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1. 发明授权

US4329449A Method of using recycled mother liquors to produce aldosides 失效
标题翻译：使用回收母液生产醛糖苷的方法
公开(公告)号：US4329449A
公开(公告)日：1982-05-11
申请号：US126257
申请日：1980-03-03
申请人： Claris D. Roth , Kenneth B. Moser , William A. Bomball
发明人： Claris D. Roth , Kenneth B. Moser , William A. Bomball
IPC分类号： B01J19/24 , C07H1/00 , C07H15/04
CPC分类号： C07H15/04 , B01J19/243 , C07H1/00 , B01J2219/00069 , B01J2219/00094 , B01J2219/00099 , B01J2219/00123 , B01J2219/00153 , B01J2219/00159 , B01J2219/00162 , B01J2219/00186 , Y02P20/582
摘要： The present invention relates to the preparation of aldoside mixtures, recovering at least a portion of one aldoside component therefrom and reusing the remaining portion of the aldoside mixture to prepare additional aldoside. The aldoside mixture may be prepared by slurrying the carbohydrate in alcohol and passing the slurry through a continuous reactor at an elevated temperature under fluid pressure in the presence of an acid catalyst. The resultant aldoside mixture may then be partitioned into a mother liquor portion and an aldoside portion by selectively recovering at least a portion of one aldoside from the crude aldoside mixture with the remaining mother liquor being recycled.Crude glycoside mixtures prepared from starch and methanol slurries are suitable substrates for selectively recovering methyl-alpha-D-glucopyranoside. The methyl-alpha-D-glucopyranoside may be easily crystallized and recovered from the glycoside mixture because of its lower solubility in methanol. The resultant mother liquor (rich in the remaining components of the glycoside mixture) in combination with freshly added starch and methanol provides a reaction medium which optimizes methyl-alpha-D-glucopyranoside production.
摘要翻译：本发明涉及醛糖苷混合物的制备，从其中回收至少一部分一种醛苷成分，并重新使用其余部分的醛糖苷混合物制备另外的醛糖苷。醛糖苷混合物可以通过将碳水化合物在醇中制浆并使浆液在升高的温度下在酸性催化剂的存在下在流体压力下通过连续反应器来制备。然后通过选择性地从粗醛苷混合物中回收至少一部分来自粗制醛苷混合物的一种醛糖苷，将所得的醛糖苷混合物分配成母液部分和醛糖苷部分，剩余的母液被再循环。由淀粉和甲醇浆液制备的粗糖苷混合物是选择性回收甲基-α-D-吡喃葡萄糖苷的合适底物。由于甲基-α-D-吡喃葡萄糖苷在甲醇中的溶解度较低，甲基-α-D-吡喃葡萄糖苷可以容易地结晶并从糖苷混合物中回收。所得到的母液（富含剩余组分的糖苷混合物）与新鲜淀粉和甲醇的组合提供了优化甲基-α-D-吡喃葡萄糖苷生产的反应介质。

2. 发明授权

US4223129A Continuous process for making alkyl aldosides from starch or other carbohydrates 失效
标题翻译：从淀粉或其他碳水化合物制备烷基醛糖的连续方法
公开(公告)号：US4223129A
公开(公告)日：1980-09-16
申请号：US938750
申请日：1978-09-01
申请人： Claris D. Roth , Kenneth B. Moser , William A. Bomball
发明人： Claris D. Roth , Kenneth B. Moser , William A. Bomball
IPC分类号： B01J19/24 , C07H1/00 , C07H15/04
CPC分类号： C07H15/04 , B01J19/243 , C07H1/00 , B01J2219/00069 , B01J2219/00094 , B01J2219/00099 , B01J2219/00123 , B01J2219/00153 , B01J2219/00159 , B01J2219/00162 , B01J2219/00186
摘要： A continuous process for making alkyl aldosides from polysaccharides and more particularly mixed alkyl glycosides from starch by direct alcoholysis. A polysaccharide, such as starch, is slurried in an alcohol and passed through a heated, confined zone under pressure in the presence of an acid catalyst to form a mixed alkyl aldoside. The alcohols which may be used include methanol, ethanol, propanol and butanol, their isomers and mixtures thereof. Higher alkyl glycosides are surfactants and, in some instances, it is advantageous to use higher alcohols, such as decyl and dodecyl alcohols, to obtain particular surfactant properties in the resulting alkyl glycosides. Mixed alkyl glycosides are useful in detergent applications, and as backbone polymers in polyurethane foams.
摘要翻译：通过直接醇解制备来自多糖的烷基醛糖的连续方法，更特别是来自淀粉的混合烷基糖苷。将多糖如淀粉在醇中制浆，并在酸催化剂存在下通过加压的限制区，形成混合的烷基醛糖苷。可以使用的醇包括甲醇，乙醇，丙醇和丁醇，它们的异构体及其混合物。高级烷基糖苷是表面活性剂，在某些情况下，使用高级醇如癸基和十二烷醇有利于在所得的烷基糖苷中获得特定的表面活性剂。混合烷基糖苷可用于洗涤剂应用中，也可用作聚氨酯泡沫中的主链聚合物。

3. 发明授权

US4834903A Alkylene oxide adducts of glycoside surfactants and detergent compositions containing same 失效
标题翻译：糖苷表面活性剂和含有它们的洗涤剂组合物的环氧烷加成物
公开(公告)号：US4834903A
公开(公告)日：1989-05-30
申请号：US203604
申请日：1988-06-02
申请人： Claris D. Roth , Kenneth B. Moser , Gail M. Howell , Allen D. Urfer
发明人： Claris D. Roth , Kenneth B. Moser , Gail M. Howell , Allen D. Urfer
IPC分类号： C11D1/66
CPC分类号： C11D1/662 , Y10S516/01 , Y10S516/92
摘要： Remarkably good surfactancy characteristics are exhibited by alkylene oxide (e.g., ethylene oxide, propylene oxide, etc.) adducts of relatively low degree of polymerication, (D.P.), long chain glycoside compositions of the sort which are predominantly composed of long chain monoglycoside species and in which the types and relative proportions of any long chain polyglycoside species contained therein are such that the average degree of polymerization of such long chain glycoside constituents is less than 2.7.The subject low D.P. long chain polyglycoside alkylene oxide adducts exhibit surfactancy and/or detergency characteristics at least about as good as, and in some respects substantially better than, the corresponding alkylene oxide adducts of higher D.P. long chain glycoside materials.
摘要翻译：具有相对较低聚合度的环氧烷（例如环氧乙烷，环氧丙烷等）加合物，（DP），主要由长链单糖苷类物质组成的长链糖苷组合物表现出极好的表面活性特性，其中包含其中的任何长链多糖苷种类的类型和相对比例使得这种长链糖苷组分的平均聚合度小于2.7。主题低D.P. 长链多糖苷环氧烷加成物表现出至少大约等于和在某些方面基本上优于较高D.P.的相应的烯化氧加合物的表面活性和/或去污力特性。长链糖苷物质。

4. 依法登记的发明

USH444H Process for making molded articles with mold release agents 失效
标题翻译：用脱模剂制造模制品的方法
公开(公告)号：USH444H
公开(公告)日：1988-03-01
申请号：US735900
申请日：1985-05-20
申请人： Claris D. Roth , Kenneth B. Moser
发明人： Claris D. Roth , Kenneth B. Moser
IPC分类号： B29C33/60 , B29C45/00 , B29C67/24 , C08G18/32
CPC分类号： B29C33/60 , B29C45/0001 , B29C67/246 , B29K2075/00 , B29K2105/04 , C08G18/3218 , C08G2120/00
摘要： A glycoside compound containing one or more fatty acid ester or ether groups is used as a mold release agent in the production of molded articles from polymeric resinous materials. Said mold release agent can function as either external or internal mold release agent. The molded article also has improved tie coating properties.

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