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1. 发明申请

WO2007054953A1 IMPROVED PROCESS FOR THE RECOVERY OF SULPHATE OF POTASH (SOP) FROM SULPHATE RICH BITTERN 审中-公开
标题翻译：改善磷酸氢盐（SOP）从硫酸氢盐中恢复的改进方法
公开(公告)号：WO2007054953A1
公开(公告)日：2007-05-18
申请号：PCT/IN2005/000441
申请日：2005-12-27
申请人： COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH , PAUL, Parimal , GHOSH, Pushpito Kumar , LANGALIA, Kaushik Jethalal , SUBRAMANIAN, Palani Sivagnana , ERINGATHODI, Suresh , PATRA, Subrata , AGNIHOTRI, Pragati
发明人： PAUL, Parimal , GHOSH, Pushpito Kumar , LANGALIA, Kaushik Jethalal , SUBRAMANIAN, Palani Sivagnana , ERINGATHODI, Suresh , PATRA, Subrata , AGNIHOTRI, Pragati
IPC分类号： C01D5/00 , C05D1/02
CPC分类号： C05D1/02 , C01D3/06 , C01D5/00 , Y02P20/125
摘要： The present invention relates to a process for the recovery of sulphate of potash (SOP) from bittern. Kainite is obtained by fractional crystallization of the bittern. Kainite is converted into schoenite with simultaneous removal of NaCl and the filtrate (SEL) is used for production of KCl. Schoenite is reacted with aqueous KCl to yield SOP and the filtrate (KEL) is recycled in the kainite to schoenite conversion step. The production of KCl from SEL is carried out with the aid of dipicrylamine (DPA) . Lime is treated with DPA in water for the production of highly soluble Ca (DPA) 2, which in turn treated with SEL to produce insoluble K(DPA) .K(DPA) is treated with HCl to produce KCl and insoluble DPA, which can be recycled for the production of Ca (DPA) 2. The aqueous KCl thus obtained is treated with schoenite to prepare SOP. The KEL obtained along with SOP is recycled to generate schoenite.
摘要翻译：本发明涉及一种从苦酒中回收钾盐（SOP）的硫酸盐的方法。赤铁矿通过盐水的分级结晶获得。将凯氏铁矿转化成同时去除氯化钠的白铁矿，滤液（SEL）用于生产氯化钾。白铁矿与KCl水溶液反应以产生SOP，并将滤液（KEL）在赤铁矿中再循环至闪长岩转化步骤。来自SEL的KCl的生产在二辛基胺（DPA）的辅助下进行。石灰在水中用DPA处理，用于生产高度可溶的Ca（DPA）2，其又用SEL处理以产生不溶性K（DPA）.KC（DPA）用HCl处理以产生KCl和不溶性DPA，其可以再循环用于生产Ca（DPA）2.用氯铂酸处理得到的KCl水溶液以制备SOP。与SOP一起获得的KEL被再循环以产生白铁矿。

2. 发明申请

WO2011027353A1 INTEGRATED PROCESS FOR THE PRODUCTION OF JATROPHA METHYL ESTER AND BY PRODUCTS 审中-公开
标题翻译：用于生产JATROPHA甲基酯和产品的综合方法
公开(公告)号：WO2011027353A1
公开(公告)日：2011-03-10
申请号：PCT/IN2010/000192
申请日：2010-03-29
申请人： COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH , GHOSH, Pushpito, Kumar , MISHRA, Sandhya, Chandrika, Prasad , GANDHI, Mahesh, Ramniklal , UPADHYAY, Sumesh, Chandra , PAUL, Parimal , ANAND, Pritpal, Singh , POPAT, Kiritkumar, Mangaldas , SHRIVASTAV, Anupama, Vijaykumar , MISHRA, Sanjiv, Kumar , ONDHIYA, Neelam , MARU, Ramesh, Dudabhai , DYAL, Gangadharan , BRAHMBHATT, Harshad , BORICHA, Vinod , CHAUDHARY, Doongar, Ram , REBARY, Babulai , ZALA, Krushnadevsingh, Sukhdevsinh
发明人： GHOSH, Pushpito, Kumar , MISHRA, Sandhya, Chandrika, Prasad , GANDHI, Mahesh, Ramniklal , UPADHYAY, Sumesh, Chandra , PAUL, Parimal , ANAND, Pritpal, Singh , POPAT, Kiritkumar, Mangaldas , SHRIVASTAV, Anupama, Vijaykumar , MISHRA, Sanjiv, Kumar , ONDHIYA, Neelam , MARU, Ramesh, Dudabhai , DYAL, Gangadharan , BRAHMBHATT, Harshad , BORICHA, Vinod , CHAUDHARY, Doongar, Ram , REBARY, Babulai , ZALA, Krushnadevsingh, Sukhdevsinh
IPC分类号： C11C1/08 , C11C3/00 , C10L1/02
CPC分类号： C11C3/06 , C10G2300/1014 , C10L1/026 , C11C1/08 , C11C3/003 , C12P7/625 , Y02E50/13 , Y02P30/20
摘要： The present invention provides a simpler and more energy efficient process for the preparation of fatty acid methyl ester (biodiesel) from sun dried whole seed capsules of Jatropha curcas integrated with value addition of seed shells, deoiled cake and crude glycerol co-product stream. More specifically, the invention relates to a method of dispensing with the need for excess methanol recovery through distillation, cost-effective resin treatment for the refining of methyl ester and utilization of co-streams for preparation of high density energy briquettes and Polyhydroxyalkanoate biodegradable polymer in efficient and cost-effective manner.
摘要翻译：本发明提供了一种更简单和更节能的方法，用于从麻疯树的太阳干燥全种子胶囊制备脂肪酸甲酯（生物柴油），其中加入了种子壳，去油饼和粗甘油副产物流。更具体地，本发明涉及一种分配需要通过蒸馏进行过量甲醇回收的方法，用于精制甲酯的成本有效的树脂处理和用于制备高密度能量团块和聚羟基链烷酸酯可生物降解聚合物的共流的方法高效和经济有效的方式。

3. 发明申请

WO2013150363A1 SELECTIVE EXTRACTION OF POTASSIUM CHLORIDE FROM SCHOENITE END LIQUOR EMPLOYING TARTARIC ACID AS SAFE, BENIGN AND RECYCLABLE EXTRACTANT 审中-公开
标题翻译：选择性提取氯化钾作为安全，通用和可回收的萃取剂使用塔可酸
公开(公告)号：WO2013150363A1
公开(公告)日：2013-10-10
申请号：PCT/IB2013/000582
申请日：2013-04-02
申请人： COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH
发明人： MAITI, Pratyush , GHOSH, Pushpito Kumar , GHARA, Krishna, Kanta , SOLANKI, Jignesh , BRAHMBHATT, Harshad, Raman , CHUNAWALA, Jatin, Ramesh , ERINGATHODI, Suresh , PAUL, Parimal
IPC分类号： C01D3/06 , C01D3/08
CPC分类号： C01D3/08 , C01D3/06 , C22B26/10
摘要： Although U S patent 8,182,784 teaches the recovery of potassium chloride from schoenite end liquor (SEL) using dipicrylamine as extractant, and consequently simplifies the recovery of sulphate of potash (SOP) from kainite mixed salt employing the scheme disclosed in U S patent 7,041,268, the hazards associated with this extractant have thwarted practical utilization of the invention. Many other extractants for potash recovery have been disclosed in the prior art but none has been found suitable so far for practical exploitation. It is disclosed herein that the bitartrate ion, and particularly L-bitartrate, precipitates out potassium bitartrate very efficiently from SEL with ca. 90% utilization of the extractant. In contrast, recovery of potassium bi-tartrate from sea bittern directly is relatively much lower. It is further disclosed that this precipitate can be treated with magnesium hydroxide and magnesium chloride to throw out magnesium tartrate with ca. 90% recovery while yielding a nearly saturated solution of potassium chloride which can be utilized for the reaction with schoenite to obtain SOP. It is further demonstrated that the magnesium tartrate can be treated with an appropriate amount of aqueous HCl and added into a subsequent batch of SEL to throw out potassium bitartrate once again which demonstrates the recyclability of the extractant. The overall loss of tartrate over a cycle was ca. 20% but the dissolved tartrate remaining in the K-depleted SEL and KCl solutions can be precipitated out as calcium tartrate from which tartaric acid can be recovered by known methods, curtailing thereby the loss of tartaric acid per kg of KCl to
摘要翻译：尽管美国专利8,182,784教导了使用二辛基胺作为萃取剂从白铁矿末端溶液（SEL）中回收氯化钾，从而简化了使用美国专利7,041,268中公开的方案从卡培酸盐混合盐中回收硫酸钾（SOP）该提取剂阻碍了本发明的实际应用。许多其它用于钾盐回收的萃取剂已经在现有技术中公开，但迄今为止没有发现适用于实际的开发。本文公开了酒石酸盐离子，特别是L-酒石酸盐，从SEL中非常有效地沉淀出酒石酸钾。萃取剂的利用率达90％。相比之下，直接从海盐酸盐中回收酒石酸钾相对要低得多。进一步公开，可以用氢氧化镁和氯化镁处理该沉淀物，以约 90％的回收率，同时产生几乎饱和的氯化钾溶液，可用于与白铁矿反应获得SOP。进一步证明酒石酸镁可以用适量的HCl水溶液处理，并再次添加到随后的一批SEL中以再次排出酒石酸钾，这表明萃取剂的可回收性。在一个循环中酒石酸的总体损失约为 20％，但残留在K-消耗的SEL和KCl溶液中的溶解酒石酸盐可以以酒石酸钙沉淀出，酒石酸可以通过已知方法从其中回收，从而减少酒石酸/ kg KCl的损失至<5g。也证明了通过类似的方法，含有ca. 4％KCl可以浓缩至20-22％KCl，具有优异的酒石酸利用效率，并且该溶液也可类似地用于SOP制备。含有其他阴离子如硫酸盐，硝酸盐，磷酸盐和碳酸盐的钾盐也可以由分离的酒石酸钾制备。

4. 发明申请

WO2017002137A1 SUSTAINABLE BIOMATERIAL NANOCOMPOSITES FOR WATER TREATMENT AND PROCESS FOR PREPARATION THEREOF 审中-公开
标题翻译：用于水处理的可持续生物材料纳米复合材料及其制备方法
公开(公告)号：WO2017002137A1
公开(公告)日：2017-01-05
申请号：PCT/IN2016/050216
申请日：2016-07-01
申请人： COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH
发明人： PAUL, Parimal , NATARAJ, Sanna Kotrappanavar , KUMAR, Anshu , PRAJAPATI, Pradeep Kumar
IPC分类号： C02F1/28 , C08L5/04 , C08L5/08
CPC分类号： C08L5/04 , C02F1/002 , C02F1/281 , C02F1/286 , C02F1/288 , C02F1/444 , C02F1/505 , C02F2101/14 , C02F2101/22 , C02F2101/308 , C02F2303/16 , C02F2305/08 , C08K3/08 , C08K2003/0806 , C08L5/08
摘要： Invention discloses a sustainable biomaterial Scaffold (BMS) nanocomposites useful for removal of fluoride, reactive black and Cr(VI) for water purification and process for the preparation of biomaterial Scaffold (BMS) nanocomposites. Its application in removal of fluoride (F-), chromium (Cr(VI)) and color contaminants from water is reported. This BMS nanocomposite exhibited as high as ~168 mg g-1 and ~60 mg g-1 fluoride uptake efficiency at pH 4 and pH 7 respectivily, and ~8.5 mg g-1 Cr(VI) uptake capacity. With this material, >99 % reactive black-5 (RB-5) removal was achieved with remarkable surface regeneration property.
摘要翻译：本发明公开了一种可持续的生物材料支架（BMS）纳米复合材料，用于去除氟化物，反应性黑色和用于水净化的Cr（VI）和用于制备生物材料支架（BMS）纳米复合材料的方法。报道了其在去除氟化物（F-），铬（Cr（VI））和颜色污染物从水中的应用。该BMS纳米复合材料在pH4和pH7下表现高达〜168 mg g-1和〜60 mg g-1氟化物摄取效率，以及〜8.5 mg g-1 Cr（VI）摄取能力。使用该材料，实现了具有显着的表面再生性能> 99％的反应性黑-5（RB-5）去除。

5. 发明授权

EP2751028B1 SELECTIVE EXTRACTION OF POTASSIUM CHLORIDE FROM SCHOENITE END LIQUOR EMPLOYING TARTARIC ACID AS SAFE, BENIGN AND RECYCLABLE EXTRACTANT 有权
标题翻译：钾肥FROM schonite端液体作为一种安全，良性的和可重复使用的提取介质选择性提取一个带葡萄酒ACID
公开(公告)号：EP2751028B1
公开(公告)日：2015-12-09
申请号：EP13722048.9
申请日：2013-04-02
申请人： Council of Scientific & Industrial Research
发明人： MAITI, Pratyush , GHOSH, Pushpito Kumar , GHARA, Krishna, Kanta , SOLANKI, Jignesh , BRAHMBHATT, Harshad, Raman , CHUNAWALA, Jatin, Ramesh , ERINGATHODI, Suresh , PAUL, Parimal
IPC分类号： C01D3/06 , C01D3/08
CPC分类号： C01D3/08 , C01D3/06 , C22B26/10

6. 发明公开

EP1945567A1 IMPROVED PROCESS FOR THE RECOVERY OF SULPHATE OF POTASH (SOP) FROM SULPHATE RICH BITTERN 有权
标题翻译：改进的方法制取硫酸钾（SOP，钾肥硫酸酯）在硫酸RICH母亲SOLE
公开(公告)号：EP1945567A1
公开(公告)日：2008-07-23
申请号：EP05850953.0
申请日：2005-12-27
申请人： COUNCIL OF SCIENTIFIC & INDUSTRIAL RESEARCH
发明人： PAUL, Parimal , GHOSH, Pushpito Kumar , LANGALIA, Kaushik Jethalal , SUBRAMANIAN, Palani Sivagnana , ERINGATHODI, Suresh , PATRA, Subrata , AGNIHOTRI, Pragati
IPC分类号： C01D5/00 , C05D1/02
CPC分类号： C05D1/02 , C01D3/06 , C01D5/00 , Y02P20/125
摘要： The present invention relates to a process for the recovery of sulphate of potash (SOP) from bittern. Kainite is obtained by fractional crystallization of the bittern. Kainite is converted into schoenite with simultaneous removal of NaCl and the filtrate (SEL) is used for production of KCl. Schoenite is reacted with aqueous KCl to yield SOP and the filtrate (KEL) is recycled in the kainite to schoenite conversion step. The production of KCl from SEL is carried out with the aid of dipicrylamine (DPA) . Lime is treated with DPA in water for the production of highly soluble Ca (DPA) 2, which in turn treated with SEL to produce insoluble K(DPA) .K(DPA) is treated with HCl to produce KCl and insoluble DPA, which can be recycled for the production of Ca (DPA) 2. The aqueous KCl thus obtained is treated with schoenite to prepare SOP. The KEL obtained along with SOP is recycled to generate schoenite.

7. 发明公开

EP2751028A1 SELECTIVE EXTRACTION OF POTASSIUM CHLORIDE FROM SCHOENITE END LIQUOR EMPLOYING TARTARIC ACID AS SAFE, BENIGN AND RECYCLABLE EXTRACTANT 有权
标题翻译：钾肥FROM schonite端液体作为一种安全，良性的和可重复使用的提取介质选择性提取一个带葡萄酒ACID
公开(公告)号：EP2751028A1
公开(公告)日：2014-07-09
申请号：EP13722048.9
申请日：2013-04-02
申请人： Council of Scientific & Industrial Research An Indian registered body incorporated under the Registration of Societies Act (Act XXI of 1860)
发明人： MAITI, Pratyush , GHOSH, Pushpito Kumar , GHARA, Krishna, Kanta , SOLANKI, Jignesh , BRAHMBHATT, Harshad, Raman , CHUNAWALA, Jatin, Ramesh , ERINGATHODI, Suresh , PAUL, Parimal
IPC分类号： C01D3/06 , C01D3/08
CPC分类号： C01D3/08 , C01D3/06 , C22B26/10
摘要： Although U S patent 8,182,784 teaches the recovery of potassium chloride from schoenite end liquor (SEL) using dipicrylamine as extractant, and consequently simplifies the recovery of sulphate of potash (SOP) from kainite mixed salt employing the scheme disclosed in U S patent 7,041,268, the hazards associated with this extractant have thwarted practical utilization of the invention. Many other extractants for potash recovery have been disclosed in the prior art but none has been found suitable so far for practical exploitation. It is disclosed herein that the bitartrate ion, and particularly L-bitartrate, precipitates out potassium bitartrate very efficiently from SEL with ca. 90% utilization of the extractant. In contrast, recovery of potassium bi-tartrate from sea bittern directly is relatively much lower. It is further disclosed that this precipitate can be treated with magnesium hydroxide and magnesium chloride to throw out magnesium tartrate with ca. 90% recovery while yielding a nearly saturated solution of potassium chloride which can be utilized for the reaction with schoenite to obtain SOP. It is further demonstrated that the magnesium tartrate can be treated with an appropriate amount of aqueous HCl and added into a subsequent batch of SEL to throw out potassium bitartrate once again which demonstrates the recyclability of the extractant. The overall loss of tartrate over a cycle was ca. 20% but the dissolved tartrate remaining in the K-depleted SEL and KCl solutions can be precipitated out as calcium tartrate from which tartaric acid can be recovered by known methods, curtailing thereby the loss of tartaric acid per kg of KCl to

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