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1. 发明申请

US20130303361A1 SILICON-ALUMINUM MIXED OXIDE POWDER 有权
标题翻译：硅铝混合氧化物粉末
公开(公告)号：US20130303361A1
公开(公告)日：2013-11-14
申请号：US13997677
申请日：2012-02-03
申请人： Christian Schulze Isfort , Horst-Werner Zanthoff , Thomas Quandt , Christian Boeing
发明人： Christian Schulze Isfort , Horst-Werner Zanthoff , Thomas Quandt , Christian Boeing
IPC分类号： B01J31/26
CPC分类号： B01J21/12 , B01J35/002 , B01J35/1014 , B01J35/1019 , C01B33/183 , C01P2002/50 , C01P2004/50 , C01P2006/12 , C07C1/20
摘要： Silicon-aluminum mixed oxide powder having a weight ratio of (Al2O3/SiO2)ttl in the total primary particle of from 0.003 to 0.05, a weight ratio (Al2O3/SiO2)surface of the primary particles in a surface layer having a thickness of about 5 nm which is less than in the total primary particle and a BET surface area of from 50 to 250 m2/g.It is prepared by igniting one or more silicon compounds selected from the group consisting of CH3SiCl3, (CH3)2SiCl2, (CH3)3SiCl and (n-C3H7)SiCl3, a hydrolysable and oxidizable aluminum compound, at least one fuel gas and air and burning the flame into a reaction chamber, subsequently separating the solid from gaseous materials and subsequently treating the solid with water vapor.The silicon-aluminum mixed oxide powder can be used as catalyst.
摘要翻译：总一次粒子中的重量比（Al 2 O 3 / SiO 2）tt1为0.003〜0.05的硅铝混合氧化物粉末，表层的一次粒子的重量比（Al 2 O 3 / SiO 2）表面的厚度为约 5nm，小于总一次粒子，BET表面积为50〜250m 2 / g。通过点燃一种或多种选自CH 3 SiCl 3，（CH 3）2 Cl 2，（CH 3）3 SiCl和（n-C 3 H 7）SiCl 3）的硅化合物，可水解和可氧化的铝化合物，至少一种燃料气体和空气以及将火焰燃烧到反应室中，随后将固体与气态物质分离，随后用水蒸汽处理固体。硅铝混合氧化物粉末可用作催化剂。

2. 发明授权

US08980784B2 Silicon-aluminum mixed oxide powder 有权
标题翻译：硅铝混合氧化物粉末
公开(公告)号：US08980784B2
公开(公告)日：2015-03-17
申请号：US13997677
申请日：2012-02-03
申请人： Christian Schulze Isfort , Horst-Werner Zanthoff , Thomas Quandt , Christian Boeing
发明人： Christian Schulze Isfort , Horst-Werner Zanthoff , Thomas Quandt , Christian Boeing
IPC分类号： B01J21/12 , C01B33/18 , B01J35/00 , B01J35/10 , C07C1/20
CPC分类号： B01J21/12 , B01J35/002 , B01J35/1014 , B01J35/1019 , C01B33/183 , C01P2002/50 , C01P2004/50 , C01P2006/12 , C07C1/20
摘要： Silicon-aluminum mixed oxide powder having a weight ratio of (Al2O3/SiO2)ttl in the total primary particle of from 0.003 to 0.05, a weight ratio (Al2O3/SiO2)surface of the primary particles in a surface layer having a thickness of about 5 nm which is less than in the total primary particle and a BET surface area of from 50 to 250 m2/g. It is prepared by igniting one or more silicon compounds selected from the group consisting of CH3SiCl3, (CH3)2SiCl2, (CH3)3SiCl and (n-C3H7)SiCl3, a hydrolysable and oxidizable aluminum compound, at least one fuel gas and air and burning the flame into a reaction chamber, subsequently separating the solid from gaseous materials and subsequently treating the solid with water vapor. The silicon-aluminum mixed oxide powder can be used as catalyst.
摘要翻译：总一次粒子中的重量比（Al 2 O 3 / SiO 2）tt1为0.003〜0.05的硅铝混合氧化物粉末，表层的一次粒子的重量比（Al 2 O 3 / SiO 2）表面的厚度为约 5nm，小于总一次粒子，BET表面积为50〜250m 2 / g。通过点燃一种或多种选自CH 3 SiCl 3，（CH 3）2 Cl 2，（CH 3）3 SiCl和（n-C 3 H 7）SiCl 3）的硅化合物，可水解和可氧化的铝化合物，至少一种燃料气体和空气以及将火焰燃烧到反应室中，随后将固体与气态物质分离，随后用水蒸汽处理固体。硅铝混合氧化物粉末可用作催化剂。

3. 发明申请

US20150258535A1 PRODUCTION OF CATALYSTS BASED ON BORON ZEOLITES 审中-公开
标题翻译：基于硼硼沸石生产催化剂
公开(公告)号：US20150258535A1
公开(公告)日：2015-09-17
申请号：US14432928
申请日：2013-09-24
申请人： Asli Nau , Horst-Werner Zanthoff , Frank Geilen , Thomas Quandt , Dietrich Maschmeyer , Markus Winterberg , Stephan Peitz , Reiner Bukohl , Christian Boeing
发明人： Asli Nau , Horst-Werner Zanthoff , Frank Geilen , Thomas Quandt , Dietrich Maschmeyer , Markus Winterberg , Stephan Peitz , Reiner Bukohl , Christian Boeing
IPC分类号： B01J29/86 , B01J37/00 , B01J37/08 , B01J37/04 , B01J37/06
CPC分类号： B01J29/86 , B01J37/009 , B01J37/04 , B01J37/06 , B01J37/08 , B01J2229/37 , C01B37/007
摘要： The process described here has made it possible to obtain boron-containing silicates having a zeolitic structure which display negligible DME and C8 selectivities combined with high activities when used as catalysts for the dissociation of MTBE.
摘要翻译：这里描述的方法使得可以获得具有沸石结构的含硼硅酸盐，当用作MTBE解离的催化剂时，可以显示出可忽略的DME和C8选择性与高活性相结合。

4. 发明授权

US08877667B2 Process for regenerating a catalyst 有权
标题翻译：再生催化剂的方法
公开(公告)号：US08877667B2
公开(公告)日：2014-11-04
申请号：US13381676
申请日：2010-06-16
申请人： Christian Boeing , Dirk Roettger , Reiner Bukohl , Markus Winterberg , Dietrich Maschmeyer
发明人： Christian Boeing , Dirk Roettger , Reiner Bukohl , Markus Winterberg , Dietrich Maschmeyer
IPC分类号： B01J38/04 , B01J38/06 , B01J38/02 , B01J23/92 , B01J23/02 , B01J21/12
CPC分类号： B01J38/06 , B01J21/12 , B01J23/02 , B01J23/92
摘要： The invention relates to a process for regenerating catalysts containing mixed oxides from the group of alkali metal and/or alkaline earth metal oxides, aluminium oxide and silicon oxide, characterized in that the regeneration comprises the following features: i) treatment of the catalyst in situ, ii) contacting of the catalyst with water, iii) treatment of the catalyst within a temperature range from 100 to 400° C., iv) treatment of the catalyst within a pressure range from 0.1 to 2 MPa, v) treatment of the catalyst over a period of 0.1 to 24 h, vi) treatment of the catalyst with a specific catalyst hourly space velocity of 0.1 to 100 h−1.
摘要翻译：本发明涉及一种从碱金属和/或碱土金属氧化物，氧化铝和氧化硅组中再生含有混合氧化物的催化剂的方法，其特征在于再生包括以下特征：i）原位处理催化剂，ii）催化剂与水的接触，iii）在100-400℃的温度范围内处理催化剂，iv）在0.1-2MPa的压力范围内处理催化剂，v）处理催化剂在0.1至24小时的时间内，vi）用特定催化剂处理催化剂，小时空速为0.1至100h-1。

5. 发明申请

US20130030233A1 PROCESS FOR OLIGOMERIZING OLEFINS 有权
标题翻译：低聚烯醇的方法
公开(公告)号：US20130030233A1
公开(公告)日：2013-01-31
申请号：US13394827
申请日：2010-08-12
申请人： Christian Boeing , Dietrich Maschmeyer , Markus Winterberg , Stefan Buchholz , Berthold Melcher , Marco Haumann , Peter Wasserscheid
发明人： Christian Boeing , Dietrich Maschmeyer , Markus Winterberg , Stefan Buchholz , Berthold Melcher , Marco Haumann , Peter Wasserscheid
IPC分类号： B01J31/12 , C07C2/34 , B82Y30/00
CPC分类号： C10G50/00 , B01J21/04 , B01J21/066 , B01J21/08 , B01J21/10 , B01J21/18 , B01J21/185 , B01J31/0274 , B01J31/0279 , B01J31/0281 , B01J31/0284 , B01J31/0288 , B01J31/0292 , B01J31/143 , B01J31/2234 , B01J31/2404 , B01J31/26 , B01J35/023 , B01J35/1019 , B01J35/1042 , B01J2231/20 , B01J2231/323 , B01J2531/847 , B82Y30/00 , C07C2/32 , C07C2/36 , C07C2531/24 , C10G2300/1088 , C10G2300/70 , C10G2400/22 , C07C11/02
摘要： The invention provides a catalyst system composed of: a) a support material selected from at least one of the following materials: silicon dioxide, aluminium oxide, magnesium oxide, zirconium oxide and mixed oxides thereof, carbon nanotubes; b) an ionic liquid; c) a catalytically active composition comprising nickel; d) an activator selected from the group of Lewis acids with alkylating properties. Additionally provided is the use of the catalyst systems of the invention in the oligomerization of unsaturated hydrocarbon mixtures.
摘要翻译：本发明提供了一种催化剂体系，该催化剂体系包括：a）选自以下材料中的至少一种的二氧化硅，氧化铝，氧化镁，氧化锆及其混合氧化物的载体材料，碳纳米管; b）离子液体; c）包含镍的催化活性组合物; d）选自具有烷基化性质的路易斯酸的活化剂。另外提供了本发明的催化剂体系在不饱和烃混合物的低聚反应中的用途。

6. 发明授权

US09200216B2 Process for oligomerizing olefins 有权
标题翻译：烯烃低聚方法
公开(公告)号：US09200216B2
公开(公告)日：2015-12-01
申请号：US13394827
申请日：2010-08-12
申请人： Christian Boeing , Dietrich Maschmeyer , Markus Winterberg , Stefan Buchholz , Berthold Melcher , Marco Haumann , Peter Wasserscheid
发明人： Christian Boeing , Dietrich Maschmeyer , Markus Winterberg , Stefan Buchholz , Berthold Melcher , Marco Haumann , Peter Wasserscheid
IPC分类号： C10G50/00 , B01J31/02 , B01J31/14 , B01J31/22 , B01J31/24 , B01J31/26 , B82Y30/00 , C07C2/32 , C07C2/36 , B01J21/04 , B01J21/06 , B01J21/08 , B01J21/10 , B01J21/18 , B01J35/02 , B01J35/10
CPC分类号： C10G50/00 , B01J21/04 , B01J21/066 , B01J21/08 , B01J21/10 , B01J21/18 , B01J21/185 , B01J31/0274 , B01J31/0279 , B01J31/0281 , B01J31/0284 , B01J31/0288 , B01J31/0292 , B01J31/143 , B01J31/2234 , B01J31/2404 , B01J31/26 , B01J35/023 , B01J35/1019 , B01J35/1042 , B01J2231/20 , B01J2231/323 , B01J2531/847 , B82Y30/00 , C07C2/32 , C07C2/36 , C07C2531/24 , C10G2300/1088 , C10G2300/70 , C10G2400/22 , C07C11/02
摘要： The invention provides a catalyst system composed of: a) a support material selected from at least one of the following materials: silicon dioxide, aluminum oxide, magnesium oxide, zirconium oxide and mixed oxides thereof, carbon nanotubes; b) an ionic liquid; c) a catalytically active composition comprising nickel; d) an activator selected from the group of Lewis acids with alkylating properties. Additionally provided is the use of the catalyst systems of the invention in the oligomerization of unsaturated hydrocarbon mixtures.
摘要翻译：本发明提供了一种催化剂体系，该催化剂体系包括：a）选自以下材料中的至少一种的二氧化硅，氧化铝，氧化镁，氧化锆及其混合氧化物的载体材料，碳纳米管; b）离子液体; c）包含镍的催化活性组合物; d）选自具有烷基化性质的路易斯酸的活化剂。另外提供了本发明的催化剂体系在不饱和烃混合物的低聚反应中的用途。

7. 发明申请

US20140194648A1 PROCESS FOR PRODUCING 2-ETHYLHEPTANOIC ACID 审中-公开
标题翻译：生产2-乙酰丙酸的方法
公开(公告)号：US20140194648A1
公开(公告)日：2014-07-10
申请号：US14122041
申请日：2012-05-15
申请人： Christian Boeing , Dietrich Maschmeyer , Markus Winterberg , Michael Grass , Andreas Gevers , Hinnerk Gordon Becker
发明人： Christian Boeing , Dietrich Maschmeyer , Markus Winterberg , Michael Grass , Andreas Gevers , Hinnerk Gordon Becker
IPC分类号： C07C51/09 , C07C67/08
CPC分类号： C07C51/09 , B01J21/04 , B01J23/42 , B01J23/44 , B01J23/755 , B01J35/1019 , C07C67/08 , C08K5/0016 , C08K5/10 , C07C53/128
摘要： Process for producing 2-ethylheptanoic acid.
摘要翻译： 2-乙基庚酸的制备方法。

8. 发明申请

US20140088226A1 DIANHYDROHEXITOL DIESTERS OF 2-ETHYLHEPTANOIC ACID 审中-公开
标题翻译：二乙二醇酸的二氢呋喃糖醇
公开(公告)号：US20140088226A1
公开(公告)日：2014-03-27
申请号：US14119994
申请日：2012-04-26
申请人： Andreas Gevers , Hinnerk Becker , Michael Grass , Markus Winterberg , Dietrich Maschmeyer , Christian Boeing
发明人： Andreas Gevers , Hinnerk Becker , Michael Grass , Markus Winterberg , Dietrich Maschmeyer , Christian Boeing
IPC分类号： C08K5/1535
CPC分类号： C08K5/1535 , C07D493/04 , C08K5/0016 , C08L27/06
摘要： Dianhydrohexitol diesters of 2-ethylheptanoic acid
摘要翻译： 2-乙基庚酸的二氢己糖二酯

9. 发明申请

US20120142985A1 PREPARATION OF ISOBUTENE BY DISSOCIATION OF MTBE 有权
标题翻译：通过MTBE的分离制备ISOBUTEN
公开(公告)号：US20120142985A1
公开(公告)日：2012-06-07
申请号：US13381680
申请日：2010-06-16
申请人： Markus Winterberg , Dirk Roettger , Armin Rix , Reiner Bukohl , Walter Luh , Holger Wiederhold , Gunnar Schilling , Christian Boeing
发明人： Markus Winterberg , Dirk Roettger , Armin Rix , Reiner Bukohl , Walter Luh , Holger Wiederhold , Gunnar Schilling , Christian Boeing
IPC分类号： C07C1/20 , F28F1/00
CPC分类号： C07C11/09 , C07C1/20
摘要： The invention relates to a method for producing isobutene by cracking MTBE, wherein the following steps are carried out: a) MTBE synthesis; reacting isobutene-containing hydrocarbon mixtures (II) with methanol (III), contained in one or more methanol-containing streams (VIII, IX), on acidic ion exchangers obtaining a stream (IV) containing MTBE and TBA, b) MTBE separation; separating a stream (V) containing MTBE and TBA from stream (IV) by means of distillation, c) MTBE cracking; cracking the stream (V) on a heterogenic catalyst in the gas phase, thus obtaining a stream (VI) which contains at least isobutene, methanol, MTBE, water, and optionally TBA, d) isobutene separation; separating the stream (VI) by means of distillation, thus obtaining a stream (VII) containing more than 50 mass % of the amounts of methanol, TBA, and water contained in stream (VI), and a stream (XVII) containing isobutene, e) water separation; separating, water from the stream (VII) to below 1 mass % by means of distillation, thus obtaining a stream (VIII), f) recirculating; complete or partial recirculation of the methanol-containing stream (VIII) into the MTBE synthesis. The invention further relates to a tube bundle device comprising the following elements: i) tube bundle, ii) tube bottom, iii) deflection plates, iv) inner shell, iv) pressure bearing outer shell, comprising at least one inlet and outlet, vi) shell chamber, comprising a fluid releasing or absorbing heat, characterized in that the inner shell is connected to the deflection plates attached over the length of the tube bundle without a gap, or with a small gap, and is connected to the tube bottom, wherein the fluid present in the shell chamber encloses the inner shell on both sides.
摘要翻译：本发明涉及通过裂解MTBE生产异丁烯的方法，其中进行以下步骤：a）MTBE合成; 使含异丁烯的烃混合物（II）与含有一种或多种含甲醇的物流（VIII，IX）中的甲醇（III）在酸性离子交换剂上反应，得到含有MTBE和TBA的物流（Ⅳ），b）MTBE分离; 通过蒸馏从流（IV）分离含有MTBE和TBA的物流（V）; c）MTBE裂解; 在气相中的异源催化剂上裂解物流（V），从而获得至少含有异丁烯，甲醇，MTBE，水和任选的TBA的流（VI），d）异丁烯分离; 通过蒸馏分离料流（VI），从而获得含有大于50质量％的流（VI）中所含的甲醇，TBA和水量的流（VII）和含有异丁烯的料流（XVII） e）水分离; 通过蒸馏从水（VII）中将水分离成低于1质量％，从而获得流（VIII），f）再循环; 将含甲醇的物流（VIII）完全或部分再循环到MTBE合成中。本发明还涉及一种管束装置，其包括以下元件：i）管束，ii）管底，iii）偏转板，iv）内壳，iv）承压外壳，包括至少一个入口和出口，vi ）壳体，其包括释放或吸收热量的流体，其特征在于，所述内壳连接到在所述管束的长度上连接的所述偏转板，而没有间隙或具有小间隙，并且连接到所述管底部，其中存在于壳室中的流体在两侧封闭内壳。

10. 发明授权

US08940951B2 Preparation of isobutene by dissociation of MTBE 有权
标题翻译：通过MTBE离解制备异丁烯
公开(公告)号：US08940951B2
公开(公告)日：2015-01-27
申请号：US13381680
申请日：2010-06-16
申请人： Markus Winterberg , Dirk Roettger , Armin Rix , Reiner Bukohl , Walter Luh , Holger Wiederhold , Gunnar Schilling , Christian Boeing
发明人： Markus Winterberg , Dirk Roettger , Armin Rix , Reiner Bukohl , Walter Luh , Holger Wiederhold , Gunnar Schilling , Christian Boeing
IPC分类号： C07C1/20 , C07C11/09
CPC分类号： C07C11/09 , C07C1/20
摘要： A process for preparing isobutene by dissociation of MTBE, including: a) reaction of isobutene-containing hydrocarbon mixtures, with methanol, present in one or more methanol-containing streams, over acidic ion exchangers to give a stream, containing MTBE and TBA; b) separation of a stream containing MTBE and TBA, from a stream by distillation; c) dissociation of a stream in the gas phase over a heterogeneous catalyst to give a stream containing at least isobutene, methanol, MTBE and water and possibly TBA, d) separation of a stream by distillation to give a stream containing in each case more than 50% by mass of the amounts of methanol, TBA and water present in another stream and a stream containing isobutene, e) separation of water from stream to below 1% by mass by distillation to give a stream, f) total or partial recirculation of the methanol-containing stream.
摘要翻译：一种通过MTBE离解制备异丁烯的方法，包括：a）通过酸性离子交换剂使存在于一个或多个含甲醇的物流中的含异丁烯的烃混合物与甲醇反应，得到含有MTBE和TBA的物流; b）通过蒸馏从流中分离含有MTBE和TBA的物流; c）气相中的物流在非均相催化剂上的解离，得到至少含有异丁烯，甲醇，MTBE和水以及可能的TBA的物流，d）通过蒸馏分离物流，得到含有多于 50重量％的甲醇，TBA和存在于另一个流中的水和含有异丁烯的物流，e）通过蒸馏将水从流分离成低于1质量％，得到流，f）全部或部分再循环含甲醇的流。

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