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1. 发明授权

US5122305A Solid-state radiation-emitting compositions and devices 失效
标题翻译：固态辐射发射组合物和装置
公开(公告)号：US5122305A
公开(公告)日：1992-06-16
申请号：US495580
申请日：1990-03-20
申请人： Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Timothy J. Shepodd , Leroy E. Leonard , Robert E. Ellefson , John T. Gill , Robert J. Walko , Clifford L. Renschler
发明人： Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Timothy J. Shepodd , Leroy E. Leonard , Robert E. Ellefson , John T. Gill , Robert J. Walko , Clifford L. Renschler
IPC分类号： C09K11/04 , G21H3/02
CPC分类号： C09K11/04 , G21H3/02
摘要： The invention relates to a composition for the volumetric generation of radiation, wherein a first substance functions as a source of exciting radiation, and a second substance interacts with the exciting radiation to provide a second radiation. The compositions comprise a porous substrate which is loaded with: a source of exciting radiation, a component capable of emitting radiation upon interaction with the exciting radiation, or both. In the composition, a composite is formed from a carrier material and at least one of the source of the exciting radiation or the component which is capable of interacting with the exciting radiation. The composite is then employed for loading a porous substrate, preferably an aerogel substrate.
摘要翻译：本发明涉及一种用于辐射体积产生的组合物，其中第一物质用作激发辐射源，第二物质与激发辐射相互作用以提供第二辐射。组合物包括多孔基底，其加载有：激发辐射源，能够与激发辐射相互作用时发射辐射的成分，或两者。在组合物中，由载体材料和能够与激发辐射相互作用的激发辐射源或组分中的至少一个形成复合材料。然后将复合材料用于装载多孔基材，优选气凝胶基质。

2. 发明授权

US5078919A Composition containing aerogel substrate loaded with tritium 失效
标题翻译：含有装载有氚的气凝胶基质的组合物
公开(公告)号：US5078919A
公开(公告)日：1992-01-07
申请号：US495578
申请日：1990-03-20
申请人： Carol S. Ashley , C. Jeffrey Brinker , Robert E. Ellefson , John T. Gill , Scott Reed , Robert J. Walko
发明人： Carol S. Ashley , C. Jeffrey Brinker , Robert E. Ellefson , John T. Gill , Scott Reed , Robert J. Walko
IPC分类号： C09K11/04
CPC分类号： C09K11/04
摘要： The invention provides a process for loading an aerogel substrate with tritium and the resultant compositions. According to the process, an aerogel substrate is hydrolyzed so that surface OH groups are formed. The hydrolyzed aerogel is then subjected to tritium exchange employing, for example, a tritium-containing gas, whereby tritium atoms replace H atoms of surface OH groups. OH and/or CH groups of residual alcohol present in the aerogel may also undergo tritium exchange.
摘要翻译：本发明提供了一种用氚填充气凝胶基质和所得组合物的方法。根据该方法，将气凝胶基材水解，形成表面OH基。然后使用例如含氚气体对水解气凝胶进行氚交换，由此氚原子代替表面OH基团的H原子。存在于气凝胶中的OH和/或CH基的残余醇也可以进行氚交换。

3. 发明授权

US5240647A Process for making solid-state radiation-emitting composition 失效
标题翻译：制备固态发射辐射的组合物的方法
公开(公告)号：US5240647A
公开(公告)日：1993-08-31
申请号：US753470
申请日：1991-09-03
申请人： Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Robert J. Walko
发明人： Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Robert J. Walko
IPC分类号： C09K11/04
CPC分类号： C09K11/04
摘要： The invention provides a process for loading an aerogel substrate with tritium and the resultant compositions. According to the process, an aerogel substrate is hydrolyzed so that surface OH groups are formed. The hydrolyzed aerogel is then subjected to tritium exchange employing, for example, a tritium-containing gas, whereby tritium atoms replace H atoms of surface OH groups. OH and/or CH groups of residual alcohol present in the aerogel may also undergo tritium exchange.
摘要翻译：本发明提供了一种用氚填充气凝胶基质和所得组合物的方法。根据该方法，将气凝胶基材水解，形成表面OH基。然后使用例如含氚气体对水解气凝胶进行氚交换，由此氚原子代替表面OH基团的H原子。存在于气凝胶中的OH和/或CH基的残余醇也可以进行氚交换。

4. 发明授权

US5306445A Inorganic volumetric light source excited by ultraviolet light 失效
标题翻译：紫外线激发的无机体光源
公开(公告)号：US5306445A
公开(公告)日：1994-04-26
申请号：US884445
申请日：1992-05-18
申请人： Scott Reed , Robert J. Walko , Carol S. Ashley , C. Jeffrey Brinker
发明人： Scott Reed , Robert J. Walko , Carol S. Ashley , C. Jeffrey Brinker
IPC分类号： C09K11/04 , G21G4/00
CPC分类号： C09K11/04
摘要： The invention relates to a composition for the volumetric generation of radiation. The composition comprises a porous substrate loaded with a component capable of emitting radiation upon interaction with an exciting radiation. Preferably, the composition is an aerogel substrate loaded with a component, e.g., a phosphor, capable of interacting with exciting radiation of a first energy, e.g., ultraviolet light, to produce radiation of a second energy, e.g., visible light.
摘要翻译：本发明涉及用于辐射体积产生的组合物。所述组合物包含负载有与激发辐射相互作用时能够发射辐射的组分的多孔基材。优选地，组合物是装载有能够与例如紫外光的第一能量的激发辐射相互作用的组分（例如磷光体）的气凝胶基质，以产生例如可见光的第二能量的辐射。

5. 发明授权

US5313485A Luminescent light source for laser pumping and laser system containing same 失效
标题翻译：用于激光泵浦的发光光源和含有激光泵浦的激光系统
公开(公告)号：US5313485A
公开(公告)日：1994-05-17
申请号：US966473
申请日：1992-10-26
申请人： Roy A. Hamil , Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Robert J. Walko
发明人： Roy A. Hamil , Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Robert J. Walko
IPC分类号： H01S3/0915
CPC分类号： H01S3/0915
摘要： The invention relates to a pumping lamp for use with lasers comprising a porous substrate loaded with a component capable of emitting light upon interaction of the component with exciting radiation and a source of exciting radiation. Preferably, the pumping lamp comprises a source of exciting radiation, such as an electron beam, and an aerogel or xerogel substrate loaded with a component capable of interacting with the exciting radiation, e.g., a phosphor, to produce light, e.g., visible light, of a suitable band width and of a sufficient intensity to generate a laser beam from a laser material.
摘要翻译：本发明涉及一种与激光一起使用的泵浦灯，其包括多孔基底，该多孔基底装载有能够在激发辐射与激发辐射源相互作用时发光的部件。优选地，泵浦灯包括诸如电子束的激发辐射源，以及装载有能够与激发辐射例如磷光体相互作用的部件的气凝胶或干凝胶基底，以产生光，例如可见光，具有合适的带宽和足够的强度以产生来自激光材料的激光束。

6. 发明授权

US5137659A Solid-state radiation-emitting compositions and devices 失效
标题翻译：固态辐射发射组合物和装置
公开(公告)号：US5137659A
公开(公告)日：1992-08-11
申请号：US495579
申请日：1990-03-20
申请人： Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Robert J. Walko
发明人： Carol S. Ashley , C. Jeffrey Brinker , Scott Reed , Robert J. Walko
IPC分类号： C09K11/04
CPC分类号： C09K11/04
摘要： The invention relates to a composition for the volumetric generation of radiation, wherein a first substance functions as a source of exciting radiation, and a second substance interacts with the exciting radiation to provide a second radiation. The compositions comprise a porous substrate which is loaded with: a source of exciting radiation, a component capable of emitting radiation upon interaction with the exciting radiation, or both. Preferably, the composition is an aerogel substrate loaded with both a source of exciting radiation, such as tritium, and a component capable of interacting with the exciting radiation, e.g., a phosphor, to produce radiation of a second energy.
摘要翻译：本发明涉及一种用于辐射体积产生的组合物，其中第一物质用作激发辐射源，第二物质与激发辐射相互作用以提供第二辐射。组合物包括多孔基底，其加载有：激发辐射源，能够与激发辐射相互作用时发射辐射的成分，或两者。优选地，组合物是装载有诸如氚的激发辐射源的气凝胶基质和能够与激发的辐射（例如磷光体）相互作用以产生第二能量的辐射的成分。

7. 发明授权

US6057377A Molecular receptors in metal oxide sol-gel materials prepared via molecular imprinting 有权
标题翻译：通过分子印迹制备的金属氧化物溶胶 - 凝胶材料中的分子受体
公开(公告)号：US6057377A
公开(公告)日：2000-05-02
申请号：US183848
申请日：1998-10-30
申请人： Darryl Y. Sasaki , C. Jeffrey Brinker , Carol S. Ashley , Charles E. Daitch , Kenneth J. Shea , Daniel J. Rush
发明人： Darryl Y. Sasaki , C. Jeffrey Brinker , Carol S. Ashley , Charles E. Daitch , Kenneth J. Shea , Daniel J. Rush
IPC分类号： C03C1/00 , C03C3/06 , C03C3/00 , B01D21/01 , C03C14/00 , G01N31/00
CPC分类号： C03C1/006 , C03C3/06 , C03C2203/28 , C03C2203/52 , Y10T436/10
摘要： A method is provided for molecularly imprinting the surface of a sol-gel material, by forming a solution comprised of a sol-gel material, a solvent, an imprinting molecule, and a functionalizing siloxane monomer of the form Si(OR).sub.3-n X.sub.n, wherein n is an integer between zero and three and X is a functional group capable of reacting with the imprinting molecule, evaporating the solvent, and removing the imprinting molecule to form the molecularly imprinted metal oxide sol-gel material. The use of metal oxide sol-gels allows the material porosity, pore size, density, surface area, hardness, electrostatic charge, polarity, optical density, and surface hydrophobicity to be tailored and be employed as sensors and in catalytic and separations operations.
摘要翻译：提供了通过形成由溶胶 - 凝胶材料，溶剂，印迹分子和Si（OR）3-nXn形式的官能化硅氧烷单体组成的溶液来分子印刷溶胶 - 凝胶材料的表面的方法其中n是0和3之间的整数，X是能够与压印分子反应的官能团，蒸发溶剂，以及去除压印分子以形成分子印迹的金属氧化物溶胶 - 凝胶材料。使用金属氧化物溶胶凝胶允许定制材料孔隙率，孔径，密度，表面积，硬度，静电电荷，极性，光密度和表面疏水性，并用作传感器和催化分离操作。

8. 发明授权

US06495352B1 Sol-gel method for encapsulating molecules 有权
标题翻译：用于封装分子的溶胶 - 凝胶法
公开(公告)号：US06495352B1
公开(公告)日：2002-12-17
申请号：US09548638
申请日：2000-04-13
申请人： C. Jeffrey Brinker , Carol S. Ashley , Rimple Bhatia , Anup K. Singh
发明人： C. Jeffrey Brinker , Carol S. Ashley , Rimple Bhatia , Anup K. Singh
IPC分类号： C12N1114
CPC分类号： C12N11/14 , Y10S436/815 , Y10S436/829
摘要： A method for encapsulating organic molecules, and in particular, biomolecules using sol-gel chemistry. A silica sol is prepared from an aqueous alkali metal silicate solution, such as a mixture of silicon dioxide and sodium or potassium oxide in water. The pH is adjusted to a suitably low value to stabilize the sol by minimizing the rate of siloxane condensation, thereby allowing storage stability of the sol prior to gelation. The organic molecules, generally in solution, is then added with the organic molecules being encapsulated in the sol matrix. After aging, either a thin film can be prepared or a gel can be formed with the encapsulated molecules. Depending upon the acid used, pH, and other processing conditions, the gelation time can be from one minute up to several days. In the method of the present invention, no alcohols are generated as by-products during the sol-gel and encapsulation steps. The organic molecules can be added at any desired pH value, where the pH value is generally chosen to achieve the desired reactivity of the organic molecules. The method of the present invention thereby presents a sufficiently mild encapsulation method to retain a significant portion of the activity of the biomolecules, compared with the activity of the biomolecules in free solution.
摘要翻译：一种封装有机分子的方法，特别是使用溶胶 - 凝胶化学的生物分子。二氧化硅溶胶由碱金属硅酸盐水溶液如二氧化硅和氧化钠在水中的混合物制备。通过使硅氧烷缩合的速度最小化，将pH调节到适当的低值以稳定溶胶，由此允许在凝胶化之前溶胶的储存稳定性。然后通常在溶液中的有机分子加入被包封在溶胶基质中的有机分子。老化后，可以制备薄膜或用封装的分子形成凝胶。根据使用的酸，pH和其他加工条件，凝胶化时间可以从一分钟到几天。在本发明的方法中，在溶胶 - 凝胶和包封步骤期间不产生作为副产物的醇。有机分子可以以任何所需的pH值加入，其中通常选择pH值以实现有机分子的所需反应性。因此，与游离溶液中的生物分子的活性相比，本发明的方法提供了足够温和的包封方法以保持生物分子的活性的显着部分。

9. 发明申请

US20200276286A1 SILICIFIED CELL REPLICAS, METHODS OF MAKING, AND METHODS OF USING 审中-公开
公开(公告)号：US20200276286A1
公开(公告)日：2020-09-03
申请号：US16647245
申请日：2018-09-13
申请人： Rita E. Serda , C. Jeffrey Brinker , Jacob Ongudi Agola , Jimin Guo , Sarah Adams , STC.UNM
发明人： Rita E. Serda , C. Jeffrey Brinker , Jacob Ongudi Agola , Jimin Guo , Sarah Adams
IPC分类号： A61K39/00 , A61K39/39
摘要： A silicified cell replica includes a silicified cell or a silicified subcellular fragment. The silicified cell replica may be used to induce an immunological response, treat a bacterial infection, or treat a patient with cancer.

10. 发明申请

US20180344641A1 MESOPOROUS SILICA NANOPARTICLES AND SUPPORTED LIPID BI-LAYER NANOPARTICLES FOR BIOMEDICAL APPLICATIONS 审中-公开
公开(公告)号：US20180344641A1
公开(公告)日：2018-12-06
申请号：US15757269
申请日：2016-09-02
申请人： C. Jeffrey Brinker , Paul N. Durfee , Jason Townson , Yu-Shen Lin , Stanley Shihyao Chou , Jacob Erstling
发明人： C. Jeffrey Brinker , Paul N. Durfee , Jason Townson , Yu-Shen Lin , Stanley Shihyao Chou , Jacob Erstling
IPC分类号： A61K9/127 , A61K47/62 , A61K47/69 , A61P31/14 , A61P35/02
CPC分类号： A61K9/1271 , A61K9/5146 , A61K47/62 , A61K47/6923 , B82Y5/00 , B82Y40/00
摘要： The present disclosure is directed to methods of producing monosized protocells from monosized mesoporous silica nanoparticles (mMSNPs) and their use for targeted drug delivery formulations and systems and for biomedical applications. The present disclosure is also directed in part to a multilamellar or unilamellar protocell vaccine to deliver full length viral protein and/or plasmid encoded viral protein to antigen presenting cells (APCs) in order to induce an immunogenic response to a virus.

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