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1. 发明申请

WO2017048930A1 METHODS OF PREPARING A CATALYST 审中-公开
标题翻译：制备催化剂的方法
公开(公告)号：WO2017048930A1
公开(公告)日：2017-03-23
申请号：PCT/US2016/051902
申请日：2016-09-15
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP
发明人： PRAETORIUS, Jeremy M. , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , CYMBALUK, Ted H. , BOXELL, Conner D , CLEAR, Kathy S , SOLENBERGER, Alan L
IPC分类号： C08F10/02
CPC分类号： B01J23/26 , B01J21/08 , B01J35/1019 , B01J35/1023 , B01J35/1047 , B01J37/0203 , B01J37/0236 , B01J37/08 , C08F10/02 , C08F110/02 , C08F4/22 , C08F4/24 , C08F4/025 , C08F4/16 , C08F2500/12
摘要： A method comprising a) drying a support material comprising silica at temperature in the range of from about 150° C to about 220° C to form a dried support; b) contacting the dried support with methanol to form a slurried support; c) subsequent to b), cooling the slurried support to a temperature of less than about 60° C to form a cooled slurried support; d) subsequent to c), contacting the cooled slurried support with a titanium alkoxide to form a titanated support; and e) thermally treating the titanated support by heating to a temperature of equal to or greater than about 150° C for a time period of from about 5 hours to about 30 hours to remove the methanol and yield a dried titanated support.
摘要翻译：一种方法，包括：a）在约150℃至约220℃的温度范围内干燥包含二氧化硅的载体材料以形成干燥的载体; b）使干燥的载体与甲醇接触以形成浆状载体; c）在b）之后，将所述浆状载体冷却至小于约60℃的温度以形成冷却的浆状载体; d）在c）之后，将冷却的浆状载体与钛醇盐接触以形成钛酸化的载体; 和e）通过加热到等于或大于约150℃的温度约5小时至约30小时的时间来热处理钛酸化的载体以除去甲醇并产生干燥的钛酸化载体。

2. 发明申请

WO2011002497A1 DUAL METALLOCENE CATALYST SYSTEMS FOR DECREASING MELT INDEX AND INCREASING POLYMER PRODUCTION RATES 审中-公开
标题翻译：用于减少熔融指数的双金属催化剂体系和提高聚合物生产率
公开(公告)号：WO2011002497A1
公开(公告)日：2011-01-06
申请号：PCT/US2010/001842
申请日：2010-06-28
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MASINO, Albert P. , MURRAY, Rex E. , YANG, Qing , SECORA, Steven J , JAYARATNE, Kumudini C. , BEAULIEU, William B , DING, Errun , GLASS, Gary L , SOLENBERGER, Alan L , CYMBALUK, Ted H.
发明人： MASINO, Albert P. , MURRAY, Rex E. , YANG, Qing , SECORA, Steven J , JAYARATNE, Kumudini C. , BEAULIEU, William B , DING, Errun , GLASS, Gary L , SOLENBERGER, Alan L , CYMBALUK, Ted H.
IPC分类号： C08F10/00
CPC分类号： C08F4/642 , C08F4/12 , C08F4/52 , C08F4/65904 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08F4/65927 , C08F4/76 , C08F10/00 , C08F110/02 , C08F210/16 , C08F2500/01 , C08F2500/12 , C08F2500/08 , C08F210/14
摘要： The present invention provides dual catalyst systems and polymerization processes employing these dual catalyst systems. The disclosed polymerization processes can produce olefin polymers at higher production rates, and these olefin polymers may have a higher molecular weight and/or a lower melt index.
摘要翻译：本发明提供了使用这些双重催化剂体系的双重催化剂体系和聚合方法。公开的聚合方法可以以更高的生产速率生产烯烃聚合物，并且这些烯烃聚合物可以具有较高的分子量和/或较低的熔体指数。

3. 发明申请

WO2014164614A1 METHOD FOR THE PREPARATION OF POLYMERIZATION CATALYSTS 审中-公开
标题翻译：聚合催化剂的制备方法
公开(公告)号：WO2014164614A1
公开(公告)日：2014-10-09
申请号：PCT/US2014/023009
申请日：2014-03-11
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MCDANIEL, Max P , COLLINS, Kathy S , SCHWERDTFEGER, Eric D , SOLENBERGER, Alan L
发明人： MCDANIEL, Max P , COLLINS, Kathy S , SCHWERDTFEGER, Eric D , SOLENBERGER, Alan L
IPC分类号： C08F10/00
CPC分类号： C08F4/22 , C08F10/00 , C08F4/24 , C08F4/025 , C08F110/02 , C08F2500/12
摘要： A method comprising contacting a support material with a transition metal compound to produce a mixture; thermally treating the mixture in the presence of oxygen at a temperature in a range of from about 100° C to about 500° C for a period of from about 1 hour to about 10 hours, wherein at least a portion of the transition metal sublimes onto the support material to produce a support material comprising a dispersed transition metal; and thermally treating the support material comprising the dispersed transition metal in an oxidizing atmosphere at a temperature in a range of from about 550° C to about 900° C for a period of from about 1 hour to about 10 hours to produce a polymerization catalyst.
摘要翻译：一种方法，包括使支撑材料与过渡金属化合物接触以产生混合物; 在氧气存在下，在约100℃至约500℃的温度范围内热处理混合物约1小时至约10小时，其中至少一部分过渡金属升华到用于生产包含分散的过渡金属的载体材料的载体材料; 并在包含分散的过渡金属的载体材料的氧化气氛中在约550℃至约900℃的温度范围内热处理约1小时至约10小时，以制备聚合催化剂。

4. 发明申请

WO2013081826A1 LONG CHAIN BRANCHED POLYMERS AND METHODS OF MAKING SAME 审中-公开
标题翻译：长链分支聚合物及其制备方法
公开(公告)号：WO2013081826A1
公开(公告)日：2013-06-06
申请号：PCT/US2012/064986
申请日：2012-11-14
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
发明人： YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , COLLINS, Kathy S
IPC分类号： C08F110/02
CPC分类号： C08F110/02 , B01J23/26 , B01J35/1009 , B01J35/1014 , B01J35/1019 , C08F10/02 , C08F210/02 , C08F2500/04 , C08F2500/09 , C08F4/69 , C08F4/025
摘要： A polymer having a long chain branching content peaking at greater than about 20 long chain branches per million carbon atoms, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 8 long chain branches per million carbon atoms, a polydispersity index of greater than about 20 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 1 long chain branches per chain, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution.
摘要翻译：具有长链支化含量高于每百万个碳原子大于约20个长支链的聚合物，多分散指数大于约10，其中长链支化在分子量的较高分子量部分下降至约零分配。具有长链支化含量高于每百万个碳原子大于约8个长链分支的聚合物，多分散指数大于约20，其中长链支化在分子量分布的较高分子量部分下降至约零。具有长链支化含量在每链大于约1个长链分支峰值的聚合物，以及多分散指数大于约10，其中长链支链在分子量分布的较高分子量部分下降至约零。

5. 发明申请

WO2011002498A1 THE USE OF HYDROGEN SCAVENGING CATALYSTS TO CONTROL POLYMER MOLECULAR WEIGHT AND HYDROGEN LEVELS IN A POLYMERIZATION REACTOR 审中-公开
标题翻译：使用氢气加压催化剂控制聚合反应器中的聚合物分子量和氢含量
公开(公告)号：WO2011002498A1
公开(公告)日：2011-01-06
申请号：PCT/US2010/001843
申请日：2010-06-28
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP , MURRAY, Rex E. , BEAULIEU, William B. , YANG, Qing , DING, Errun , GLASS, Gary L , SOLENBERGER, Alan L , SECORA, Steven J.
发明人： MURRAY, Rex E. , BEAULIEU, William B. , YANG, Qing , DING, Errun , GLASS, Gary L , SOLENBERGER, Alan L , SECORA, Steven J.
IPC分类号： C08F10/00 , C08F2/38
CPC分类号： C08F210/14 , C08F4/65904 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F10/00 , C08F210/02 , C08F210/08 , C08F210/16 , C08F2410/03 , C08F2420/00 , C08F2420/02 , Y10S526/943 , C08F4/65925 , C08F4/65927 , C08F2/38 , C08F2500/12 , C08F2500/01 , C08F2500/08 , C08F4/70 , C08F4/545
摘要： The present invention provides dual catalyst systems containing a metallocene catalyst and a hydrogen scavenging catalyst, and polymerization processes employing these dual catalyst systems. Due to a reduction in hydrogen levels in the polymerization processes, olefin polymers produced from these polymerization processes may have a higher molecular weight, a lower melt index, and higher levels of unsaturation.
摘要翻译：本发明提供了含有茂金属催化剂和除氢催化剂的双重催化剂体系，以及采用这些双重催化剂体系的聚合方法。由于聚合过程中氢含量的降低，由这些聚合方法制备的烯烃聚合物可能具有较高的分子量，较低的熔体指数和更高的不饱和度。

6. 发明申请

WO2018064050A3 METHODS OF PREPARING A CATALYST 审中-公开
标题翻译：制备催化剂的方法
公开(公告)号：WO2018064050A3
公开(公告)日：2018-04-05
申请号：PCT/US2017/053468
申请日：2017-09-26
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP
发明人： MCDANIEL, Max P , SCHWERDTFEGER, Eric D , PRAETORIUS, Jeremy M. , SOLENBERGER, Alan L , CLEAR, Kathy S
IPC分类号： C08F4/16 , C08F4/22 , C08F4/02 , C08F10/02
摘要： A method of preparing a catalyst comprising a) contacting (i) a silica- support, (ii) an oxotitanium compound, (iii) a chromium-containing compound, and (iv) an optional solvent to form a first aqueous mixture comprising a pre-catalyst and a reaction media having from 1 wt.% to 99 wt.% water; b) thermally treating the pre-catalyst by heating to a temperature of from 400 °C to 1000 °C for a time period of from 1 minute to 24 hours to form the catalyst. A method of preparing a catalyst comprising contacting a hydrated support material comprising silica with a chromium-containing compound to form a first aqueous mixture comprising a chrominated support; contacting the first aqueous mixture comprising a chrominated support with a solution comprising (i) a solvent and (ii) an oxotitanium compound to form a second aqueous mixture comprising a pre- catalyst; and thermally treating the pre-catalyst to form the catalyst.
摘要翻译：（i）二氧化硅载体，（ii）氧钛化合物，（iii）含铬化合物和（iv）任选的溶剂的催化剂的制备方法，所述方法包括：a）形成包含预催化剂和具有1重量％至99重量％水的反应介质的第一含水混合物; b）通过加热至400℃至1000℃的温度1分钟至24小时来热处理预催化剂以形成催化剂。一种制备催化剂的方法，包括使包含二氧化硅的水合载体材料与含铬化合物接触以形成包含着色载体的第一含水混合物; 使包含着色载体的第一含水混合物与包含（i）溶剂和（ii）氧钛化合物的溶液接触以形成包含预催化剂的第二含水混合物; 并热处理预催化剂以形成催化剂。

7. 发明申请

WO2018064050A2 METHODS OF PREPARING A CATALYST 审中-公开
标题翻译：制备催化剂的方法
公开(公告)号：WO2018064050A2
公开(公告)日：2018-04-05
申请号：PCT/US2017/053468
申请日：2017-09-26
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP
发明人： MCDANIEL, Max P , SCHWERDTFEGER, Eric D , PRAETORIUS, Jeremy M. , SOLENBERGER, Alan L , CLEAR, Kathy S
IPC分类号： C08F4/16 , C08F4/22 , C08F4/02 , C08F10/02
CPC分类号： C08F110/02 , C08F10/02 , C08F4/22 , C08F4/16 , C08F4/025 , C08F2500/04 , C08F2500/12 , C08F210/16 , C08F210/14
摘要： A method of preparing a catalyst comprising a) contacting (i) a silica-support, (ii) an oxotitanium compound, (iii) a chromium-containing compound, and (iv) an optional solvent to form a first aqueous mixture comprising a pre-catalyst and a reaction media having from about 1 wt.% to about 99 wt.% water; b) thermally treating the pre-catalyst by heating to a temperature of from about 400 C to about 1000 C for a time period of from about 1 minute to about 24 hours to form the catalyst. A method of preparing a catalyst comprising contacting a hydrated support material comprising silica with a chromium-containing compound to form a first aqueous mixture comprising a chrominated support; contacting the first aqueous mixture comprising a chrominated support with a solution comprising (i) a solvent and (ii) an oxotitanium compound to form a second aqueous mixture comprising a pre-catalyst; and thermally treating the pre-catalyst to form the catalyst.
摘要翻译：（i）二氧化硅 - 载体，（ii）氧钛化合物，（iii）含铬化合物和（iv）任选的溶剂的催化剂的制备方法，该方法包括：a）形成包含预催化剂和具有约1重量％至约99重量％水的反应介质的第一含水混合物; b）通过加热至约400℃至约1000℃的温度热处理预催化剂约1分钟至约24小时的时间以形成催化剂。一种制备催化剂的方法，包括使包含二氧化硅的水合载体材料与含铬化合物接触以形成包含着色载体的第一含水混合物; 使包含着色载体的第一含水混合物与包含（i）溶剂和（ii）氧钛化合物的溶液接触以形成包含预催化剂的第二含水混合物; 并热处理预催化剂以形成催化剂。

8. 发明申请

WO2016176189A1 METHODS OF PREPARING A CATALYST 审中-公开
标题翻译：制备催化剂的方法
公开(公告)号：WO2016176189A1
公开(公告)日：2016-11-03
申请号：PCT/US2016/029327
申请日：2016-04-26
申请人： CHEVRON PHILLIPS CHEMICAL COMPANY LP
发明人： PRAETORIUS, Jeremy M. , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , CYMBALUK, Ted H. , BOXELL, Conner D , CLEAR, Kathy S , SOLENBERGER, Alan L
IPC分类号： C08F10/02 , C08F4/24 , C08F4/02
CPC分类号： C08F110/02 , C08F10/02 , C08F4/24 , C08F4/025 , C08F2500/12
摘要： A method comprising a) calcining a silica support at temperature in the range of from about 100 °C to about 500 °C to form a precalcined silica support; b) contacting the precalcined silica support with a titanium alkoxide to form a titanated support; c) subsequent to b), contacting the titanated support with a polyol to form a polyol associated titanated support (PATS); d) contacting at least one of the silica support, pre-calcined silica support, the titanated support, the PATS, or combinations thereof with a chromium-containing compound to form a polymerization catalyst precursor; e) drying the polymerization catalyst precursor to form a dried polymerization catalyst precursor; and f) calcining the dried polymerization catalyst precursor to produce a polymerization catalyst, wherein less than about 0.1 wt.% of a highly reactive volatile organic compound (HRVOC) is emitted during the calcining of the dried polymerization catalyst precursor.
摘要翻译：一种方法，包括a）在约100℃至约500℃的温度范围内煅烧二氧化硅载体以形成预煅烧二氧化硅载体; b）使预煅烧的二氧化硅载体与钛醇盐接触以形成钛酸化的载体; c）在b）之后，使钛酸化的载体与多元醇接触以形成多元醇相关的钛化载体（PATS）; d）将二氧化硅载体，预煅烧二氧化硅载体，钛化载体，PATS或其组合中的至少一种与含铬化合物接触以形成聚合催化剂前体; e）干燥聚合催化剂前体以形成干燥的聚合催化剂前体; 和f）煅烧所述干燥的聚合催化剂前体以产生聚合催化剂，其中在干燥的聚合催化剂前体的煅烧过程中发射小于约0.1重量％的高反应性挥发性有机化合物（HRVOC）。

9. 发明授权

EP3288985B1 METHODS OF PREPARING A CATALYST 有权
公开(公告)号：EP3288985B1
公开(公告)日：2020-04-15
申请号：EP16728426.4
申请日：2016-04-26
申请人： Chevron Phillips Chemical Company LP
发明人： PRAETORIUS, Jeremy M. , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , CYMBALUK, Ted H. , BOXELL, Conner D , CLEAR, Kathy S , SOLENBERGER, Alan L
IPC分类号： C08F10/02 , C08F4/24 , C08F4/02

10. 发明公开

EP3246345A1 LONG CHAIN BRANCHED POLYMERS AND METHODS OF MAKING SAME 审中-公开
标题翻译：长链支化聚合物及其制备方法
公开(公告)号：EP3246345A1
公开(公告)日：2017-11-22
申请号：EP17180324.0
申请日：2012-11-14
申请人： Chevron Phillips Chemical Company LP
发明人： YU, Youlu , SCHWERDTFEGER, Eric D , MCDANIEL, Max P , SOLENBERGER, Alan L , CLEAR, Kathy S
IPC分类号： C08F110/02
CPC分类号： C08F110/02 , B01J23/26 , B01J35/1009 , B01J35/1014 , B01J35/1019 , C08F10/02 , C08F210/02 , C08F2500/04 , C08F2500/09 , C08F4/69 , C08F4/025
摘要： A polymer having a long chain branching content peaking at greater than about 1 long chain branches per chain, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 20 long chain branches per million carbon atoms, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution.
摘要翻译：具有长链支化含量的聚合物在每个链上峰值大于约1个长链分支，并且多分散指数大于约10，其中长链支化在分子量分布的较高分子量部分下降到大约零。长链支化含量峰值高于约20个长链支链/百万个碳原子的聚合物，以及大于约10的多分散指数，其中长链支化在分子量的较高分子量部分下降到大约零分配。

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