOSHITAKE MAKOTO , NAKANISHI KOJI , NAKAJIMA HISATAKA , KOBAYASHI HIDEKI , MURAKAMI MASASHI , TAKEUCHI KASUMI
IPC分类号： G02B1/04 , C08L83/04 , C08L83/05 , C08L83/07
CPC分类号： C08L83/04 , C08G77/045 , C08G77/12 , C08G77/20 , C08G77/70 , C08L83/00
摘要： PROBLEM TO BE SOLVED: To obtain an addition reaction curing type organopolysiloxane resin composition that has excellent fluidity, moldability, provides a cured material having small reduction in hardness at a high temperature in spite of having transparency, high hardness and high strengths, and to provide an optical mumber having these properties. SOLUTION: The addition reaction curing type organopolysiloxane resin composition comprises (A) 100 pts. wt. of an organopolysiloxane resin having ≥3,000 weight-average molecular weight and containing at least an alkenyl group and phenyl group, (B) 10-50 pts. wt. of an organopolysiloxane containing an alkenyl group and phenyl group, (C) 20-100 pts. wt. of an organohydrogen oligosiloxane or organohydrogen polysiloxane and (D) a catalytic amount of an addition reaction curing catalyst, and provides a cured material having 60-100 hardness by type D durometer of ASTM standard D2240-86 at 25°C and 40-100 at 150°C. The optical member having the above properties is an addition reaction cured material of the components (A), (B) and (C). COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：待解决的问题为了获得具有优异的流动性，成型性的加成反应固化型有机基聚硅氧烷树脂组合物，尽管具有透明性，高硬度和高强度，但提供了在高温下硬度降低小的固化材料，并提供具有这些性质的光学模板。解决方案：加成反应固化型有机聚硅氧烷树脂组合物包含（A）100个。重量。的具有≥3,000重均分子量并且至少含有烯基和苯基的有机聚硅氧烷树脂，（B）10-50个点。重量。的含有烯基和苯基的有机聚硅氧烷，（C）20-100个。重量。的有机氢低聚硅氧烷或有机氢聚硅氧烷和（D）催化量的加成反应固化催化剂，并且通过ASTM标准D2240-86的D型硬度在25℃和40-100℃下提供具有60-100硬度的固化材料 150℃。具有上述性质的光学部件是组分（A），（B）和（C）的加成反应固化材料。版权所有（C）2005，JPO＆NCIPI

6. 发明专利

JP2005163009A (meth)acryloxy group-containing organopolysiloxane resin, high-energy beam curable organopolysiloxane resin composition, optical transmission member, and method for producing the optical transmission member 审中-公开
标题翻译：（METH）含丙烯酸基团的有机聚硅氧烷树脂，高能量光束可固化的有机聚硅氧烷树脂组合物，光传输部件和用于生产光传输部件的方法
公开(公告)号：JP2005163009A
公开(公告)日：2005-06-23
申请号：JP2004178042
申请日：2004-06-16
申请人： Dow Corning Asia Ltd , Dow Corning Toray Co Ltd , ダウコーニングアジア株式会社 , 東レ・ダウコーニング株式会社
发明人： WATANABE TOSHINORI , OGAWA TAKUYA , TAKEUCHI KASUMI , YOSHITAKE MAKOTO
IPC分类号： G03F7/027 , C08G77/20 , G02B6/12 , G02B6/13 , G03F7/075
摘要： PROBLEM TO BE SOLVED: To obtain a high-energy beam curable organopolysiloxane resin composition capable of being rapidly cured by irradiation of a high-energy beam and capable of giving a cured product having high light transmittance in a communication wavelength range, to obtain an organopolysiloxane resin used for the composition, to provide an optical transmission member formed of the cured product having the high light transmittance in the communication wavelength range, and to provide a method for simply, rapidly and efficiently producing the optical transmission member. SOLUTION: The organopolysiloxane resin contains (meth)acryloxy groups and aromatic groups. The high-energy beam curable organopolysiloxane resin composition (which is, for example, cured by ultraviolet light) comprises the organopolysiloxane resin containing the (meth)acryloxy groups and the aromatic groups, a photopolymerization catalyst, and if necessary, an organic solvent. The optical transmission member is formed of the cured product which is given by irradiating the organopolysiloxane resin with the high-energy beam in the coexistence of the photopolymerization catalyst. The method for producing the optical transmission member comprises coating a base material with the composition and irradiating the coated material with the high-energy beam. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决的问题为了获得能够通过照射高能束快速固化并且能够在通信波长范围内给出具有高透光率的固化产物的高能量可光束固化的有机聚硅氧烷树脂组合物，得到用于该组合物的有机聚硅氧烷树脂，以提供由在通信波长范围内具有高透光率的固化产物形成的光传输部件，并提供简单，快速且有效地制造光传输部件的方法。解决方案：有机聚硅氧烷树脂含有（甲基）丙烯酰氧基和芳族基团。高能量束固化型有机聚硅氧烷树脂组合物（例如通过紫外线固化）包含含有（甲基）丙烯酰氧基和芳香族基团的有机聚硅氧烷树脂，光聚合催化剂，根据需要含有有机溶剂。光传输部件由固化产物形成，其通过在光聚合催化剂的共存下用高能束照射有机聚硅氧烷树脂而得到。制造光传输部件的方法包括用该组合物涂覆基材并用高能束照射涂覆材料。版权所有（C）2005，JPO＆NCIPI

7. 发明专利

JP2005179541A Addition reaction-curable type organopolysiloxane resin composition 有权
标题翻译：添加反应固化型有机聚硅氧烷树脂组合物
公开(公告)号：JP2005179541A
公开(公告)日：2005-07-07
申请号：JP2003423726
申请日：2003-12-19
申请人： Dow Corning Asia Ltd , Dow Corning Toray Silicone Co Ltd , ダウコーニングアジア株式会社 , 東レ・ダウコーニング・シリコーン株式会社
发明人： YOSHITAKE MAKOTO , NAKANISHI KOJI , MURAKAMI MASASHI , TAKEUCHI KASUMI
IPC分类号： C08L83/04 , C08L83/05 , C08L83/07 , G02B1/04
CPC分类号： G02B1/04 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/70 , C08L83/04 , C08L83/00
摘要： PROBLEM TO BE SOLVED: To provide an addition reaction-curable type organopolysiloxane resin composition having excellent fluidity and moldability, providing a cured product having transparency, high hardness and high strength, and hardly becoming cloudy even after heated in high humidity, especially the addition reaction-curable type organopolysiloxane resin composition providing the cured product having the high hardness and the high strength even having SOLUTION: The addition reaction-curable type organopolysiloxane resin composition comprises (A) 100 pts. wt. organopolysiloxane resin at least having an alkenyl group, a hydroxy group and a phenyl group, (B) 20-100 pts. wt. organohydrogenoligosiloxane or organohydrogenpolysiloxane at least having the phenyl group, and (C) a catalytic amount of a catalyst for curing by an addition reaction. The cured product has 60-100 hardness measured by a type D durometer, and the reduction rate of transmittance of 850 nm light after leaving the cured product in an atmosphere of 85 %RH and 85°C for 15 hr and further leaving the resultant cured product in an atmosphere of 25 %RH and 25°C for ≤6 hr after taking out into the condition from the initial transmittance is ≤10%. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决问题：提供具有优异的流动性和成型性的加成反应固化型有机聚硅氧烷树脂组合物，提供具有透明性，高硬度和高强度的固化产物，甚至在高湿度下加热后也几乎不变浑浊，特别是该加成反应固化型有机聚硅氧烷树脂组合物即使具有<1Pa·s的粘度，也提供具有高硬度和高强度的固化产物。解决方案：加成反应固化型有机聚硅氧烷树脂组合物包含（A）100个。重量。至少具有烯基，羟基和苯基的有机聚硅氧烷树脂，（B）20-100重量份。重量。至少具有苯基的有机氢羟基二硅氧烷或有机氢聚硅氧烷，和（C）催化量的通过加成反应固化的催化剂。固化产物具有通过D型硬度计测量的60-100硬度，并且在85％RH和85℃的气氛中将固化产物离开固化产物15小时后的850nm光的透射率的还原率，并进一步留下所得固化在25％RH和25℃的气氛中，从初始透射率进入条件后≤6小时的产品≤10％。版权所有（C）2005，JPO＆NCIPI

8. 发明专利

JPH1010741A ULTRAVIOLET-CURING POLYSILOXANE COMPOSITION AND PRODUCTION OF CURED SUBSTANCE PATTERN USING SAME 失效
公开(公告)号：JPH1010741A
公开(公告)日：1998-01-16
申请号：JP16748896
申请日：1996-06-27
申请人： DOW CORNING ASIA KK
发明人： TACHIKAWA MAMORU , BRIAN ROBERT HARKNESS , TAKEUCHI KASUMI
IPC分类号： G03F7/004 , C08F2/46 , C08K5/07 , C08K5/20 , C08L83/04 , C08L83/07 , C09D183/04 , G03F7/029 , G03F7/075 , H01L21/027 , H01L21/312
摘要： PROBLEM TO BE SOLVED: To prevent the blocking of curing by air or oxygen, to attain efficient curing by slight irradiation with UV and to obtain a cured substance pattern having superior heat resistance by heat treatment after pattern formation by using a specified material generating a free radical under the action of UV. SOLUTION: This UV-curing compsn. consists of a free radical generating material generating a free radical under the action of UV and polymer molecules each having a functional group polymerized by the action of the free radical. The free radical generating material is at least one kind of benzoin ether and is contained by 0.001-10wt.% of the total amt. of this compsn. The polymer molecules are silicone polymer molecules whose skeleton structure is represented by the formula (R3 SiO1/2 )a (R'2 SiO2/2 )b (R"SiO3/2 )c -(SiO4/2 )d (where each of R, R' and R" is H, 1-10C satd. or unsatd. hydrocarbon).

9. 发明专利

JPH09268228A ULTRAVIOLET-CURING COMPOSITION AND FORMATION OF CURED MATERIAL PATTERN USING THE SAME 失效
公开(公告)号：JPH09268228A
公开(公告)日：1997-10-14
申请号：JP7889396
申请日：1996-04-01
申请人： DOW CORNING ASIA LTD
发明人： BURAIAN ROBAATO HAAKUNESU , TAKEUCHI KASUMI , TACHIKAWA MAMORU
IPC分类号： C08L83/05 , C08G77/06 , C08G77/12 , C08G77/16 , C08G77/22 , C08K5/3432 , C08L83/04 , G03F7/004 , G03F7/075
摘要： PROBLEM TO BE SOLVED: To obtain an ultraviolet-curing composition very little in weight reduction after curing, not causing curing damage caused by air or oxygen, capable of forming a silicone curing film, comprising a specific base generating substance and a prescribed polymer component. SOLUTION: This ultraviolet-curing composition comprises (A) a base generating substance to produce a base by an acton of ultraviolet light and (B) and Si-H bond-containing polymer component capable of being reacted with OH group by the action of the based and forming an Si-H band and hydrogen. The component A is selected from N-substituted 4-(o-nitrophenyl)dihydropyridines and the amount of the component A is 0.01-20% based on the total weight. The average composition of the component B is shown by the formula (R2 SiO2/2 )a (RSiO3/2 )b (R is H, a mono radical selected from a 1-8C hydrocarbon and its derivative with the proviso that the sum of amounts contained in which one or both of Rs in the R2 SiO2/2 are H and R is H in the RSiO3/2 is >=5% (a+b); 0

10. 发明专利

JPH08127657A PRODUCTION OF CURED DIPHENYLSILOXANE AND CURED PRODUCT 失效
公开(公告)号：JPH08127657A
公开(公告)日：1996-05-21
申请号：JP26739594
申请日：1994-10-31
申请人： DOW CORNING ASIA LTD
发明人： BURAIAN ROBAATO HAAKUNESU , TAKEUCHI KASUMI , MICHINO TETSUYUKI , TACHIKAWA MAMORU
IPC分类号： C08F299/08 , C08F290/00 , C08G77/20 , C08G77/22 , C08G77/38 , C08G77/42 , C08G77/442
摘要： PURPOSE: To obtain a diphenylsiloxane cured product useful as a siloxane-based material having improved processability while keeping the thermal stability, rigidity, electrical characteristics, etc., of the base resin by curing a diphenylsiloxane oligomer having both terminals terminated with specific functional groups. CONSTITUTION: A diphenylsiloxane oligomer of the formula [at least one of R to R and at least one of R to R are each H or a 2-10C (un)saturated hydrocarbon group (excluding phenyl and alkyl-substituted phenyl) and the remaining R to R and R to R groups are each methyl, phenyl, etc.; R , R , R and R are each an organic group; R and R or R and R are not phenyl at the same time; (m) is 1-50; (k) and (n) are each 0-3] is cured in the presence of a catalyst for curing, in the presence of a polymerization initiator or a polymerization catalyst or in the absence of a curing catalyst and polymerization initiator under heating or irradiation with light. Concretely, a hexaphenyltrisiloxane having both terminals terminated with (4-vinylphenyl) dimethylsilyl groups is heated at 300 deg.C for 2min to effect the curing of the siloxane by polymerization reaction.

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