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1. 发明专利

JPS58213632A Production of alumina 失效
标题翻译：生产铝
公开(公告)号：JPS58213632A
公开(公告)日：1983-12-12
申请号：JP9731682
申请日：1982-06-07
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： ASAOKA SACHIO , SENDOU TAKASHI , NAKAMURA MUNEKAZU
IPC分类号： C01F7/14 , C01F7/34
CPC分类号： C01F7/141 , C01F7/34
摘要： PURPOSE: To produce alumina having uniform primary particles, by repeating the process comprising the heating of an aqueous solution containing seed aluminum hydroxide and the addition of an acid or alkali to the solution, and the process comprising the adjustment of the pH of the solution within a specific range by the addition of an Al-containing neutralizing agent.
CONSTITUTION: An aqueous solution containing aluminum hydroxide forming a seed crystal is maintained at ≥50°C, and mixed with an acid (e.g. nitric acid, sulfuric acid, etc.) or an alkali (e.g. sodium hydroxide) free from precipitating ions under stirring to adjust the pH of the aqueous solution to ≤5 or ≥11. Thereafter, a neutralizing agent containing aluminum (e.g. sodium aluminate, aluminum sulfate, etc.) is added to the solution to adjust the pH to 6W11. The process of adding the acid or alkali and the process of adding the Al-containing neutralizing agent are repeated several times. The formation of secondary nucleus can be prevented, and stable alumina having improved sharpness of the pore size distribution can be obtained by this process.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：通过重复包括加热含有氢氧化铝的水溶液和向溶液中加入酸或碱的方法来生产具有均一的一次颗粒的氧化铝，并且该方法包括调节溶液的pH值通过添加含Al中和剂的特定范围。构成：将含有形成晶种的氢氧化铝的水溶液保持在> = 50℃，并与不含沉淀离子的酸（例如硝酸，硫酸等）或碱（例如氢氧化钠）混合在搅拌下调节水溶液的pH至<= 5或> = 11。此后，向溶液中加入含有铝的中和剂（例如铝酸钠，硫酸铝等），将pH调节至6-11。加入酸或碱的方法和加入含Al中和剂的过程重复几次。可以防止次核的形成，并且可以通过该方法获得具有改善的孔径分布锐度的稳定的氧化铝。

2. 发明专利

JPS61136907A Recovering method of high-purity carbon monoxide 失效
标题翻译：高纯度一氧化碳的回收方法
公开(公告)号：JPS61136907A
公开(公告)日：1986-06-24
申请号：JP25945784
申请日：1984-12-08
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： AZUMA SHUNICHI , ASAOKA SACHIO , KAITA JUN , SUZUKI ISAO
IPC分类号： C01B32/40
摘要： PURPOSE: To recover efficiently high-purity CO by substituting the inside of the narrow pores of porous absorbent absorbent adsorbed with CO by means of the absorbed CO.
CONSTITUTION: After a mixed gas contg. CO is brought into contact with a porous CO absorbent wherein Cu(I) and Al(III) are deposited on a porous inorganic carrier (e.g. porous alumina) to absorb CO selectively, at least the nonabsorbed gas of the inside of the porous narrow pores of the absorbent is substituted with the absorbed CO.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过用吸收的CO代替吸附CO的多孔吸收剂吸收剂吸收剂的内部，有效回收高纯度CO。 CO与多孔CO吸收剂接触，其中Cu（I）和Al（III）沉积在多孔无机载体（例如多孔氧化铝）上以选择性地吸收CO，至少是多孔窄孔内部的未吸收气体的吸收剂被吸收的CO代替。

3. 发明专利

JPS6197121A Method for recovering carbon monoxide 失效
标题翻译：回收一氧化碳的方法
公开(公告)号：JPS6197121A
公开(公告)日：1986-05-15
申请号：JP21725684
申请日：1984-10-18
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： AZUMA SHUNICHI , ASAOKA SACHIO , SUZUKI ISAO , YOSHIDA HARUHIKO , WATABE KOJI
IPC分类号： C01B32/40 , B01J20/02 , B01J20/06
摘要： PURPOSE: To separate economically high purity CO from a gaseous mixture contg. CO by bringing the gaseous mixture into contact with a porous CO absorbent to absorb selectively CO and by desorbing the absorbed CO by evacuation combined with heating.
CONSTITUTION: A porous CO absorbent is manufactured by supporting univalent Cu or univalent Cu and tervalent Al on an inorg. porous body such as porous alumina. A gaseous mixture contg. CO such as exhaust gas from a blast furnace, a coke oven or a converter in an iron mill is brought into contact with the porous CO absorbent to absorb selectively CO. After unabsorbed gas is removed by evacuation, evacuation and heating or heating and evacuation are successively carried out to desorb the absorbed CO from the absorbent. Evacuation and heating may be carried out at the same time. Thus, CO is separated from the gaseous mixture.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：将经济高纯度CO与气体混合物分开。 CO通过使气体混合物与多孔CO吸收剂接触以选择性吸收CO，并通过与加热结合的抽空解吸所吸收的CO。构成：通过在一个inorg上支持一价Cu或一价Cu和三价Al来制造多孔CO吸收剂。多孔体如多孔氧化铝。气体混合物将来自高炉，焦炉或炼铁炉的转炉等CO，CO与多孔CO吸收剂接触，选择性地吸收CO，通过抽真空除去未吸收的气体，抽真空，加热或加热排空先后从吸收剂中解吸吸收的CO。疏散和加热可以同时进行。因此，CO与气体混合物分离。

4. 发明专利

JPS5969424A Manufacture of alumina having low bulk density 失效
标题翻译：具有低体积密度的铝的制造
公开(公告)号：JPS5969424A
公开(公告)日：1984-04-19
申请号：JP17783882
申请日：1982-10-08
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： ASAOKA SACHIO , SENDOU TAKASHI
IPC分类号： C01F7/02 , C01F7/14 , C01F7/34 , C01F7/44
CPC分类号： C01F7/441 , C01F7/02 , C01F7/141 , C01F7/34
摘要： PURPOSE: To manufacture easily and inexpensively alumina powder having a large surface area, a large pore volume and a low bulk density by growing crystals from alumina hydrogel, washing the resulting pseuso boehmite gel in water, and spray-drying and aclcining it.
CONSTITUTION: Aluminum sulfate and/or sodium aluminate as an alumina hydrogel forming substance is added to alumina hydrogel formed at 6W11pH and ≤50°C as seed gel in the presence of sulfuric acid radicals under conditions required to form pseuso boehmite, and crystals are grown to obtain pseuso boehmite gel forming a thinly coagulated body. The resulting gel is well washed in water, spray-dried, and calcined to obtain alumina having 2W5ml/g pore volume, 150W300m
2 /g surface area and 0.10W0.25g/ml bulk density. At 400W800°C calcining temp. γ-alumina is obtd., and at 800W1,100°C δ- or θ-alumina is obtd.
COPYRIGHT: (C)1984,JPO&Japio
摘要翻译：目的：通过从氧化铝水凝胶中生长晶体，通过在水中洗涤所得的水溶性勃姆石凝胶，制造容易且廉价的氧化铝粉末，其表面积大，孔体积大，体积密度低，喷雾干燥和加热。构成：将硫酸铝和/或铝酸钠作为氧化铝水凝胶形成物质添加到在6-11pH和<= 50℃下形成的氧化铝水凝胶中，作为形成pseuso勃姆石所需条件的硫酸根存在下的种子凝胶，并生长晶体以获得形成薄凝结体的pseuso勃姆石凝胶。将所得凝胶在水中充分洗涤，喷雾干燥并煅烧，得到具有2-5ml / g孔体积，150-300m 2 / g表面积和0.10-0.25g / ml堆积密度的氧化铝。煅烧温度400-800℃ 可以看到γ-氧化铝，并且在800-1100℃下可以看到δ-或θ-氧化铝。

5. 发明专利

JPS58190823A Manufacture of alumina carrier 失效
标题翻译：氧化铝载体的制造
公开(公告)号：JPS58190823A
公开(公告)日：1983-11-07
申请号：JP6991182
申请日：1982-04-26
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： ASAOKA SACHIO , SENDOU TAKASHI
IPC分类号： C01F7/14 , B01J21/00 , B01J21/04 , B01J35/10 , C01F7/02 , C01F7/34
CPC分类号： C01F7/02
摘要： PURPOSE: To manufacture an alumina carrier having a regulated pore volume and pore diameter by continuously adding an Alsalt and a pH controller at least one of which contains a sulfate radical to a slurry contg. Al(OH)
3 under conditions under which boehmite crystals are grown to form gel.
CONSTITUTION: A slurry contg. seed Al(OH)
3 is adjusted to 6W11 pH and kept at ≥50°C, and an Al salt and a pH controller are continuously added to the slurry at 20W500mol%/hr rate expressed in terms of Al while keeping the slurry at 6W11 pH. At least one of the Al salt and the pH controller contains practically a sulfate radical. Thus, boehmite gel is formed, and the gel is dried and calcined to manufacture an alumina carrier.
COPYRIGHT: (C)1983,JPO&Japio
摘要翻译：目的：通过连续添加Alsalt和pH控制器来制造具有调节的孔体积和孔径的氧化铝载体，其中至少一个含有硫酸根离子至浆料。在其上生长勃姆石晶体以形成凝胶的条件下，Al（OH）3。构成：将种子Al（OH）3调节至6-11 pH并保持在> = 50℃，并以Al-Al表示的20-500mol％/ hr速率将Al盐和pH控制剂连续加入到浆料中同时保持浆液在6-11 pH。 Al盐和pH控制器中的至少一个实际上含有硫酸根。因此，形成勃姆石凝胶，将凝胶干燥并煅烧以制造氧化铝载体。

6. 发明专利

JPS61138531A Reforming method of carbon monoxide absorbent 失效
标题翻译：一氧化碳吸收剂的改造方法
公开(公告)号：JPS61138531A
公开(公告)日：1986-06-26
申请号：JP26058584
申请日：1984-12-10
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： AZUMA SHUNICHI , ASAOKA SACHIO , KAWAMURA IKUKO , SUZUKI ISAO
IPC分类号： B01D53/14 , B01J20/02 , B01J20/22 , C01B32/40
摘要： PURPOSE: To reform an absorbent so that carbon monoxide is absorbed and separated by the fluctuation of pressure by bringing the carbon monoxide absorbent contg. cuprous chloride, aluminum chloride, an aromatic compd. and a porous body into contact with a polar gas.
CONSTITUTION: A carbon monoxide absorbent consisting of a porous body, cuprous chloride, aluminum chloride and an aromatic compd. is brought into contact with a polar gas such as stream and hydrogen sulfide. The absorbent obtained by this method is reformed so that carbon monoxide is selectively absorbed from a gaseous mixture thereby and carbon monoxide is easily absorbed and separated by the fluctuation pressure.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：改造吸收剂，使一氧化碳吸收并通过使一氧化碳吸收剂受到压力的波动而分离。氯化亚铜，氯化铝，芳香族化合物。和与极性气体接触的多孔体。构成：由多孔体，氯化亚铜，氯化铝和芳香族化合物组成的一氧化碳吸收剂。与极性气体如流和硫化氢接触。通过该方法获得的吸收剂被重整，使得一氧化碳从气态混合物中选择性吸收，一氧化碳容易被波动压力吸收和分离。

7. 发明专利

JPS60191017A Manufacture of ferrierite 失效
标题翻译： FERRIERITE制造
公开(公告)号：JPS60191017A
公开(公告)日：1985-09-28
申请号：JP4290084
申请日：1984-03-08
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： NISHIJIMA HIROAKI , ASAOKA SACHIO , KONDOU TADAMI , SUZUKI ISAO
IPC分类号： C01B33/26 , C01B39/44
CPC分类号： C01B39/445
摘要： PURPOSE:To produce ferrierite effectively with few loads of an organic compound at a comparatively low temp. by adding the specified organic compound and allowing to react each other in manufacture of the ferrierite due to a hydrothermal synthesis method. CONSTITUTION:Tetramethylammonium salt (for example, tetramethylammonium hydroxide) is used as an organic additive. Namely, an alkaline metallic salt (A) (for example, sodium hydroxide), an alumina source (B) (for example, aluminum chloride), a silica source (C) (for example, silica sol) and said organic additive are contained so that the relation shown by the formula (expressed in terms of oxide) (M is alkaline metal; R is an organic additive; a=1.6-5; b>15; c=0.05- 1) is satisfied and an aq. mixture (amount of water is about 100-1,000mol times per 1mol Al2O3) is produced and the aq. mixture is allowed to react with each other by maintaining it at 100-200 deg.C for about one day or more under self- pressure.
摘要翻译：目的：在较低温度下，少量有机化合物有效生产镁碱沸石。通过加入指定的有机化合物，并通过水热合成方法在镁碱沸石的制造中彼此反应。构成：将四甲基铵盐（例如氢氧化四甲基铵）用作有机添加剂。即，含有碱金属盐（A）（例如氢氧化钠），氧化铝源（B）（例如氯化铝），二氧化硅源（C）（例如硅溶胶）和所述有机添加剂）使得由式（以氧化物表示）（M为碱金属; R为有机添加剂; a = 1.6-5; b> 15; c = 0.05-1）表示的关系，混合物（水的量为每1mol Al 2 O 3约100-1,000mol），混合物通过在自压下在100-200℃保持约一天或更长时间使其彼此反应。

8. 发明专利

JPS6197122A Method for absorbing and desorbing carbon nonoxide 失效
标题翻译：吸收和去除碳氧化物的方法
公开(公告)号：JPS6197122A
公开(公告)日：1986-05-15
申请号：JP21725784
申请日：1984-10-18
申请人： Chiyoda Chem Eng & Constr Co Ltd
发明人： AZUMA SHUNICHI , ASAOKA SACHIO , SUZUKI ISAO , YOSHIDA HARUHIKO , WATABE KOJI
IPC分类号： C01B32/40 , B01J20/02 , B01J20/34
摘要： PURPOSE: To separate efficiently and economically high purity CO from a gaseous mixture contg. CO by bringing the gaseous mixture into contact with a porous CO absorbent to absorb selectively CO and by irradiating microwaves to desorb the absorbed CO.
CONSTITUTION: A porous CO absorbent is manufactured by adsorbing and supporting a copper halide such as cuprous chloride and an aluminum halide such as aluminum chloride on a porous inorg. oxide carrier such as porous alumina with an org. solvent. A gaseous mixture contg. CO such as exhaust gas from a blast furnace, a coke oven or a converter in an iron mill is brought into contact with the porous CO absorbent to absorb selectively CO. Microwaves are then irradiated for ≤1min short time preferably under reduced pressure to desorb the absorbed CO from the absorbent by heating. Thus, CO is separated from the gaseous mixture.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：从气体混合物中有效和经济地分离高纯度CO。 CO，通过使气体混合物与多孔CO吸收剂接触以选择性吸收CO，并通过照射微波来解吸所吸收的CO。构成：通过吸附和支持卤化铜如氯化亚铜和卤化铝制造多孔CO吸收剂例如多孔inorg上的氯化铝。氧化物载体，例如具有组织的多孔氧化铝。溶剂。气体混合物将来自高炉，焦炉或炼铁炉的转炉等CO，CO与多孔CO吸收剂接触以选择性地吸收CO。然后，微波在短时间内优选在减压下照射<= 1min以解吸通过加热吸收吸收的CO。因此，CO与气体混合物分离。

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