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1. 发明授权

US07910040B2 Manufacturing process of conductive polymer composite bipolar plate for fuel cell having high gas permeability-resistance and heat-resistance 有权
标题翻译：具有高耐气体渗透性和耐热性的用于燃料电池的导电聚合物复合双极板的制造方法
公开(公告)号：US07910040B2
公开(公告)日：2011-03-22
申请号：US11175141
申请日：2005-07-07
申请人： Chen-Chi Martin Ma , Hsu-Chiang Kuan , Han-Lang Wu , Hsun-Yu Su , Shu-Hang Liao , Chuan-Yu Yen , Yu-Feng Lin , Ying-Ying Cheng
发明人： Chen-Chi Martin Ma , Hsu-Chiang Kuan , Han-Lang Wu , Hsun-Yu Su , Shu-Hang Liao , Chuan-Yu Yen , Yu-Feng Lin , Ying-Ying Cheng
IPC分类号： H01M4/64
CPC分类号： B29C70/025 , B29C70/60 , B29C70/882 , B29L2031/3468
摘要： A composite bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein carbon fiber 1-20 wt %, modified organo clay or noble metal plated modified organo clay 0.5-10 wt %, and one or more conductive fillers selected form: carbon nanotube (CNT) 0.1-5 wt %, nickel plated carbon fiber 0.5-10 wt %, nickel plated graphite 2.5-40 wt %, and carbon black 2-30 wt %, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) to form a bipolar plate having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：用于聚合物电解质膜燃料电池（PEMFC）的复合双极板如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量为60重量％至95重量％基于石墨粉末和乙烯基酯的总重量，其中碳纤维1-20重量％，改性有机粘土或贵金属镀覆的改性有机粘土为0.5-10重量％，以及一种或多种选自以下形式的导电填料：碳纳米管（ CNT）0.1-5重量％，镀镍碳纤维0.5-10重量％，镀镍石墨2.5-40重量％，碳黑2-30重量％，基于乙烯基酯树脂的重量，在复合 b）从步骤a）模制BMC材料，以形成在80-200℃和500-4000psi下具有所需成形的双极板。

2. 发明申请

US20060267235A1 Manufacturing process of conductive polymer composite bipolar plate for fuel cell having high gas permeability-resistance and heat-resistance 有权
标题翻译：具有高耐气体渗透性和耐热性的用于燃料电池的导电聚合物复合双极板的制造方法
公开(公告)号：US20060267235A1
公开(公告)日：2006-11-30
申请号：US11175141
申请日：2005-07-07
申请人： Chen-Chi Ma , Hsu-Chiang Kuan , Han-Lang Wu , Hsun-Yu Su , Shu-Hang Liao , Chuan-Yu Yen , Yu-Feng Lin , Ying-Ying Cheng
发明人： Chen-Chi Ma , Hsu-Chiang Kuan , Han-Lang Wu , Hsun-Yu Su , Shu-Hang Liao , Chuan-Yu Yen , Yu-Feng Lin , Ying-Ying Cheng
IPC分类号： B29C70/88
CPC分类号： B29C70/025 , B29C70/60 , B29C70/882 , B29L2031/3468
摘要： A composite bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein carbon fiber 1-20 wt %, modified organo clay or noble metal plated modified organo clay 0.5-10 wt %, and one or more conductive fillers selected form: carbon nanotube (CNT) 0.1-5 wt %, nickel plated carbon fiber 0.5-10 wt %, nickel plated graphite 2.5-40 wt %, and carbon black 2-30 wt %, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) to form a bipolar plate having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：用于聚合物电解质膜燃料电池（PEMFC）的复合双极板如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量为60重量％至95重量％基于石墨粉末和乙烯基酯的总重量，其中碳纤维1-20重量％，改性有机粘土或贵金属镀覆的改性有机粘土为0.5-10重量％，以及一种或多种选自以下形式的导电填料：碳纳米管 CNT）0.1-5重量％，镀镍碳纤维0.5-10重量％，镀镍石墨2.5-40重量％，碳黑2-30重量％，基于乙烯基酯树脂的重量，在复合 b）从步骤a）模制BMC材料，以形成在80-200℃和500-4000psi下具有所需成形的双极板。

3. 发明授权

US07883650B2 Fabrication of carbon nanotubes reinforced polymer composite bipolar plates for fuel cell 有权
标题翻译：用于燃料电池的碳纳米管增强聚合物复合双极板的制造
公开(公告)号：US07883650B2
公开(公告)日：2011-02-08
申请号：US12289046
申请日：2008-10-20
申请人： Chen-Chi Martin Ma , Chih-Hung Hung , Shu-Hang Liao , Chuan-Yu Yen , Jeng-Chih Weng , Yu-Feng Lin
发明人： Chen-Chi Martin Ma , Chih-Hung Hung , Shu-Hang Liao , Chuan-Yu Yen , Jeng-Chih Weng , Yu-Feng Lin
IPC分类号： C04B35/00
CPC分类号： H01B1/24 , H01M8/0213 , H01M8/0221 , H01M8/0226 , Y10S977/745 , Y10S977/748
摘要： A composite bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein carbon nanotubes together with a polyether amine dispersant or modified carbon nanotubes 0.05-10 wt %, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) to form a bipolar plates having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：用于聚合物电解质膜燃料电池（PEMFC）的复合双极板如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量为60重量％至95重量％基于石墨粉末和乙烯基酯的总重量，其中在配混期间加入碳纳米管与聚醚胺分散剂或基于乙烯基酯树脂重量0.05-10重量％的改性碳纳米管; b）将步骤a）中的BMC材料模制成在80-200℃和500-4000psi下具有所需成形的双极板。

4. 发明申请

US20100059718A1 Fabrication of carbon nanotubes reinforced polymer composite bipolar plates for fuel cell 有权
标题翻译：用于燃料电池的碳纳米管增强聚合物复合双极板的制造
公开(公告)号：US20100059718A1
公开(公告)日：2010-03-11
申请号：US12289046
申请日：2008-10-20
申请人： Chen-Chi Martin Ma , Chih-Hung Hung , Shu-Hang Liao , Chuan-Yu Yen , Jeng-Chih Weng , Yu-Feng Lin
发明人： Chen-Chi Martin Ma , Chih-Hung Hung , Shu-Hang Liao , Chuan-Yu Yen , Jeng-Chih Weng , Yu-Feng Lin
IPC分类号： H01B1/24
CPC分类号： H01B1/24 , H01M8/0213 , H01M8/0221 , H01M8/0226 , Y10S977/745 , Y10S977/748
摘要： A composite bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein carbon nanotubes together with a polyether amine dispersant or modified carbon nanotubes 0.05-10 wt %, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) to form a bipolar plates having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：用于聚合物电解质膜燃料电池（PEMFC）的复合双极板如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量为60重量％至95重量％基于石墨粉末和乙烯基酯的总重量，其中在配混期间加入碳纳米管与聚醚胺分散剂或基于乙烯基酯树脂重量0.05-10重量％的改性碳纳米管; b）将步骤a）中的BMC材料模制成在80-200℃和500-4000psi下具有所需成形的双极板。

5. 发明授权

US09202635B2 Composite substrate for counter electrode of dye-sensitized solar cell 有权
标题翻译：染料敏化太阳能电池对电极复合基片
公开(公告)号：US09202635B2
公开(公告)日：2015-12-01
申请号：US12588379
申请日：2009-10-14
申请人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
发明人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
IPC分类号： H01L31/02 , H01G9/20 , B82Y10/00 , B82Y30/00 , C08J3/20 , C08J5/00 , C08J5/04 , H01L51/44
CPC分类号： H01G9/2022 , B82Y10/00 , B82Y30/00 , C08J3/203 , C08J5/005 , C08J5/04 , C08J2367/02 , H01G9/2031 , H01G9/2059 , H01L51/444 , Y02E10/542
摘要： A substrate for counter electrode of dye-sensitized solar cell is made of a composite material, which is prepared by: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein 0.01-10 wt % of an electrically conductive filler, based on the weight of the vinyl ester resin, is optionally added during the compounding; b) molding the BMC material from step a) to form a substrate for the counter electrode having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：染料敏化太阳能电池对电极基板由复合材料制成，该复合材料通过以下方法制备：a）将乙烯基酯和石墨粉末复合以形成批量模塑料（BMC）材料，石墨粉末含量为60wt％相对于石墨粉末和乙烯基酯的总重量为95重量％，其中在配混期间任选加入基于乙烯基酯树脂重量的0.01-10重量％的导电填料; b）从步骤a）模制BMC材料，以形成在80-200℃和500-4000psi下具有所需成型的对电极的基材。

6. 发明申请

US20100154871A1 Composite substrate for counter electrode of dye-sensitized solar cell 有权
标题翻译：染料敏化太阳能电池对电极复合基片
公开(公告)号：US20100154871A1
公开(公告)日：2010-06-24
申请号：US12588379
申请日：2009-10-14
申请人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
发明人： Chen-Chi Martin Ma , Chuan-Yu Yen , Shu-Hang Liao , Ming-Yu Yen , Min-Chien Hsiao
IPC分类号： H01L31/02 , C08J5/00 , B29B13/00
CPC分类号： H01G9/2022 , B82Y10/00 , B82Y30/00 , C08J3/203 , C08J5/005 , C08J5/04 , C08J2367/02 , H01G9/2031 , H01G9/2059 , H01L51/444 , Y02E10/542
摘要： A substrate for counter electrode of dye-sensitized solar cell is made of a composite material, which is prepared by: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein 0.01-10 wt % of an electrically conductive filler, based on the weight of the vinyl ester resin, is optionally added during the compounding; b) molding the BMC material from step a) to form a substrate for the counter electrode having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：染料敏化太阳能电池对电极基板由复合材料制成，该复合材料通过以下方法制备：a）将乙烯基酯和石墨粉末复合以形成批量模塑料（BMC）材料，石墨粉末含量为60wt％相对于石墨粉末和乙烯基酯的总重量为95重量％，其中在配混期间任选加入基于乙烯基酯树脂重量的0.01-10重量％的导电填料; b）从步骤a）模制BMC材料，以形成在80-200℃和500-4000psi下具有所需成型的对电极的基材。

7. 发明申请

US20100269270A1 Preparation of a nanocomposite photoanode for dye-sensitized solar cells 审中-公开
标题翻译：制备用于染料敏化太阳能电池的纳米复合光电阳极
公开(公告)号：US20100269270A1
公开(公告)日：2010-10-28
申请号：US12458809
申请日：2009-07-23
申请人： Chen-Chi M. Ma , Chuan-Yu Yen , Yu-Feng Lin , Shu-Hang Liao
发明人： Chen-Chi M. Ma , Chuan-Yu Yen , Yu-Feng Lin , Shu-Hang Liao
IPC分类号： D06P5/00
CPC分类号： H01G9/2031 , H01G9/2059 , Y02E10/542
摘要： A process for preparing a photoanode of dye-sensitized solar cells (DSSCs) is disclosed, which contains nano TiO2 and functionalized carbon nanomateiral. The process includes reacting a dispersion of functionalized carbon nanomateiral and a TiO2 precursor in a liquid organic medium under sol-gel conditions to form a carbon nanomaterial/nano TiO2 composite colloidal solution; mixing with an aqueous polymer solution, and forming a paste suitable for coating by concentrating the resulting mixture; coating the paste on a conductive glass substrate and calcining the coated layer at 300-520° C. in air for 10-60 minutes to obtain a conductive glass plate having a coating of nanocomposite, which can be used to prepare a photoanode of DSSCs by immersing in a dye solution to adsorb a dye thereon.
摘要翻译：公开了一种制备染料敏化太阳能电池（DSSC）的光电阳极的方法，其包含纳米TiO 2和官能化的碳纳米材料。该方法包括在溶胶 - 凝胶条件下使官能化的碳纳米材料和TiO2前体的分散体在液体有机介质中反应形成碳纳米材料/纳米TiO2复合胶体溶液; 与聚合物水溶液混合，并通过浓缩所得混合物形成适于涂覆的浆料; 将该糊状物涂布在导电性玻璃基板上，在空气中在300〜520℃下煅烧涂布层10〜60分钟，得到具有纳米复合材料的导电性玻璃板，其可用于制备DSSC的光电阳极浸渍在染料溶液中以吸附染料。

8. 发明申请

US20100127424A1 Fabrication of metal meshes/carbon nanotubes/polymer composite bipolar plates for fuel cell 审中-公开
标题翻译：用于燃料电池的金属网/碳纳米管/聚合物复合双极板的制造
公开(公告)号：US20100127424A1
公开(公告)日：2010-05-27
申请号：US12457353
申请日：2009-06-09
申请人： Chen-Chi Martin Ma , Min-Chien Hsiao , Shu-Hang Liao , Ming-Yu Yen , Chaun-Yu Yen , Jeng-Chin Weng , Shuo-Jen Lee
发明人： Chen-Chi Martin Ma , Min-Chien Hsiao , Shu-Hang Liao , Ming-Yu Yen , Chaun-Yu Yen , Jeng-Chin Weng , Shuo-Jen Lee
IPC分类号： B29C51/42
CPC分类号： H01M8/0234 , H01M8/0239 , H01M8/0243 , H01M2008/1095
摘要： A reinforced mesh structure containing bipolar plate for a polymer electrolyte membrane fuel cell (PEMFC) is prepared as follows: a) compounding vinyl ester and graphite powder to form bulk molding compound (BMC) material, the graphite powder content ranging from 60 wt % to 95 wt % based on the total weight of the graphite powder and vinyl ester, wherein 0.05-10 wt % reactive carbon nanotubes modified by acyl chlorination-amidization reaction, based on the weight of the vinyl ester resin, are added during the compounding; b) molding the BMC material from step a) with a metallic net being embedded in the molded BMC material to form a bipolar plates having a desired shaped at 80-200° C. and 500-4000 psi.
摘要翻译：含有用于聚合物电解质膜燃料电池（PEMFC）的双极板的增强网格结构如下制备：a）将乙烯基酯和石墨粉末混合以形成本体模塑料（BMC）材料，石墨粉末含量范围为60wt％至基于石墨粉末和乙烯基酯的总重量为95重量％，其中在配混期间加入基于乙烯基酯树脂的重量，通过酰基氯化酰胺化反应改性的0.05-10重量％的反应性碳纳米管; b）将来自步骤a）的BMC材料模制成金属网嵌入到模制的BMC材料中以形成在80-200℃和500-4000psi下具有所需成形的双极板。

9. 发明申请

US20100283174A1 Fabrication of polymer grafted carbon nanotubes/polypropylene composite bipolar plates for fuel cell 审中-公开
标题翻译：用于燃料电池的聚合物接枝碳纳米管/聚丙烯复合双极板的制备
公开(公告)号：US20100283174A1
公开(公告)日：2010-11-11
申请号：US12591026
申请日：2009-11-05
申请人： Chen-Chi Martin Ma , Min-Chien Hsiao , Shu-Hang Liao , Jeng-Chih Weng , Shuo-Jen Lee , Ay Su
发明人： Chen-Chi Martin Ma , Min-Chien Hsiao , Shu-Hang Liao , Jeng-Chih Weng , Shuo-Jen Lee , Ay Su
IPC分类号： B29C43/02
CPC分类号： H01M8/0226 , B29C43/003 , B29C2043/025 , H01M8/0213 , H01M8/0221 , H01M2008/1095
摘要： A composite bipolar plate for a proton exchange membrane fuel cell (PEMFC) is prepared as follows: a) melt compounding a polypropylene resin and graphite powder to form a melt compounding material, the graphite powder content ranging from 50 wt % to 95 wt % based on the total weight of the melt compounding material and the polypropylene resin being a homopolymer of propylene or a random copolymer of propylene and ethylene, butylenes or hexalene, wherein 0.01-15 wt % of polymer-grafted carbon nanotubes by an acyl chlorination-amidization reaction, based on the weight of the polypropylene resin, are added during the compounding; and b) molding the melt compounding material from step a) to form a bipolar plates having a desired shaped at 100-250° C. and 500-4000 psi.
摘要翻译：用于质子交换膜燃料电池（PEMFC）的复合双极板如下制备：a）将聚丙烯树脂和石墨粉末熔融混合以形成熔融混合材料，石墨粉末含量为基于50重量％至95重量％关于熔融配混材料和聚丙烯树脂是丙烯均聚物或丙烯与乙烯，丁烯或六烯的无规共聚物的总重量，其中通过酰氯酰胺化反应制备聚合物接枝的碳纳米管的0.01-15重量％基于聚丙烯树脂的重量，在配混期间加入; 和b）从步骤a）模制熔融混合材料，以形成在100-250℃和500-4000psi下具有所需成型的双极板。

10. 发明申请

US20100127428A1 Fabrication of carbon nanotubes reinforced semi-crystalline polymer composite bipolar plates for fuel cell 审中-公开
标题翻译：用于燃料电池的碳纳米管增强半结晶聚合物复合双极板的制造
公开(公告)号：US20100127428A1
公开(公告)日：2010-05-27
申请号：US12458649
申请日：2009-07-20
申请人： Chen-Chi M. Ma , Shu-Hang Liao , Chuan-Yu Yen , Cheng-Chih Weng , Ching-Hung Yang , Ming-Yu Yen , Min-Chien Hsiao , Shuo-Jen Lee , Yi-Hsiu Hsiao
发明人： Chen-Chi M. Ma , Shu-Hang Liao , Chuan-Yu Yen , Cheng-Chih Weng , Ching-Hung Yang , Ming-Yu Yen , Min-Chien Hsiao , Shuo-Jen Lee , Yi-Hsiu Hsiao
IPC分类号： C08L23/12 , C08L23/14 , C08K3/04 , B29C45/00 , B29C43/02
CPC分类号： B29C45/0013 , B29B2009/125 , B29C43/003 , B29K2023/12 , B29K2105/16 , B29K2105/167 , B29K2303/04 , B29K2503/04 , B29L2031/3468 , C08L23/10 , H01M8/0213 , H01M8/0221 , H01M8/0226 , H01M2008/1095
摘要： A composite bipolar plate for a polymer electrolyte membrane membrane fuel cell (PEMFC) is prepared as follows: a) melt compounding a polypropylene resin and graphite powder at 100-250° C. and 30-150 rpm to form a melt compounding material, the graphite powder content ranging from 50 wt % to 95 wt % based on the total weight of the graphite powder and the polypropylene resin, and the polypropylene resin being a homopolymer of propylene or a copolymer of propylene and ethylene, wherein 0.05-20 wt % carbon nanotubes, based on the weight of the polypropylene resin, are added during the melt compounding; and b) molding the melt compounding material from step a) to form a bipolar plate having a desired shaped at 100-250° C. and 500-4000 psi.
摘要翻译：用于聚合物电解质膜式燃料电池（PEMFC）的复合双极板如下制备：a）在100-250℃和30-150rpm下将聚丙烯树脂和石墨粉末熔融混合以形成熔融配混材料，基于石墨粉末和聚丙烯树脂的总重量，石墨粉末含量为50重量％至95重量％，聚丙烯树脂为丙烯均聚物或丙烯与乙烯的共聚物，其中0.05-20重量％的碳在熔融配混过程中加入基于聚丙烯树脂重量的纳米管; 和b）从步骤a）模制熔融配混材料以形成在100-250℃和500-4000psi下具有所需成型的双极板。

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