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1. 发明授权

US07591937B2 Method of fixing macro-objects to an electricity conducting- or semi-conducting surface by means of electrografting, surfaces thus obtained and applications thereof 有权
标题翻译：通过电动移动将大型物体固定到导电或半导电表面的方法，如此获得的表面及其应用
公开(公告)号：US07591937B2
公开(公告)日：2009-09-22
申请号：US10508665
申请日：2003-03-19
申请人： Christophe Bureau , Guy Deniau , José Gonzalez , Serge Palacin
发明人： Christophe Bureau , Guy Deniau , José Gonzalez , Serge Palacin
IPC分类号： C25D11/32 , C25D11/34
CPC分类号： C09D5/4476 , Y10T29/49126 , Y10T29/49128 , Y10T29/49165 , Y10T428/12493
摘要： The invention relates to a method of fixing macro-objects to an electricity conducting- or semi-conducting surface by means of electrografting. The invention also relates to the electricity conducting- or semi-conducting-surfaces obtained using the aforementioned method and to the applications of same.
摘要翻译：本发明涉及一种通过电动移动将大型物体固定到导电或半导电表面的方法。本发明还涉及使用上述方法获得的导电或半导体表面及其应用。

2. 发明授权

US07119030B2 Process for lining a surface using an organic film 有权
标题翻译：使用有机膜衬里表面的方法
公开(公告)号：US07119030B2
公开(公告)日：2006-10-10
申请号：US10523641
申请日：2003-08-25
申请人： Christophe Bureau , Guy Deniau , Serge Palacin
发明人： Christophe Bureau , Guy Deniau , Serge Palacin
IPC分类号： H01L21/469 , H01L21/31
CPC分类号： C09D5/4476 , Y10T29/49126 , Y10T29/49128 , Y10T29/49165
摘要： The present invention relates to a method for cladding a simple or complex surface, electrically conducting or semiconducting, by means of an organic film from at least one precursor of said organic film, characterized in that the cladding of the surface by the organic film is carried out by electro-initiated grafting of said, at least one, precursor of said surface by applying at least one potential sweep on this surface carried out in such a way that at any point of said surface the maximum potential of each potential sweep, in absolute value and relative to a reference electrode, is greater than or equal to the value of the potential (vbloc) from which the curves of a graph expressing the quantity of electro-grafted precursor on a surface identical to said surface in function of the number of potential sweeps are all superposed and independent of this vbloc potential.
摘要翻译：本发明涉及一种通过有机膜从有机膜的至少一种前体包覆简单或复杂的表面，导电或半导体的方法，其特征在于，通过有机膜包覆表面通过在该表面上施加至少一个电位扫描，使得在所述表面的任何点处具有绝对的每个电位扫描的最大电位，使所述表面的至少一个前体电接触，值和相对于参比电极的电流值大于或等于表示电接枝前体的量在与表面相同的表面上的电位（v _{所述表面的电势扫描次数的函数全部叠加并且独立于该电势。}

3. 发明申请

US20060110929A1 Anhydrous film for lip make-up or care 有权
标题翻译：用于唇膏化妆或护理的无水膜
公开(公告)号：US20060110929A1
公开(公告)日：2006-05-25
申请号：US10523641
申请日：2003-08-25
申请人： Christophe Bureau , Guy Deniau , Serge Palacin
发明人： Christophe Bureau , Guy Deniau , Serge Palacin
IPC分类号： H01L21/31
CPC分类号： C09D5/4476 , Y10T29/49126 , Y10T29/49128 , Y10T29/49165
摘要： The present invention relates to a method for cladding a simple or complex surface, electrically conducting or semiconducting, by means of an organic film from at least one precursor of said organic film, characterised in that the cladding of the surface by the organic film is carried out by electro-initiated grafting of said, at least one, precursor of said surface by applying at least one potential sweep on this surface carried out in such a way that at any point of said surface the maximum potential of each potential sweep, in absolute value and relative to a reference electrode, is greater than or equal to the value of the potential (vbloc) from which the curves of a graph expressing the quantity of electro-grafted precursor on a surface identical to said surface in function of the number of potential sweeps are all superposed and independent of this vbloc potential.
摘要翻译：本发明涉及一种通过有机膜从有机膜的至少一种前体包覆简单或复杂的表面，导电或半导体的方法，其特征在于，通过有机膜包覆表面通过在该表面上施加至少一个电位扫描，使得在所述表面的任何点处具有绝对的每个电位扫描的最大电位，使所述表面的至少一个前体电接触，值和相对于参比电极的电流值大于或等于表示电接枝前体的量在与表面相同的表面上的电位（v _{所述表面的电势扫描次数的函数全部叠加并且独立于该电势。}

4. 发明申请

US20050170195A1 Method of fixing macro-objects to an electricity conducting- or semi-conducting surface by means of electrografting, surfaces thus obtained and appplications thereof 有权
标题翻译：通过电动移动将大型物体固定到导电或半导电表面的方法，如此获得的表面及其应用
公开(公告)号：US20050170195A1
公开(公告)日：2005-08-04
申请号：US10508665
申请日：2003-03-19
申请人： Christophe Bureau , Guy Deniau , Jose Gonzalez , Serge Palacin
发明人： Christophe Bureau , Guy Deniau , Jose Gonzalez , Serge Palacin
IPC分类号： C09D4/00 , C09D5/44 , C25D9/02 , C25D13/06 , C25D5/10
CPC分类号： C09D5/4476 , Y10T29/49126 , Y10T29/49128 , Y10T29/49165 , Y10T428/12493
摘要： The invention relates to a method of fixing macro-objects to an electricity conducting- or semi-conducting surface by means of electrografting. The invention also relates to the electricity conducting- or semi-conducting-surfaces obtained using the aforementioned method and to the applications of same.
摘要翻译：本发明涉及一种通过电动移动将大型物体固定到导电或半导电表面的方法。本发明还涉及使用上述方法获得的导电或半导体表面及其应用。

5. 发明申请

US20080145706A1 METHOD FOR PREPARING AN ORGANIC FILM AT THE SURFACE OF SOLID SUPPORT UNDER NON-ELECTROCHEMICAL CONDITIONS, SOLID SUPPORT THUS OBTAINED AND PREPARATION KIT 有权
标题翻译：在非电化学条件下在固体表面上制备有机膜的方法，获得和制备试剂盒的固体支持
公开(公告)号：US20080145706A1
公开(公告)日：2008-06-19
申请号：US11835004
申请日：2007-08-07
申请人： Vincent Mevellec , Sebastien Roussel , Serge Palacin , Guy Deniau
发明人： Vincent Mevellec , Sebastien Roussel , Serge Palacin , Guy Deniau
IPC分类号： B05D3/02 , B32B9/04
CPC分类号： C09D4/00 , B82Y30/00 , C08J7/02 , C08J7/04 , C23C18/04 , C23C18/08 , C23C18/14 , C23C18/28 , C23C18/31 , H01L51/0006 , H01L51/0021 , H01L51/0075 , Y10T428/31616 , Y10T428/31681
摘要： This invention relates to a method for preparing an organic film at the surface of a solid support, with a step of contacting said surface with a liquid solution including (i) at least one protic solvent, (ii) at least one adhesion primer, under non-electrochemical conditions, and allowing the formation of radical entities based on the adhesion primer. The liquid solution can also include (iii) at least one monomer different from the adhesion primer and radically polymerisable. This invention also relates to a non-electrically-conductive solid support on which an organic film according to said method is grafted, and a kit for preparing an essentially polymeric organic film at the surface of a solid support.
摘要翻译：本发明涉及一种在固体支持物表面制备有机膜的方法，其中使所述表面与液体溶液接触的步骤包括：（i）至少一种质子溶剂，（ii）至少一个粘合底漆，非电化学条件，并且允许基于粘合引物形成基团实体。液体溶液还可以包括（iii）至少一种不同于粘合底漆的单体和可自由基聚合的单体。本发明还涉及一种非导电固体载体，其上接枝有根据所述方法的有机膜，以及用于在固体载体表面制备基本上聚合的有机膜的试剂盒。

6. 发明授权

US09725602B2 Method for preparing an organic film at the surface of a solid support under non-electrochemical conditions, solid support thus obtained and preparation kit 有权
公开(公告)号：US09725602B2
公开(公告)日：2017-08-08
申请号：US11960109
申请日：2007-12-19
申请人： Vincent Mevellec , Sebastien Roussel , Serge Palacin , Guy Deniau , Thomas Berthelot , Cecile Baudin , Adhitya Trenggono
发明人： Vincent Mevellec , Sebastien Roussel , Serge Palacin , Guy Deniau , Thomas Berthelot , Cecile Baudin , Adhitya Trenggono
IPC分类号： B05D3/10 , C09D4/00 , H01L51/00
CPC分类号： C09D4/00 , H01L51/0006 , H01L51/0075 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31678 , Y10T428/31989 , Y10T428/31993
摘要： This invention relates to a method for preparing an organic film at the surface of a solid support, with a step of contacting said surface with a liquid solution including (i) at least one solvent, (ii) at least one adhesion primer, under non-electrochemical conditions, and allowing the formation of radical entities based on the adhesion primer. The liquid solution can also include (iii) at least one monomer different from the adhesion primer and radically polymerizable. This invention also relates to a non-electrically-conductive solid support on which an organic film according to said method is grafted, and a kit for preparing an essentially polymeric organic film at the surface of a solid support.

7. 发明授权

US08152986B2 Process for forming organic films on electrically conductive or semi-conductive surfaces using aqueous solutions 有权
标题翻译：使用水溶液在导电或半导体表面上形成有机膜的方法
公开(公告)号：US08152986B2
公开(公告)日：2012-04-10
申请号：US11364360
申请日：2006-02-28
申请人： Guy Deniau , Serge Palacin
发明人： Guy Deniau , Serge Palacin
IPC分类号： C25D11/00
CPC分类号： C25D7/00 , A61L31/10 , C08F283/00 , C08F291/00 , C08F292/00 , C08L51/003 , C08L51/10 , C09D5/4476 , H01C17/06586 , H01G4/14 , H01G9/0036 , H01L51/0006 , H01L51/0034 , C08L2666/02
摘要： The present invention concerns the area of surface coatings in the form of organic films, the coatings being in the form of organic films. It most especially relates to a method for forming copolymer organic films by electrochemical grafting on electrically conductive or semi-conductive surfaces using electrolytic aqueous solutions containing at least one protic solvent, at least one radically polymerizable monomer and at least one surfactant. The invention also concerns surfaces obtained with the use of this method, their applications especially for preparation of microelectronic components, biomedical devices or screening kits, as well as the electrolyte solution used in the course of the method.
摘要翻译：本发明涉及有机膜形式的表面涂层的面积，该涂层为有机膜的形式。特别涉及使用含有至少一种质子性溶剂，至少一种可自由基聚合的单体和至少一种表面活性剂的电解水溶液在导电或半导电表面上通过电化学接枝形成共聚物有机膜的方法。本发明还涉及使用该方法获得的表面，其特别用于制备微电子部件，生物医学装置或筛选试剂盒的应用，以及在该方法中使用的电解质溶液。

8. 发明申请

US20080193668A1 METHOD FOR PREPARING AN ORGANIC FILM AT THE SURFACE OF A SOLID SUPPORT UNDER NON-ELECTROCHEMICAL CONDITIONS, SOLID SUPPORT THUS OBTAINED AND PREPARATION KIT 有权
标题翻译：在非电化学条件下在固体支持表面制备有机膜的方法，获得和制备试剂盒的固体支持
公开(公告)号：US20080193668A1
公开(公告)日：2008-08-14
申请号：US11960109
申请日：2007-12-19
申请人： Vincent Mevellec , Sebastien Roussel , Serge Palacin , Guy Deniau , Thomas Berthelot , Cecile Baudin , Adhitya Trenggono
发明人： Vincent Mevellec , Sebastien Roussel , Serge Palacin , Guy Deniau , Thomas Berthelot , Cecile Baudin , Adhitya Trenggono
IPC分类号： B05D3/06 , B32B33/00 , B32B15/00 , B32B21/00 , B32B29/00 , B32B5/16 , B05D3/10 , B32B9/00 , B05D1/32 , B05D3/00
CPC分类号： C09D4/00 , H01L51/0006 , H01L51/0075 , Y10T428/25 , Y10T428/26 , Y10T428/31504 , Y10T428/31678 , Y10T428/31989 , Y10T428/31993
摘要： This invention relates to a method for preparing an organic film at the surface of a solid support, with a step of contacting said surface with a liquid solution including (i) at least one solvent, (ii) at least one adhesion primer, under non-electrochemical conditions, and allowing the formation of radical entities based on the adhesion primer. The liquid solution can also include (iii) at least one monomer different from the adhesion primer and radically polymerizable. This invention also relates to a non-electrically-conductive solid support on which an organic film according to said method is grafted, and a kit for preparing an essentially polymeric organic film at the surface of a solid support.
摘要翻译：本发明涉及一种在固体支持物表面制备有机膜的方法，其中使所述表面与液体溶液接触的步骤包括：（i）至少一种溶剂，（ii）至少一种粘附底漆， - 电化学条件，并且允许基于粘合引物形成基团实体。液体溶液还可以包括（iii）至少一种不同于粘合底漆的单体和可自由基聚合的单体。本发明还涉及一种非导电固体载体，其上接枝有根据所述方法的有机膜，以及用于在固体载体表面制备基本上聚合的有机膜的试剂盒。

9. 发明授权

US08288009B2 Formation of ultra-thin films that are grafted to electrically-conducting or semi-conducting surfaces 失效
标题翻译：形成接枝到导电或半导体表面的超薄膜
公开(公告)号：US08288009B2
公开(公告)日：2012-10-16
申请号：US11908692
申请日：2006-03-13
申请人： Guy Deniau , Serge Palacin
发明人： Guy Deniau , Serge Palacin
IPC分类号： B32B27/32 , B32B27/00 , B05D3/02
CPC分类号： C25D9/02 , Y10T428/26 , Y10T428/265 , Y10T428/31855
摘要： The present invention relates to the use of precursors of following formula (I): independently of E or Z configuration, in which: R2 is an electron-withdrawing group, R1, R3, R4 and R5, which are identical or different, represent a hydrogen atom, an alkyl radical or an aryl radical, in the formation, by electrochemical grafting, of a homogeneous organic film, preferably with a thickness of less than or equal to 10 nm, on an electrically conducting or semiconducting surface; and to the corresponding process for the formation of an ultrathin homogeneous organic film on an electrically conducting or semiconducting surface.
摘要翻译：本发明涉及下列通式（I）的前体：与E或Z构型无关，其中：R 2是吸电子基团，R 1，R 3，R 4和R 5相同或不同，表示氢原子，烷基或芳基，通过电化学接枝，在导电或半导体表面上优选具有小于或等于10nm的厚度的均匀有机膜; 以及在导电或半导体表面上形成超薄均相有机膜的相应工艺。

10. 发明申请

US20080124832A1 Formation of Ultra-Thin Films that are Grafted to Electrically-Conducting or Semi-Conducting Surfaces 失效
标题翻译：嫁接到导电或半导体表面的超薄膜的形成
公开(公告)号：US20080124832A1
公开(公告)日：2008-05-29
申请号：US11908692
申请日：2006-03-13
申请人： Guy Deniau , Serge Palacin
发明人： Guy Deniau , Serge Palacin
IPC分类号： H01L51/30 , B32B9/00
CPC分类号： C25D9/02 , Y10T428/26 , Y10T428/265 , Y10T428/31855
摘要： The present invention relates to the use of precursors of following formula (I): independently of E or Z configuration, in which: R2 is an electron-withdrawing group, R1, R3, R4 and R5, which are identical or different, represent a hydrogen atom, an alkyl radical or an aryl radical, in the formation, by electrochemical grafting, of a homogeneous organic film, preferably with a thickness of less than or equal to 10 nm, on an electrically conducting or semiconducting surface; and to the corresponding process for the formation of an ultrathin homogeneous organic film on an electrically conducting or semiconducting surface.
摘要翻译：本发明涉及下列通式（I）的前体的用途：独立于E或Z构型，其中：R 2是吸电子基团，R 1 R 3，R 4，R 5和R 5相同或不同，表示氢原子，烷基或芳基在导电或半导体表面上通过电化学接枝形成均匀有机膜，优选具有小于或等于10nm的厚度; 以及在导电或半导体表面上形成超薄均相有机膜的相应工艺。

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