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1. 发明申请

WO2011106720A3 HIGH CAPACITY ION CHROMATOGRAPHY STATIONARY PHASE AND METHOD OF FORMING 审中-公开
标题翻译：高容量离子色谱固定相及其制备方法
公开(公告)号：WO2011106720A3
公开(公告)日：2011-09-01
申请号：PCT/US2011/026343
申请日：2011-02-25
申请人： DIONEX CORPORATION , SRINIVASAN, Kannan , POHL, Christopher, A. , BHARDWAJ, Sheetal , LIN, Rong
发明人： SRINIVASAN, Kannan , POHL, Christopher, A. , BHARDWAJ, Sheetal , LIN, Rong
IPC分类号： B01J41/20 , B01J41/04 , B01J39/26 , B01J47/00 , B01D15/36
摘要： The present invention provides a new design for high capacity stationary phases for chromatography, for example, ion chromatography. The stationary phases include a first polymer layer in contact with and at least partially coating the substrate of the stationary phase. The first polymer layer serves as a foundation for the attachment, and in various embodiments, the growth and attachment, of a highly hyperbranched polymer structure, typically based on one or more products of condensation polymerization. Multiple components are of use in forming the first polymer layer and the hyperbranched polymer structure, thereby providing a stationary phase that can be engineered to have a desired property such as ion capacity, ion selectivity, and the like. Exemplary condensation polymers are formed by the reaction of at least one polyfunctional compound with at least one compound of complimentary reactivity, e.g., a nucleophilic polyfunctional compound reacting with an electrophilic compound.
摘要翻译：本发明提供了用于色谱法的高容量固定相的新设计，例如离子色谱法。固定相包括与固定相的基底接触并且至少部分涂覆固定相的基底的第一聚合物层。第一聚合物层用作附着的基础，并且在各种实施方案中，高度超支化聚合物结构的生长和附着通常基于一种或多种缩聚产物。多种组分可用于形成第一聚合物层和超支化聚合物结构，从而提供可被设计成具有期望性质如离子容量，离子选择性等的固定相。示例性的缩合聚合物通过至少一种多官能化合物与至少一种互补反应性化合物（例如与亲电子化合物反应的亲核多官能化合物）反应而形成。

2. 发明申请

WO2009108521A1 ION CHROMATOGRAPHY SYSTEM WITH ELUENT RECYCLE 审中-公开
标题翻译：离子色谱系统与ELUENT RECYCLE
公开(公告)号：WO2009108521A1
公开(公告)日：2009-09-03
申请号：PCT/US2009/034108
申请日：2009-02-13
申请人： DIONEX CORPORATION , SRINIVASAN, Kannan , LIN, Rong , BHARDWAJ, Sheetal , POHL, Christopher, A.
发明人： SRINIVASAN, Kannan , LIN, Rong , BHARDWAJ, Sheetal , POHL, Christopher, A.
IPC分类号： G01N30/96
CPC分类号： G01N30/96
摘要： Non-suppressed ion chromatography apparatus including a chromatographic column (18), a source (10) of an aqueous eluent liquid stream (12), a detector (20), a recycle line (22,26) between the detector and the chromatographic columninlet, and a purifying device (24) disposed along the recycle line including ion exchange removal medium. Also, such apparatus with an electrolytic purifying device disposed along the recycle line. Also, methods of using such apparatus.
摘要翻译：非抑制离子色谱装置，包括色谱柱（18），洗脱液流（12）的水源（10），检测器（20），检测器和色谱柱柱之间的再循环管线（22,26），以及沿着包括离子交换去除介质的循环管线设置的净化装置（24）。此外，这种具有沿着再循环线设置的电解净化装置的装置。另外，使用这种装置的方法。

3. 发明申请

WO2012125493A1 ELECTROSTATICALLY BOUND HYPERBRANCHED ANION EXCHANGE SURFACE COATING PREPARED VIA CONDENSATION POLYMERIZATION USING TERTIARY AMINE LINKERS FOR IMPROVED DIVALENT ANION SELECTIVITY 审中-公开
标题翻译：通过使用苛性氨基连接剂进行缩合聚合制备的静电粘合的超薄膜阴离子交换表面涂层，用于改进的多种阴离子选择性
公开(公告)号：WO2012125493A1
公开(公告)日：2012-09-20
申请号：PCT/US2012/028586
申请日：2012-03-09
申请人： DIONEX CORPORATION , POHL, Christopher, A. , SRINIVASAN, Kannan , BHARDWAJ, Sheetal
发明人： POHL, Christopher, A. , SRINIVASAN, Kannan , BHARDWAJ, Sheetal
IPC分类号： B01J39/26 , B01J41/04 , B01J41/20 , B01J47/00 , B01J41/12 , B01D15/36
CPC分类号： B01J39/26 , B01D15/361 , B01J41/13 , B01J41/20 , B01J47/016 , Y10T428/1393
摘要： The present invention provides a new design for high capacity stationary phases for dianion selective ion chromatography. The stationary phases include one or more layers which are products of condensation polymerization. Multiple components are of use in forming the first polymer layer and the condensation polymer structure, thereby providing a stationary phase that can be engineered to have a desired property such as ion capacity, ion selectivity, and the like. Exemplary condensation polymers are formed by the reaction of at least one polyfunctional compound with at least one compound of complimentary reactivity, e.g., a nucieophilic polyfunctional compound reacting with an eiectrophilic compound.
摘要翻译：本发明提供了用于双阴离子选择性离子色谱法的高容量固定相的新设计。固定相包括一个或多个作为缩聚产物的层。多个组分可用于形成第一聚合物层和缩聚物结构，从而提供可被工程化以具有所需性质如离子容量，离子选择性等的固定相。示例性缩合聚合物通过至少一种多官能化合物与至少一种互补反应性化合物的反应形成，例如与亲水性化合物反应的亲油性多官能化合物。

4. 发明申请

WO2009105387A1 ION CHROMATOGRAPHY SYSTEMS WITH FLOW-DELAY ELUENT RECYCLE 审中-公开
标题翻译：离子色谱系统与流延迟回收
公开(公告)号：WO2009105387A1
公开(公告)日：2009-08-27
申请号：PCT/US2009/034015
申请日：2009-02-13
申请人： DIONEX CORPORATION , LIU, Yan , SRINIVASAN, Kannan , POHL, Christopher, A. , BHARDWAJ, Sheetal , LU, Zhongqing
发明人： LIU, Yan , SRINIVASAN, Kannan , POHL, Christopher, A. , BHARDWAJ, Sheetal , LU, Zhongqing
IPC分类号： G01N30/96
CPC分类号： B01D15/10 , G01N30/26 , G01N30/96 , G01N2030/965
摘要： A chromatographic method including chromatographically separating sample ionic species in an eluent stream, detecting the separated sample ionic species, catalytically combining hydrogen and oxygen gases or catalytically decomposing hydrogen peroxide in a catalytic gas elimination chamber (31), and recycling the effluent stream from the catalytic gas elimination chamber to the chromatography separation column (10). The residence time between the detector (14) and said chamber (31) is at least one minute to facilitate decomposition of unstable oxidative compounds. Also, flowing the recycle sequentially through two detector effluent flow channels of an electrolytic membrane suppressor (28). Also, applying heat or UV energy between the detector (14) and the chamber (31). Also, detecting bubbles after the chamber. Also, a Platinum group metal catalyst and ion exchange medium in the chamber. Apparatus for performing the methods.
摘要翻译：一种色谱方法，包括在洗脱液流中色谱分离样品离子物质，检测分离的样品离子物质，催化结合氢气和氧气，或催化分解催化气体消除室（31）中的过氧化氢，以及将来自催化剂的流出物流气体消除室至色谱分离柱（10）。检测器（14）和所述室（31）之间的停留时间为至少一分钟，以促进不稳定的氧化化合物的分解。此外，使循环物依次流过电解膜抑制器（28）的两个检测器流出物流动通道。而且，在检测器（14）和腔室（31）之间施加热或UV能量。另外，在室后检测气泡。此外，铂族金属催化剂和离子交换介质在室内。用于执行方法的装置。

5. 发明申请

WO2009108567A2 SAMPLE PRETREATMENT AND EXTRACTION 审中-公开
标题翻译：样品预处理和提取
公开(公告)号：WO2009108567A2
公开(公告)日：2009-09-03
申请号：PCT/US2009/034525
申请日：2009-02-19
申请人： DIONEX CORPORATION , SRINIVASAN, Kannan , RICHTER, Bruce , POHL, Christopher, A. , MURPHY, Brett , DORICH, Brian , ULLAH, S.M., Rahmat
发明人： SRINIVASAN, Kannan , RICHTER, Bruce , POHL, Christopher, A. , MURPHY, Brett , DORICH, Brian , ULLAH, S.M., Rahmat
IPC分类号： B01D11/04 , B01D15/08 , G01N1/34 , G01N30/00
CPC分类号： G01N1/34 , B01D11/0492 , B01J20/043 , B01J20/10 , B01J20/14 , B01J20/26 , B01J20/3236 , B01J2220/46 , B01J2220/66 , G01N1/4022 , G01N1/4044 , G01N1/405 , G01N30/7206 , G01N30/96 , G01N2001/4061 , Y10T436/10 , Y10T436/255
摘要： A method for pretreating and extracting a liquid sample by sorbing an aqueous liquid sample, including an organic analyte and an acid or a base, in a solid sorbent material, and at least partially neutralizing the acid or base by reaction with neutralizing ions retained on a support surface, and contacting the liquid sample-sorbed sorbent material at elevated temperature and pressure with an organic solvent to extract the analyte into said solvent, preferably in a vessel having an extraction chamber with a zirconium metal interior surface.
摘要翻译：通过在固体吸附剂材料中吸附包含有机分析物和酸或碱的含水液体样品并至少部分中和酸或碱来预处理和提取液体样品的方法通过与保留在载体表面上的中和离子反应，并使液体样品吸附的吸附剂材料在升高的温度和压力下与有机溶剂接触以将分析物提取到所述溶剂中，优选在具有提取室的容器内，表面上。

6. 发明申请

WO2004070377A2 IMPROVED CAPACITY CHEMICAL SUPPRESSORS AND METHOD OF USE 审中-公开
标题翻译：改进的能力化学抑制剂和使用方法
公开(公告)号：WO2004070377A2
公开(公告)日：2004-08-19
申请号：PCT/US2003/039219
申请日：2003-12-09
申请人： DIONEX CORPORATION , SRINIVASAN, Kannan , POHL, Christopher, A.
发明人： SRINIVASAN, Kannan , POHL, Christopher, A.
IPC分类号： G01N30/00
CPC分类号： G01N30/96 , B01D15/367 , B01D61/48 , Y10T436/25
摘要： A non-electrolytic method and apparatus for treating an aqueous sample stream including analyte ions and matrix ions of opposite charge, for pretreatment or suppression. The apparatus includes an ion exchange membrane capable of passing only ions of opposite charge to the analyte ions, a sample stream flow channel, a first aqueous stream ion receiving flow channel adjacent one side of the sample stream flow channel and separated therefrom by the first ion exchange membrane, and stationary flow-through ion exchange packing disposed in the sample stream flow channel. The ion receiving channel has an ion exchange capacity for the matrix ions less than about 25% of the ion exchange capacity for the matrix ions.
摘要翻译：一种用于处理包含分析物离子和相反电荷的基质离子的水样品流用于预处理或抑制的非电解方法和装置。该装置包括能够仅将相反电荷的离子通过到分析物离子的离子交换膜，样品流流动通道，邻近样品流流动通道的一侧的第一含水流离子接收流动通道，并由第一离子交换膜和设置在样品流流动通道中的固定流通离子交换填料。离子接收通道对于基质离子的离子交换容量小于基质离子的离子交换容量的约25％。

7. 发明申请

WO2005077534A1 ION EXCHANGE PARTICLE-BOUND FLOW-THROUGH POROUS MONOLITH 审中-公开
标题翻译：离子交换颗粒流动 - 多孔多孔
公开(公告)号：WO2005077534A1
公开(公告)日：2005-08-25
申请号：PCT/US2005/002615
申请日：2005-01-27
申请人： DIONEX CORPORATION , SRINIVASAN, Kannan , ZAKARIA, Philip , AVDALOVIC, Nebojsa , POHL, Christopher, A. , HADDAD, Paul, R.
发明人： SRINIVASAN, Kannan , ZAKARIA, Philip , AVDALOVIC, Nebojsa , POHL, Christopher, A. , HADDAD, Paul, R.
IPC分类号： B01J39/18
CPC分类号： B01D15/361 , B01J20/28042 , B01J20/28097 , B01J47/018 , B01J2220/54 , B01J2220/82
摘要： A flow-through ion exchange medium comprising a monolithic stationary phase having interconnecting pores defined by pore walls, and fine ion exchange polymeric layering particles irreversibly bound directly or indirectly to the pore walls, and methods of making such medium and its use on chromatographic separators.
摘要翻译：一种流通离子交换介质，其包括具有由孔壁限定的互连孔的整体式固定相和不可逆地直接或间接地结合孔壁的细小离子交换聚合分层颗粒，以及制备此类介质的方法及其在色谱分离器上的应用。

8. 发明申请

WO2011100248A1 ELECTROCHEMICAL DETECTION CELL FOR LIQUID CHROMATOGRAPHY SYSTEM 审中-公开
标题翻译：用于液相色谱系统的电化学检测细胞
公开(公告)号：WO2011100248A1
公开(公告)日：2011-08-18
申请号：PCT/US2011/024061
申请日：2011-02-08
申请人： DIONEX CORPORATION , CHENG, Jun , JANDIK, Petr , POHL, Christopher, A.
发明人： CHENG, Jun , JANDIK, Petr , POHL, Christopher, A.
IPC分类号： H01M14/00 , G01N27/26
CPC分类号： G01N27/30 , G01N27/301 , G01N27/4166 , G01N30/64
摘要： A detection cell for a chromatography system includes a cell body having an inlet, an outlet, and a counter electrode, a working electrode, a sample flow passageway extending between the inlet and the outlet and in fluid contact with the counter and working electrodes, and a palladium/noble metal reference electrode system. A method of using the detection cell is also described.
摘要翻译：用于色谱系统的检测电池包括具有入口，出口和对电极的电池体，工作电极，在入口和出口之间延伸并与计数器和工作电极流体接触的样品流动通道，以及钯/贵金属参考电极系统。还描述了使用检测单元的方法。

9. 发明申请

WO2007121267A3 PULSED ELECTROCHEMICAL DETECTION METHOD 审中-公开
公开(公告)号：WO2007121267A3
公开(公告)日：2007-10-25
申请号：PCT/US2007/066465
申请日：2007-04-11
申请人： DIONEX CORPORATION , CHENG, Jun , JANDIK, Petr , LIU, Xiaodong , POHL, Christopher, A.
发明人： CHENG, Jun , JANDIK, Petr , LIU, Xiaodong , POHL, Christopher, A.
IPC分类号： G01N27/403
摘要： In one embodiment, the present invention is directed to a pulsed electrochemical detection method comprising (a) flowing a liquid sample stream including at least one analyte past a working electrode in a flow-through cell; (b) applying at least three pulsed electrical potentials to the working electrode, (1) a first conditioning potential, (2) a second detection and oxidative cleaning potential, and (3) a third reductive cleaning potential, said second potential being higher than said first and third potentials and said first potential being higher than said third potential; and (c) detecting the output from said working electrode during the time period of applying said second potential.

10. 发明申请

WO2006091404A2 ION CHROMATOGRAPHY SYSTEM USING CATALYTIC GAS ELIMINATION 审中-公开
标题翻译：使用催化气体消除的离子色谱系统
公开(公告)号：WO2006091404A2
公开(公告)日：2006-08-31
申请号：PCT/US2006/004865
申请日：2006-02-10
申请人： DIONEX CORPORATION , LIU, Yan , POHL, Christopher, A. , AVDALOVIC, Nebojsa , RIVIELLO, John, M. , SIRIRAKS, Archava
发明人： LIU, Yan , POHL, Christopher, A. , AVDALOVIC, Nebojsa , RIVIELLO, John, M. , SIRIRAKS, Archava
IPC分类号： G01N30/96
CPC分类号： G01N30/96 , G01N30/62 , G01N2030/965
摘要： A liquid chromatographic system is provided including catalytically combining hydrogen and oxygen gases in the chromatography eluent stream in a catalytic gas elimination chamber, to form water and thereby reduce the gas content in the eluent stream. Also, a liquid ion chromatographic system in which the effluent from the detector is recycled to a membrane suppressor and then is mixed with a source of eluent for recycle to the chromatographic column.
摘要翻译：提供一种液相色谱系统，其包括在催化气体消除室中的色谱洗脱液流中催化结合氢气和氧气，形成水，从而降低洗脱液流中的气体含量。此外，液体离子色谱系统将来自检测器的流出物再循环至膜抑制剂，然后与洗脱液混合以再循环至色谱柱。

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