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1. 发明申请

WO2002100831A1 4-IMINO-N-ALKOXY OR OXY-POLYALKYL-PIPERIDINE COMPOUNDS AND THEIR USE AS POLYMERIZATION REGULATORS 审中-公开
标题翻译： 4-亚氨基-N-烷基或氧代 - 聚亚烷基 - 哌啶化合物及其作为聚合调节剂的用途
公开(公告)号：WO2002100831A1
公开(公告)日：2002-12-19
申请号：PCT/EP2002/006108
申请日：2002-06-04
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , HINTERMANN, Tobias , KRAMER, Andreas , ZINK, Marie-Odile , BUGNON, Lucienne
发明人： NESVADBA, Peter , HINTERMANN, Tobias , KRAMER, Andreas , ZINK, Marie-Odile , BUGNON, Lucienne
IPC分类号： C07D211/94
CPC分类号： C07D211/94
摘要： The present invention relates to selected 4-imino-N-alkoxy-polyalkyl-peperidine compounds preparation, a polymerizable composition comprising a) at least one ethylenically unsaturated monomer and b) a 4-imino-N-alkoxy-polyalkyl-piperidine compound. Further aspects of the present invention are a process for polymerizing ethylenically unsaturated monomers, and the use of 4-imino-N-alkoxy-polyalkyl-piperidine compounds for controlled polymerization. The intermediate N-oxyl derivatives, a composition of the N-oxyl derivatives with ethylenically unsaturated monomers and a free radical initiator, as well as a process for polymerization are also subjects of the present invention.
摘要翻译：本发明涉及选择的4-亚氨基-N-烷氧基 - 多烷基 - 哌啶化合物，其可聚合组合物包含a）至少一种烯属不饱和单体和b）4-亚氨基-N-烷氧基 - 多烷基 - 哌啶化合物。本发明的其它方面是用于聚合烯属不饱和单体的方法，以及4-亚氨基-N-烷氧基 - 聚烷基 - 哌啶化合物用于受控聚合的方法。中间体N-氧基衍生物，具有烯键式不饱和单体的N-氧基衍生物和自由基引发剂的组合物以及聚合方法也是本发明的主题。

2. 发明申请

WO2005118651A1 ALKOXYAMINES CONTAINING A RADICALLY POLYMERIZABLE GROUP 审中-公开
标题翻译：含有极性可聚合基团的烷氧基胺
公开(公告)号：WO2005118651A1
公开(公告)日：2005-12-15
申请号：PCT/EP2005/052260
申请日：2005-05-17
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , KRAMER, Andreas , BUGNON, Lucienne
发明人： NESVADBA, Peter , KRAMER, Andreas , BUGNON, Lucienne
IPC分类号： C08F4/00
CPC分类号： C07D241/08 , C07D211/94
摘要： The instant invention relates to novel alkoxyamine initiators/regulators containing an ethylenically unsaturated, radically polymerizable group. The compounds are useful for the preparation of complex polymeric architectures. Further aspects of the invention are a polymerizable composition and a polymerization process comprising the alkoxyamine initiators/regulators, a macroinitiator obtainable by said polymerization process and a process for polymerizing with the macroinitiator.
摘要翻译：本发明涉及含有烯属不饱和的，可自由基聚合的基团的新的烷氧基胺引发剂/调节剂。该化合物可用于制备复合聚合物结构。本发明的其它方面是可聚合组合物和包含烷氧基胺引发剂/调节剂的聚合方法，通过所述聚合方法获得的大分子引发剂和与大分子引发剂聚合的方法。

3. 发明申请

WO2006051047A1 N-SUBSTITUTED IMIDES AS POLYMERIZATION INITIATORS 审中-公开
标题翻译：作为聚合引发剂的N-取代的咪唑
公开(公告)号：WO2006051047A1
公开(公告)日：2006-05-18
申请号：PCT/EP2005/055646
申请日：2005-10-31
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BENKHOFF, Johannes , BUGNON, Lucienne , POWELL, Karin , JUNG, Tunja
发明人： NESVADBA, Peter , BENKHOFF, Johannes , BUGNON, Lucienne , POWELL, Karin , JUNG, Tunja
IPC分类号： C08F4/00 , C07C239/16 , C07D209/48 , C07D207/40 , C07D221/14
CPC分类号： C07D207/404 , B33Y70/00 , C07D207/46 , C07D209/48 , C07D221/14 , C08F4/00
摘要： The invention relates to novel N-substituted imides and polymerizable compositions com¬ prising these N-substituted imides. The invention further relates to the use of N-substituted imides as polymerization initiators. The imides are compounds of the formula (I) and (II) wherein n is 1 or 2; m is 1 or 2; R 1 and R 2 are each, independently of one another, hydrogen, C 1 -C 18 alkyl, C 1 -C- 18 alkenyl C 6 -C 14 aryl, aralkyl, C 5 -C 12 cycloalkyl, each of which may be substituted by halogen, C 1 -C 4 -alkyl, hydroxy, C 1 -C 6 alkoxy, carbonyl, C 1 -C 6 alkoxycarbonyl; or R 1 and R 2 together with the adjacent -CO-N-CO- group may form a monocyclic, bicyclic or polycyclic ring, said ring having up to 50 non hydrogen atoms and wherein said ring may contain the structural element (formula III) more than once; R 3 if n is 1, is C 1 -C 18 alkyl, C 6 -C 14 aryl, aralkyl, C 5 -C 12 cycloalkyl, OR 10 or SR 11 , NR 12 R 13 ; wherein R 3 if n is 2, is C 2 -C 12 alkylene, C 6 -C 14 arylene, xylylene R 4 and R 5 , correspond to R 1 and R 2 ; R 6 if n is 1, is hydrogen, C 1 -C 18 alkyl, C 6 -C 14 aryl, aralkyl, C 5 -C 12 cycloalkyl, NR 14 R 15 ; wherein R 6 if n is 2, is C 2 -C 12 alkylene, C 6 -C 14 arylene, xylylene; R 7 is hydrogen, C 1 -C 18 alkyl, C 6 -C 14 aryl, aralkyl, C 5 -C 12 cycloalkyl, each of which may be substituted by halogen, C 1 -C 4 -alkyl, hydroxy, C 1 -C 6 alkoxy, carbonyl, C 1 -C 6 alkoxy- carbonyl; or R 7 and R 14 or R 7 and R 15 form together with the N-atom attached to R 7 a 5- 6 membered ring, optionally interrupted by -NH-, -N(C 1 -C 8 alkyl)-, -O- and/or S-atoms.
摘要翻译：本发明涉及新型N-取代的酰亚胺和可聚合的组合物，这些组合物包括这些N-取代的酰亚胺。本发明还涉及N-取代的酰亚胺作为聚合引发剂的用途。酰亚胺是式（I）和（II）的化合物，其中n为1或2; m为1或2; R 1和R 2各自彼此独立地为氢，C 1 -C 18烷基， C 1 -C 18 - 烯基C 6 -C 14芳基，芳烷基，C 5 - 其中每一个可被卤素取代，C 1 -C 4 - C 4 - 烷基，羟基，C 1 -C 12 - 羰基，C 1 -C 6烷氧基羰基，C 1 -C 6烷氧基羰基，C 1 -C 6烷氧基羰基，或R 1和R 2与相邻的-CO-N-CO-基团可以形成单环，双环或多环，所述环具有至多50个非氢并且其中所述环可以多次含有结构元素（式III）; 如果n为1，则R 3为C 1 -C 18烷基，C 6 -C 芳基，芳烷基，C 5 -C 12环烷基，OR 10或SR 11， NR _{12 - [R _{13 ; 如果n为2，其中R 3为C 2 -C 12亚烷基，C 6 -C > 14亚芳基，亚二甲苯基R 4和R 5对应于R 1和R 2， ; 如果n为1，则R 6为氢，C 1 -C 18烷基，C 6 -C 芳基，芳烷基，C 5 -C 12环烷基，NR 14 R 15， ; 如果n为2，其中R 6为C 12 -C 12亚烷基，C 6 -C 亚芳基，亚二甲苯; R 7是氢，C 1 -C 18烷基，C 6 -C 14烷基，C 1 -C 6烷基，芳基，芳烷基，C 5 -C 12环烷基，其各自可以被卤素取代，C 1 -C 12 - 4-烷基，羟基，C 1 -C 6烷氧基，羰基，C 1 -C 6烷基，C 1 -C 6烷基，烷氧基 - 羰基; 或R 7和R 14或R 7和R 15和与R连接的N-原子一起形成任选地被-NH-，-N（C 1 -C 8烷基） - ， - O-（C 1 -C 6）烷基取代的5-6元环， - 和/或S-原子。}}

4. 发明申请

WO2008031733A2 IMIDAZOLIDINONE NITROXIDES AS ELECTRODE MATERIALS FOR ENERGY STORAGE DEVICES 审中-公开
标题翻译：咪唑啉酮氮氧化物作为用于储能装置的电极材料
公开(公告)号：WO2008031733A2
公开(公告)日：2008-03-20
申请号：PCT/EP2007/059156
申请日：2007-09-03
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BUGNON, Lucienne , FREY, Markus
发明人： NESVADBA, Peter , BUGNON, Lucienne , FREY, Markus
IPC分类号： H01M4/02 , H01M4/60
CPC分类号： H01M4/137 , C07D233/80 , C07D471/10 , C07D498/10 , C08K5/34 , H01M4/60 , H01M10/052
摘要： The invention relates to a an electrical energy storage device, such as a capacitor or a secondary battery, utilizing as active element the oxidation and reduction cycle of a sterically hindered imidazolidinone nitroxide radical. Further aspects of the invention are a method for providing such an energy storage device, the use of the respective compounds as active elements in energy storage devices and selected novel imidazolidinone nitroxide compounds.
摘要翻译：本发明涉及利用位阻咪唑烷酮氮氧自由基的氧化和还原循环作为活性元素的电能存储装置，例如电容器或二次电池。本发明的其它方面是提供这种能量存储装置的方法，各种化合物作为能量存储装置中的活性元素的用途以及选择的新型咪唑烷酮氮氧化物化合物。

5. 发明申请

WO2007115939A1 PROCESS FOR THE PREPARATION OF CROSSLINKED NITROXIDE POLYMERS 审中-公开
标题翻译：交联的硝酸酯聚合物的制备方法
公开(公告)号：WO2007115939A1
公开(公告)日：2007-10-18
申请号：PCT/EP2007/052973
申请日：2007-03-28
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BUGNON, Lucienne
发明人： NESVADBA, Peter , BUGNON, Lucienne
IPC分类号： C08F4/00
CPC分类号： C08F4/00 , C08F8/18 , C08F2810/20 , H01M4/60 , H01M10/0525 , C08F120/36 , C08F120/60
摘要： The invention relates to a process for the preparation of crosslinked polymers bearing nitroxide groups, which are prepared by a method frequently called atom transfer radical addition polymerization (ATRA). A further aspect of the invention is the use of such polymeric crosslinked nitroxides as stabilizers for polymers against the detrimental influences of heat and UV light, as stabilizers against premature polymerization of vinyl aromatic monomers and as active electrode materials in secondary batteries.
摘要翻译：本发明涉及一种制备具有氮氧根基团的交联聚合物的方法，其通过常规称为原子转移自由基加成聚合（ATRA）的方法制备。本发明的另一方面是使用这种聚合交联的氮氧化物作为聚合物的稳定剂，防止热和紫外线的有害影响，作为稳定剂防止乙烯基芳族单体的过早聚合和作为二次电池中的活性电极材料。

6. 发明申请

WO2007107468A1 TRIAZINE CONTAINING ELECTRODE MATERIALS FOR SECONDARY BATTERIES 审中-公开
标题翻译：用于二次电池的TRIAZINE包含电极材料
公开(公告)号：WO2007107468A1
公开(公告)日：2007-09-27
申请号：PCT/EP2007/052261
申请日：2007-03-12
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BUGNON, Lucienne
发明人： NESVADBA, Peter , BUGNON, Lucienne
IPC分类号： H01M4/60 , H01M10/40 , H01M4/02
CPC分类号： H01M4/60 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/137 , H01M4/364 , H01M4/62 , H01M2004/028
摘要： The invention relates to a stable secondary battery utilizing as active element the oxidation and reduction cycle of a sterically hindered nitroxide radical, which is bonded to a triazine structural element. Further aspects of the invention are a method for providing such a secondary battery, the use of the respective compounds as active elements in secondary batteries and selected novel nitroxide compounds as such.
摘要翻译：本发明涉及一种稳定的二次电池，其利用与三嗪结构元件结合的空间位阻的氮氧自由基的氧化和还原循环作为活性元素。本发明的其他方面是提供这种二次电池的方法，各种化合物作为二次电池中的活性元素的用途以及所选择的新型氮氧化物化合物。

7. 发明申请

WO2004026915A1 POLYMERIC ALKOXYAMINES PREPARED BY ATOM TRANSFER RADICAL ADDITION (ATRA) 审中-公开
标题翻译：由原子转移辐射（ATRA）制备的聚合烷氧基胺
公开(公告)号：WO2004026915A1
公开(公告)日：2004-04-01
申请号：PCT/EP2003/010272
申请日：2003-09-16
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BUGNON, Lucienne
发明人： NESVADBA, Peter , BUGNON, Lucienne
IPC分类号： C08F4/00
CPC分类号： C08F4/00 , C08K5/3435
摘要： The instant invention pertains to polymeric alkoxyamines, which are prepared by atom transfer radical addition polymerization (ATRA). Further aspects of the invention are a process for their preparation and their use as light stabilizers, flame retardants and polymerization regulators/initiators in controlled radical polymerization processes. Yet another aspect of the invention are novel monomeric intermediate alkoxyamines, which are also useful as polymerization regulators/initiators.
摘要翻译：本发明涉及通过原子转移自由基加成聚合（ATRA）制备的聚合烷氧基胺。本发明的其它方面是其制备方法及其作为受控自由基聚合方法中的光稳定剂，阻燃剂和聚合调节剂/引发剂的用途。本发明的另一方面是新颖的单体中间体烷氧基胺，其也可用作聚合调节剂/引发剂。

8. 发明申请

WO2006131451A1 POLYMERIC NITROXIDES THEIR PREPARATION AND USE 审中-公开
标题翻译：聚合氮氧化物的制备和使用
公开(公告)号：WO2006131451A1
公开(公告)日：2006-12-14
申请号：PCT/EP2006/062651
申请日：2006-05-29
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BUGNON, Lucienne
发明人： NESVADBA, Peter , BUGNON, Lucienne
IPC分类号： C08F20/34 , C08F20/36 , C08F220/34 , C08F220/36
CPC分类号： C08F220/36
摘要： The instant invention relates to a process for the preparation of polymeric nitroxide radicals by group transfer polymerization. Further aspects of the invention are the polymers containing the nitroxide radicals as well as their use, in particular as active electrode materials in organic radical batteries.
摘要翻译：本发明涉及通过基团转移聚合制备聚合氮氧自由基的方法。本发明的其它方面是含有氮氧自由基的聚合物及其用途，特别是作为有机基团电池中的活性电极材料。

9. 发明申请

WO2004085397A1 PROCESS FOR THE OXIDATION OF SECONDARY AMINES INTO THE CORRESPONDING NITROXIDES 审中-公开
标题翻译：将二级胺氧化成相应的硝酸酯的方法
公开(公告)号：WO2004085397A1
公开(公告)日：2004-10-07
申请号：PCT/EP2004/050315
申请日：2004-03-17
申请人： CIBA SPECIALTY CHEMICALS HOLDING INC. , NESVADBA, Peter , BUGNON, Lucienne , VON BÜREN, Martin
发明人： NESVADBA, Peter , BUGNON, Lucienne , VON BÜREN, Martin
IPC分类号： C07D211/94
CPC分类号： C07D491/10 , C07B61/02 , C07D211/94
摘要： The invention relates to a process for the preparation of secondary nitroxide radicals from their corresponding secondary amines by oxidation with an organic peracid, comprising the steps a) adding to a reaction vessel a secondary amine, optionally together with an organic solvent and in one batch a base selected from the group consisting of alkali metal, alkaline earth metal or ammonium bicarbonates and alkaline earth metal or ammonium carbonates or mixtures thereof in the form of a solid together with water or as an aqueous slurry; b) dosing a peracid under stirring to the reaction mixture in an amount of 1,0 to 2,5 mol per mol of secondary amine; and c) isolating the organic phase.
摘要翻译：本发明涉及通过用有机过酸氧化从其相应的仲胺制备二级氮氧自由基的方法，包括以下步骤：a）向反应容器中加入仲胺，任选与有机溶剂一起加入一次碱选自碱金属，碱土金属或碳酸氢铵，碱土金属或铵的碳酸盐或其混合物，其形式为水与水或水性浆料; b）在搅拌下将过酸给予反应混合物，其量为每摩尔仲胺为1.0至2.5摩尔; 和c）分离有机相。

10. 发明公开

EP1543042A1 POLYMERIC ALKOXYAMINES PREPARED BY ATOM TRANSFER RADICAL ADDITION (ATRA) 审中-公开
标题翻译：聚合物烷氧基，制造的原子转移基加
公开(公告)号：EP1543042A1
公开(公告)日：2005-06-22
申请号：EP03750551.8
申请日：2003-09-16
申请人： Ciba Specialty Chemicals Holding Inc.
发明人： NESVADBA, Peter , BUGNON, Lucienne
IPC分类号： C08F4/00 , C08K5/32
CPC分类号： C08F4/00 , C08K5/3435
摘要： The instant invention pertains to polymeric alkoxyamines, which are prepared by atom transfer radical addition polymerization (ATRA). Further aspects of the invention are a process for their preparation and their use as light stabilizers, flame retardants and polymerization regulators/initiators in controlled radical polymerization processes. Yet another aspect of the invention are novel monomeric intermediate alkoxyamines, which are also useful as polymerization regulators/initiators.

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