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1. 发明授权

US07622621B2 Preparation of alkylaromatic hydrocarbons and alkylaryl sulfonates 失效
标题翻译：烷基芳烃和烷基芳基磺酸盐的制备
公开(公告)号：US07622621B2
公开(公告)日：2009-11-24
申请号：US10509508
申请日：2003-03-28
申请人： Carolyn B. Duncan , David Wayne Turner , Jane C. Cheng , Charles M. Yarbrough , Raphael Frans Caers , Ramzi Y. Saleh , James L. Propp
发明人： Carolyn B. Duncan , David Wayne Turner , Jane C. Cheng , Charles M. Yarbrough , Raphael Frans Caers , Ramzi Y. Saleh , James L. Propp
IPC分类号： C07C2/66 , C07C2/12
CPC分类号： C07C2/66 , C07C15/107 , C07C303/06 , C07C2527/1206 , C07C2527/126 , C07C2527/173 , C07C2529/70 , C07C309/31
摘要： In a process for preparing an alkylaromatic hydrocarbon composition an olefinic hydrocarbon mixture and an aromatic compound are contacted under alkylation conditions with an aromatic alkylation catalyst selected from a homogeneous acid catalyst and heterogeneous acid catalyst comprising a molecular sieve having an X-ray diffraction pattern including d-spacing maxima at 12.4±0.25, 6.9±0.15, 3.57±0.07 and 3.42±0.07 Angstroms. The olefinic hydrocarbon mixture comprises at least 5 wt % by weight of mono-olefin oligomers of the empirical formula: CnH2n wherein n is greater than or equal to 10, the mono-olefin oligomers comprising at least 20 percent by weight of olefins having at least 12 carbon atoms, and the olefins having at least 12 carbon atoms having an average of from 0.8 to 2.0 C1-C3 alkyl branches per carbon chain. Sulfonation of the alkylaromatic hydrocarbon product produces an alkylaryl sulfonate mixture that exhibits advantageous properties, such as biodegradability and hard and cold water performance.
摘要翻译：在制备烷基芳族烃组合物的方法中，烯烃混合物和芳族化合物在烷基化条件下与选自均相酸催化剂的芳族烷基化催化剂和包含具有包括d的X射线衍射图的分子筛的多相酸催化剂接触最大值为12.4±0.25,6.9±0.15,3.57±0.07和3.42±0.07埃。烯烃混合物包含至少5重量％的经验式为C n H 2n的单烯烃低聚物，其中n大于或等于10，单烯烃低聚物包含至少20重量％的至少具有至少20重量％ 12个碳原子，并且具有至少12个碳原子的烯烃在每个碳链上平均具有0.8至2.0个C 1 -C 3烷基支链。烷基芳族烃产物的磺化产生显示出有利性质的烷基芳基磺酸盐混合物，例如生物降解性和冷水和冷水性能。

2. 发明申请

US20100022802A1 Preparation of Alkylaromatic Hydrocarbons and Alkylaryl Sulfonates 失效
标题翻译：烷基芳烃和烷基芳基磺酸盐的制备
公开(公告)号：US20100022802A1
公开(公告)日：2010-01-28
申请号：US12575948
申请日：2009-10-08
申请人： Carolyn B. Duncan , David Wayne Turner , Jane C. Cheng , Charles M. Yarbrough , Raphael Frans Caers , Ramzi Y. Saleh , James L. Propp
发明人： Carolyn B. Duncan , David Wayne Turner , Jane C. Cheng , Charles M. Yarbrough , Raphael Frans Caers , Ramzi Y. Saleh , James L. Propp
IPC分类号： C07C315/00 , C07C15/00
CPC分类号： C07C2/66 , C07C15/107 , C07C303/06 , C07C2527/1206 , C07C2527/126 , C07C2527/173 , C07C2529/70 , C07C309/31
摘要： An alkylaromatic hydrocarbon composition prepared by the process which comprises oligomerizing an olefin selected from the group consisting of propylene, n-butene and mixtures thereof over an oligomerization catalyst, to form a oligomerization product comprising at least 95% by weight of mono-olefin oligomers of the empirical formula: CnH2n wherein n is greater than or equal to 10, the mono-olefin oligomers comprise at least 20% by weight of olefins having at least 12 carbon atoms, and the olefins having at least 12 carbon atoms having an average of from 0.8 to 2.0 C1-C3 alkyl branches per carbon chain. Sulfonation of the alkylaromatic hydrocarbon product produces an alkylaryl sulfonate mixture that exhibits advantageous properties, such as biodegradability and hard and cold water performance.
摘要翻译：通过该方法制备的烷基芳族烃组合物，其包括在低聚催化剂上使选自丙烯，正丁烯及其混合物的烯烃低聚，形成低聚产物，其包含至少95重量％的单烯烃低聚物经验式：C n H 2n其中n大于或等于10，单烯烃低聚物包含至少20重量％的具有至少12个碳原子的烯烃，并且具有至少12个碳原子的烯烃具有平均为每个碳链0.8至2.0个C1-C3烷基支链。烷基芳族烃产物的磺化产生显示出有利性质的烷基芳基磺酸盐混合物，例如生物降解性和冷水和冷水性能。

3. 发明授权

US08183420B2 Preparation of alkylaromatic hydrocarbons and alkylaryl sulfonates 失效
标题翻译：烷基芳烃和烷基芳基磺酸盐的制备
公开(公告)号：US08183420B2
公开(公告)日：2012-05-22
申请号：US12575948
申请日：2009-10-08
申请人： Carolyn B. Duncan , David Wayne Turner , Jane C. Cheng , Charles M. Yarbrough , Raphael Frans Caers , Ramzi Y. Saleh , James L. Propp
发明人： Carolyn B. Duncan , David Wayne Turner , Jane C. Cheng , Charles M. Yarbrough , Raphael Frans Caers , Ramzi Y. Saleh , James L. Propp
IPC分类号： C07C15/107
CPC分类号： C07C2/66 , C07C15/107 , C07C303/06 , C07C2527/1206 , C07C2527/126 , C07C2527/173 , C07C2529/70 , C07C309/31
摘要： An alkylaromatic hydrocarbon composition prepared by the process which comprises oligomerizing an olefin selected from the group consisting of propylene, n-butene and mixtures thereof over an oligomerization catalyst, to form a oligomerization product comprising at least 95% by weight of mono-olefin oligomers of the empirical formula: CnH2n wherein n is greater than or equal to 10, the mono-olefin oligomers comprise at least 20% by weight of olefins having at least 12 carbon atoms, and the olefins having at least 12 carbon atoms having an average of from 0.8 to 2.0 C1-C3 alkyl branches per carbon chain. Sulfonation of the alkylaromatic hydrocarbon product produces an alkylaryl sulfonate mixture that exhibits advantageous properties, such as biodegradability and hard and cold water performance.
摘要翻译：通过该方法制备的烷基芳族烃组合物，其包括在低聚催化剂上使选自丙烯，正丁烯及其混合物的烯烃低聚以形成低聚产物，其包含至少95重量％的单烯烃低聚物经验式：C n H 2n其中n大于或等于10，单烯烃低聚物包含至少20重量％的具有至少12个碳原子的烯烃，并且具有至少12个碳原子的烯烃具有平均为每个碳链0.8至2.0个C1-C3烷基支链。烷基芳族烃产物的磺化产生显示出有利性质的烷基芳基磺酸盐混合物，例如生物降解性和冷水和冷水性能。

4. 发明授权

US07425662B2 Oligomerization of olefins 有权
标题翻译：烯烃的低聚
公开(公告)号：US07425662B2
公开(公告)日：2008-09-16
申请号：US10509356
申请日：2003-03-28
申请人： Jon E. Stanat , Georges M. K. Mathys , David Wayne Turner , Jane C. Cheng , Stephen W. Beadle , Cesar M. Cheng Guajardo , Roger Eijkhoudt , Allen D. Godwin , Ernest E. Green , Charles M. Yarbrough , Raphael Frans Caers , Carolyn B. Duncan , Ramzi Y. Saleh
发明人： Jon E. Stanat , Georges M. K. Mathys , David Wayne Turner , Jane C. Cheng , Stephen W. Beadle , Cesar M. Cheng Guajardo , Roger Eijkhoudt , Allen D. Godwin , Ernest E. Green , Charles M. Yarbrough , Raphael Frans Caers , Carolyn B. Duncan , Ramzi Y. Saleh
IPC分类号： C07C2/20
CPC分类号： C07C2/64 , C07C2/12 , C07C45/28 , C07C51/16 , C07C2529/70 , C08F10/00 , C08F210/10 , C10G50/00 , C10M129/68 , C10M129/95 , C10M2207/28 , C11D1/667 , C11D3/2093 , C07C15/107 , C08F4/12 , C08F4/18 , C08F2500/02
摘要： A selectivated molecular sieve, e.g., ZSM-22 or ZSM-23, is used as olefin oligomerization catalyst to provide product, e.g., octenes and dodecenes from butene, having a low degree of branching and hindered double bonds.
摘要翻译：使用选择性分子筛，例如ZSM-22或ZSM-23作为烯烃低聚催化剂，以提供具有低支化度和受阻双键的产物，例如丁烯中的辛烯和十二碳烯。

5. 发明授权

US07507868B2 Olefin oligomerization process 失效
标题翻译：烯烃低聚方法
公开(公告)号：US07507868B2
公开(公告)日：2009-03-24
申请号：US10509530
申请日：2003-03-28
申请人： Carolyn B. Duncan , Raphael Frans Caers , David W. Turner , Michael J. Keenan , Ernest E. Green , Ramzi Y. Saleh
发明人： Carolyn B. Duncan , Raphael Frans Caers , David W. Turner , Michael J. Keenan , Ernest E. Green , Ramzi Y. Saleh
IPC分类号： C07C2/12
CPC分类号： C07C303/06 , C07B37/02 , C07C2/12 , C07C2/66 , C07C29/16 , C07C2529/70 , C07C15/107 , C07C31/125 , C07C309/31
摘要： In a process for oligomerizing a C2 to C6 n-olefin feedstock over surface deactivated ZSM-23, the feedstock contains from about 0.1 wt % to about 25 wt % of an iso-olefin and the C12+ fraction of the oligomerized olefin product contains less than 0.5 atom % of quaternary carbon atoms.
摘要翻译：在通过表面失活的ZSM-23使C2至C6-烯烃原料低聚的方法中，原料含有约0.1wt％至约25wt％的异烯烃，并且低聚烯烃产物的C12 +馏分含有少于 0.5原子％的季碳原子。

6. 发明授权

US07148388B2 Process for preparing and olefinic hydrocarbon mixture 有权
标题翻译：制备烯烃混合物的方法
公开(公告)号：US07148388B2
公开(公告)日：2006-12-12
申请号：US10508982
申请日：2003-03-28
申请人： Stephen W. Beadle , Cesar M. Cheng-Guajardo , Carolyn B. Duncan , David Wayne Turner , Ramzi Y. Saleh
发明人： Stephen W. Beadle , Cesar M. Cheng-Guajardo , Carolyn B. Duncan , David Wayne Turner , Ramzi Y. Saleh
IPC分类号： C07C2/66 , C07C2/68 , C07C2/70 , C07C29/16 , C07C309/31
CPC分类号： C07B37/02 , C07C2/12 , C07C29/16 , C07C303/06 , C07C2529/70 , C07C309/31 , C07C31/02
摘要： In a process for preparing an olefinic hydrocarbon mixture comprising at least 5% by weight of mono-olefin oligomers of the empirical formula: CnH2n where n is greater than or equal to 6, a feedstock comprising n-butene and propylene in a molar ratio of about 1:0.01 to about 1:0.49 is contacted under oligomerization conditions with surface deactivated ZSM-23. The resultant mono-olefin oligomers comprise at least 20 percent by weight of olefins having at least 12 carbon atoms, wherein said olefins having at least 12 carbon atoms have an average of from about 0.8 to about 2.0 C1–C3 alkyl branches per carbon chain.
摘要翻译：在制备包含至少5重量％经验式的单烯烃低聚物的烯烃混合物的方法中：<？in-line-formula description =“In-line Formulas”end =“lead”→> α-in-line-formula description =“In-line Formulas”end =“tail”？>其中n大于或等于6，原料包括正丁烯和摩尔比约1:0.01至约1:0.49的丙烯在低聚条件下与表面失活的ZSM-23接触。所得的单烯烃低聚物包含至少20重量％的具有至少12个碳原子的烯烃，其中所述具有至少12个碳原子的烯烃具有平均约0.8至约2.0C 1 -C 3 -C 3烷基支链。

7. 发明授权

US08859821B2 Polyketone plasticizers 有权
标题翻译：聚酮增塑剂
公开(公告)号：US08859821B2
公开(公告)日：2014-10-14
申请号：US13345014
申请日：2012-01-06
申请人： Allen D. Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
发明人： Allen D. Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
IPC分类号： C07C45/00 , C07C45/27 , C08L101/00 , C08G67/00 , C08G67/02 , C08L73/00
CPC分类号： C08G67/02 , C08L73/00 , C08L101/00 , C08L2666/14
摘要： The invention relates to polyketone compounds and the at least partially hydrogenated products thereof, the use of said polyketone compounds and/or the at least partially hydrogenated products thereof as plasticizers, processes of making polyketone compounds and the at least partially hydrogenated products thereof, compositions comprising the polyketone compounds and/or the at least partially hydrogenated products thereof, and to articles formed from products of the invention.
摘要翻译：本发明涉及聚酮化合物及其至少部分氢化的产物，所述聚酮化合物和/或其至少部分氢化产物作为增塑剂的用途，制备聚酮化合物的方法及其至少部分氢化的产物，包含聚酮化合物和/或其至少部分氢化的产物，以及由本发明的产物形成的制品。

8. 发明申请

US20080242895A1 Polyketone Plasticizers 失效
标题翻译：聚酮增塑剂
公开(公告)号：US20080242895A1
公开(公告)日：2008-10-02
申请号：US12058397
申请日：2008-03-28
申请人： Allen D. Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
发明人： Allen D. Godwin , Kenneth J. Buturla , Karla S. Colle , Gabor Kiss , Kirk C. Nadler , Abhimanyu O. Patil , Edris Eileen Pike , Ramzi Y. Saleh , Jon E. Stanat , Manika Varma-Nair , Stephen Zushma
IPC分类号： C07C45/27
CPC分类号： C08G67/02 , C08L73/00 , C08L101/00 , C08L2666/14
摘要： The invention relates to polyketone compounds and the at least partially hydrogenated products thereof, the use of said polyketone compounds and/or the at least partially hydrogenated products thereof as plasticizers, processes of making polyketone compounds and the at least partially hydrogenated products thereof, compositions comprising the polyketone compounds and/or the at least partially hydrogenated products thereof, and to articles formed from products of the invention.
摘要翻译：本发明涉及聚酮化合物及其至少部分氢化的产物，所述聚酮化合物和/或其至少部分氢化产物作为增塑剂的用途，制备聚酮化合物的方法及其至少部分氢化的产物，包含聚酮化合物和/或其至少部分氢化的产物，以及由本发明的产物形成的制品。

9. 发明授权

US5453561A Reactive separation process 失效
标题翻译：反应分离过程
公开(公告)号：US5453561A
公开(公告)日：1995-09-26
申请号：US187673
申请日：1994-01-27
申请人： Ramzi Y. Saleh , Michael Siskin , Glen B. Brons , Stephen N. Vaughn , Richard H. Schlosberg
发明人： Ramzi Y. Saleh , Michael Siskin , Glen B. Brons , Stephen N. Vaughn , Richard H. Schlosberg
IPC分类号： B01D17/025 , C07C7/148 , C07C11/02 , C07C29/10 , C10G50/00 , C07C7/00
CPC分类号： C07C29/10 , C07C7/148
摘要： The invention concerns a method for reactive separation of mixtures containing hydrocarbons and oxygenated hydrocarbons, by contacting a mixture of hydrocarbons such as C.sub.2 to C.sub.26 hydrocarbons and mixtures thereof and oxygenated hydrocarbons, such as C.sub.2 to C.sub.40 oxygenated hydrocarbons and mixtures thereof to form a mixture of hydrocarbons and lower molecular weight oxygenated hydrocarbons and heating the mixture in water at temperature typically from about and pressure sufficient to cleave the oxygenated hydrocarbons to lower molecular weight products to form a liquid layer containing water soluble reaction products and an organic layer containing primarily hydrocarbons.
摘要翻译：本发明涉及通过使烃类混合物例如C 2至C 26烃及其混合物和含氧烃如C2至C40含氧烃及其混合物的混合物与烃和氧化烃的混合物进行反应分离的方法，以形成混合物碳氢化合物和较低分子量的氧化烃，并将混合物在水中加热，其温度通常为足以将氧化烃切割成较低分子量产物的温度，形成含有水溶性反应产物和主要含有烃的有机层的液体层。

10. 发明授权

US5169824A Catalyst comprising amorphous NiO on silica/alumina support 失效
标题翻译：包含在二氧化硅/氧化铝载体上的无定形NiO的催化剂
公开(公告)号：US5169824A
公开(公告)日：1992-12-08
申请号：US644998
申请日：1991-01-22
申请人： Ramzi Y. Saleh , Stuart L. Soled , Nicholas C. Dispenziere
发明人： Ramzi Y. Saleh , Stuart L. Soled , Nicholas C. Dispenziere
IPC分类号： B01J23/755 , B01J37/02 , B01J37/03
CPC分类号： B01J37/0217 , B01J23/755 , B01J37/031
摘要： The present invention provides for a catalyst composition which is effective for use in the production of dimer products and higher olefin products from lower olefins such as propylene and butene in high yields and with an average degree of branching in the dimer products of less than about 1.6 methyl groups per molecule, generally in the range of from about 1.0 to 1.4 methyl groups per molecule. The present invention also provides a process for producing such dimer and higher olefin products using the catalyst composition of this invention. The catalyst of the invention comprises an amorphous nickel oxide (NiO) present as a disperse substantial monolayer on the surfaces of a silica (SiO.sub.2) support, which support also contains minor amounts of an oxide of aluminum, gallium or indium such that the ratio of NiO to metal oxide present in the catalyst is within the range of from about 4:1 to about 100:1. The catalyst may be prepared by precipitating a water insoluble nickel salt onto the surfaces of a silica support which has been impregnated with the metal oxide or onto a silica-alumina support which has been dealuminized such that the resulting nickel oxide/alumina ratio will fall within the ranges set forth above. The catalyst may then be activated by calcination in the presence of oxygen at a temperature within the range of from about 500.degree. to 700.degree. C.
摘要翻译：本发明提供了一种催化剂组合物，其有效用于以高产率从低级烯烃如丙烯和丁烯生产二烯体产物和高级烯烃产物，并且二聚体产物中的平均支化度小于约1.6 每个分子的甲基基团，通常在每分子约1.0至1.4个甲基的范围内。本发明还提供了使用本发明的催化剂组合物生产这种二聚物和较高级烯烃产物的方法。本发明的催化剂包括在二氧化硅（SiO 2）载体的表面上作为分散实质单层存在的无定形氧化镍（NiO），该载体还含有少量的铝，镓或铟的氧化物，存在于催化剂中的NiO与金属氧化物在约4:1至约100:1的范围内。催化剂可以通过将水不溶性镍盐沉淀到已经浸渍有金属氧化物的二氧化硅载体的表面上或已经脱铝的二氧化硅 - 氧化铝载体上，使得所得到的氧化镍/氧化铝比落入上述范围。催化剂然后可以在氧的存在下在约500-700℃的温度下煅烧来活化。

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