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1. 发明申请

US20140045683A1 PROCESS FOR PRODUCING IMPROVED ABSORBENT POLYMERS BY MEANS OF CRYOGENIC GRINDING 有权
标题翻译：通过低温磨削生产改进的吸收聚合物的方法
公开(公告)号：US20140045683A1
公开(公告)日：2014-02-13
申请号：US13876736
申请日：2011-10-05
申请人： Christoph Loick , Dominik Gartz , Laurent Wattebled , Jorg Harren
发明人： Christoph Loick , Dominik Gartz , Laurent Wattebled , Jorg Harren
IPC分类号： B01J20/26
CPC分类号： B01J20/267 , A61L15/22 , A61L15/60 , C08F6/008 , C08J3/12 , C08J3/245 , C08J2300/14 , C08J2333/00 , C08L33/00
摘要： A process for producing a water-absorbing polymer comprises: (i) mixing (α1) 0.1-99.99% by weight of ethylenically unsaturated monomers containing acid groups or salts thereof, or ethylenically unsaturated monomers including a protonated or quaternized nitrogen, or mixtures thereof, (α2) 0-70% by weight of ethylenically unsaturated monomers copolymerizable with (α1), (α3) 0.001-10% by weight of one or more crosslinkers, (α4) 0-30% by weight of water-soluble polymers, and (α5) 0-20% by weight of one or more assistants, where the sum of the weights (α1) to (α5) is 100%; (ii) free-radical polymerization with crosslinking to form an untreated hydrogel polymer; (iii) coarse comminution of the untreated hydrogel polymer to give pieces having a diameter from 0.1 mm to 5.0 cm; (iv) cooling and grinding the untreated hydrogel polymer; (v) drying the untreated hydrogel polymer after grinding at a temperature from 85° C. to 260° C.; (vi) postcrosslinking the hydrogel polymer and (vii) drying the water-absorbing polymer.
摘要翻译：制备吸水性聚合物的方法包括：（i）将0.1-99.99重量％含有酸基或其盐的烯属不饱和单体或包括质子化或季铵化的氮的烯键式不饱和单体或其混合物（α1）（α2）0-70重量％的可与（α1），（α3）0.001-10重量％的一种或多种交联剂共聚的烯属不饱和单体，（α4）0-30重量％的水溶性聚合物，和（α5）0-20重量％的一种或多种助剂，其中重量（α1）至（α5）的总和为100％; （ii）通过交联进行自由基聚合以形成未处理的水凝胶聚合物; （iii）未经处理的水凝胶聚合物的粗粉碎，得到直径为0.1mm至5.0cm的片; （iv）冷却和研磨未处理的水凝胶聚合物; （v）在85℃至260℃的温度下研磨后将未处理的水凝胶聚合物干燥; （vi）将水凝胶聚合物后交联，和（vii）干燥吸水聚合物。

2. 发明授权

US08859701B2 Process for producing improved absorbent polymers by means of cryogenic grinding 有权
标题翻译：通过低温研磨生产改进的吸收性聚合物的方法
公开(公告)号：US08859701B2
公开(公告)日：2014-10-14
申请号：US13876736
申请日：2011-10-05
申请人： Christoph Loick , Dominik Gartz , Laurent Wattebled , Jorg Harren
发明人： Christoph Loick , Dominik Gartz , Laurent Wattebled , Jorg Harren
IPC分类号： C08J9/36 , C08F20/06 , C08J3/12 , A61L15/60 , A61L15/22 , C08F6/00 , C08J3/24 , B01J20/26
CPC分类号： B01J20/267 , A61L15/22 , A61L15/60 , C08F6/008 , C08J3/12 , C08J3/245 , C08J2300/14 , C08J2333/00 , C08L33/00
摘要： A process for producing a water-absorbing polymer comprises: (i) mixing (α1) 0.1-99.99% by weight of ethylenically unsaturated monomers containing acid groups or salts thereof, or ethylenically unsaturated monomers including a protonated or quaternized nitrogen, or mixtures thereof, (α2) 0-70% by weight of ethylenically unsaturated monomers copolymerizable with (α1), (α3) 0.001-10% by weight of one or more crosslinkers, (α4) 0-30% by weight of water-soluble polymers, and (α5) 0-20% by weight of one or more assistants, where the sum of the weights (α1) to (α5) is 100%; (ii) free-radical polymerization with crosslinking to form an untreated hydrogel polymer; (iii) coarse comminution of the untreated hydrogel polymer to give pieces having a diameter from 0.1 mm to 5.0 cm; (iv) cooling and grinding the untreated hydrogel polymer; (v) drying the untreated hydrogel polymer after grinding at a temperature from 85° C. to 260° C.; (vi) postcrosslinking the hydrogel polymer and (vii) drying the water-absorbing polymer.
摘要翻译：制备吸水性聚合物的方法包括：（i）将（α1）0.1-99.99重量％的含有酸基团的烯属不饱和单体或包含质子化或季铵化的氮的烯属不饱和单体或其混合物，（α2）0-70重量％的可与（α1），（α3）0.001-10重量％的一种或多种交联剂共聚的烯属不饱和单体，（α4）0-30重量％的水溶性聚合物，和（α5）0-20重量％的一种或多种助剂，其中权重（α1）至（α5）之和为100％; （ii）通过交联进行自由基聚合以形成未处理的水凝胶聚合物; （iii）未经处理的水凝胶聚合物的粗粉碎，得到直径为0.1mm至5.0cm的片; （iv）冷却和研磨未处理的水凝胶聚合物; （v）在85℃至260℃的温度下研磨后将未处理的水凝胶聚合物干燥; （vi）将水凝胶聚合物后交联，和（vii）干燥吸水聚合物。

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