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1. 发明专利

JP2000178566A METHOD FOR HYDROTREATMENT OF HYDROCARBON OIL 失效
公开(公告)号：JP2000178566A
公开(公告)日：2000-06-27
申请号：JP37802098
申请日：1998-12-18
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN , KIYOFUJI HIROYUKI
IPC分类号： C10G25/00 , C10G45/06 , C10G45/08 , C10G67/06
摘要： PROBLEM TO BE SOLVED: To reduce the deactivation of a catalyst caused by coke thereby prolonging the life of the catalyst and extending the operation time for hydrotreatment by bringing a feedstock hydrocarbon oil into contact with an adsorbing agent before the hydrotreatment to adsorptively remove and decrease polycyclic aromatic compounds in the hydrocarbon oil and then carrying out hydrotreatment in the presence of a catalyst. SOLUTION: As a feedstock hydrocarbon oil, crude oils, vacuum residues, topped crudes, catalyst cracking gas oils, thermal cracking gas oils and the like can be cited. Polycyclic aromatic compounds in the feedstock hydrocarbon oil are adsorptively removed to decrease to not more than 60 wt.%, preferably not more than 40 wt.% of the initial content. As an adsorbing agent, active carbon, alumina, silica-alumina, zeolite and the like can be exemplified. A preferable adsorbing agent contains at least 0.15 mmol/g of a solid acid (measured by the ammonia adsorption method), and silica-alumina containing 20-40 wt.% of alumina is preferable. Hydrotreatment can be carried out using an ordinary hydrotreatment apparatus and an ordinary hydrotreatment catalyst.

2. 发明专利

JPH0117414B2 失效
公开(公告)号：JPH0117414B2
公开(公告)日：1989-03-30
申请号：JP10601080
申请日：1980-07-31
申请人： CATALYSTS & CHEM IND CO
发明人： JUKI JUN , FUCHIGAMI JUN
IPC分类号： C10G47/16 , B01J29/06 , B01J29/16

3. 发明专利

JPS6225418B2 失效
公开(公告)号：JPS6225418B2
公开(公告)日：1987-06-03
申请号：JP3789080
申请日：1980-03-25
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN
IPC分类号： C10G47/12 , B01J21/02 , B01J23/85 , B01J35/10

4. 发明专利

JP2006175295A Hydrogenation purification catalyst composition 有权
标题翻译：氢化纯化催化剂组合物
公开(公告)号：JP2006175295A
公开(公告)日：2006-07-06
申请号：JP2004368059
申请日：2004-12-20
申请人： Catalysts & Chem Ind Co Ltd , Petroleum Energy Center , 触媒化成工業株式会社 , 財団法人石油産業活性化センター
发明人： FUCHIGAMI JUN , ISHIHARA HISAYA , YOSHIMURA YUJI
IPC分类号： B01J29/12 , B01J35/10 , C10G45/10 , C10G45/12
摘要： PROBLEM TO BE SOLVED: To provide a hydrogenation purification catalyst composition preventing reduction of activity by poisoning of hydrogen sulfide and nitrogen generated during a hydrogenation desulfurization reaction of a light oil and reduction of activity by coagulation of noble metal, having high hydrogenation ability when used for hydrogenation purification of a cracked light oil containing a sulfur compound being hardly subjected to hydrogenation desulfurization such as alkyldibenzothiophene and exhibiting an excellent effect such as a high desulfurization activity.
SOLUTION: In the hydrogenation purification catalyst composition, an ultra-stable Y type zeolite having properties of the following (a)-(e) is carried with a noble metal component. (a) a molar ratio of SiO
2 /Al
2 O
3 is in a range of 80-800, (b) a crystal lattice constant (UD) is in a range of 24.28-24.32 Å, (c) a fine pore volume of a fine pore in a range of a fine pore diameter of 3.5-5.0 mm is 0.10 ml/g or higher, (d) a specific surface area is 700 m
2 /g or higher and (e) an Na
2 O content is 0.06 wt.% or lower.
COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：待解决的问题：提供一种氢化净化催化剂组合物，其防止轻油加氢脱硫反应中产生的硫化氢和氮中毒引起的活性降低，并且具有高氢化能力的贵金属凝结活性降低当氢化纯化含有几乎不进行氢化脱硫的硫化合物的裂解轻油如烷基二苯并噻吩并表现出优异的脱硫活性。解决方案：在氢化纯化催化剂组合物中，具有以下（a） - （e）的性质的超稳定Y型沸石与贵金属组分一起进行。（a）SiO 2 / Al 2 3 的摩尔比在80-800的范围内，（b）晶格常数（UD）在24.28-24.32埃的范围内，（c）细孔直径为3.5-5.0毫米的细孔的细孔容积为0.10毫升/克或更高，（d）a 比表面积为700m 2 / SP / g以上，（e）Na 2 O含量为0.06重量％以下。版权所有（C）2006，JPO＆NCIPI

5. 发明专利

JP2000248283A HYDROGENATION TREATMENT OF HEAVY OIL 失效
公开(公告)号：JP2000248283A
公开(公告)日：2000-09-12
申请号：JP9322199
申请日：1999-02-25
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN , ONO KENJI
IPC分类号： C10G45/08 , C10G49/04 , C10G49/26 , C10G65/12
摘要： PROBLEM TO BE SOLVED: To hydrogenate a heavy oil while eliminating clogging of a heat exchanger, or the like, and to prolong an operation period by carrying out the hydrogenation treatment under a specific condition at a point of time when a dry sludge content in a formed oil obtained by hydrogenating the heavy oil reaches a tolerance limit value. SOLUTION: At a point of time of reaction temperature when a dry sludge content in a formed oil obtained by hydrogenating a heavy oil in the presence of a catalyst, for example, under 50-250 kg/cm2G hydrogen pressure at 0.1-20 Hr-1 liquid space velocity and at the ratio of H2/mixture of 500-10,000 Nl/l reaches 0.3-0.5 wt.%, preferably 0.30-0.35 wt.% tolerance limit value, a reaction temperature is rapidly raised, the heavy oil is hydrogenated at such a reaction temperature as to make the dry sludge content in the formed oil reach

6. 发明专利

JPH05138032A HYDROCRACKING CATALYST COMPOSITION 失效
公开(公告)号：JPH05138032A
公开(公告)日：1993-06-01
申请号：JP33003691
申请日：1991-11-19
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN , HAGIO MICHIYASU , IDA TAKANORI , ARIMA YUSAKU , SATO GORO
IPC分类号： B01J29/08 , C10G47/20
摘要： PURPOSE:To obtain high desulfurization effect by performing the hydrocracking of hydrocarbon oil in a high conversion rate so that a middle fraction is obtained in high yield and the formation rate of gas and naphtha is suppressed low using vogesite type zeolite produced by bringing vogesite type zeolite receiving heat history into contact with an aluminum removing agent at pH 4 or less. CONSTITUTION:In a hydrocracking catalyst composition, vogesite type zeolite receiving heat history at 150 deg.C or higher is brought into contact with an aluminum removing agent in an aqueous phase in the presence of soluble silica at pH 4 or less to produce modified vogesite type zeolite. Herein, vogesite type zeolite receiving heat history at 150 deg.C or higher means that vogesite type zeolite being a starting raw material before the contact with the aluminum removing agent has history such that it is calcined at 150 deg.C or higher.

7. 发明专利

JPH03292396A METHOD OF HYDROTREATING KEROSINE OR GAS OIL 失效
公开(公告)号：JPH03292396A
公开(公告)日：1991-12-24
申请号：JP9475190
申请日：1990-04-10
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN , WATANABE MANABU , NAGANISHI KATSUSHIGE , KINO KATSUHIRO
IPC分类号： C10G45/08 , B01J23/88 , C10G45/12 , C10G45/72
摘要： PURPOSE:To realize improvements in catalyst activity, color, and oxidation stability by bringing kerosine or gas oil into contact with a catalyst at a specified temperature. CONSTITUTION:Kerosine or gas oil having a boiling point of 340-390 deg.C is fed into a reaction tube filled with a catalyst (e.g. 4wt.%CoO/15wt.% MoO3-B2 O3-SiO2-Al2O3 catalyst) to be brought into contact therewith under conditions of a reaction pressure of 20-70kg/cm G, a liquid hourly space velocity of 1-6hr , and a hydrogen to feedstock oil ratio of 50-200Nm /kl at such a temperature that the zone temperature on the inlet side of the reactor is equal to or higher than that on the outlet side.

8. 发明专利

JP2007100013A Method for hydrorefining of gas oil 审中-公开
标题翻译：气体加氢方法
公开(公告)号：JP2007100013A
公开(公告)日：2007-04-19
申请号：JP2005294569
申请日：2005-10-07
申请人： Catalysts & Chem Ind Co Ltd , Petroleum Energy Center , 触媒化成工業株式会社 , 財団法人石油産業活性化センター
发明人： FUCHIGAMI JUN , HORIE TAKAHISA , KAMEOKA TAKASHI
IPC分类号： C10G65/04 , C10G45/08
摘要： PROBLEM TO BE SOLVED: To provide a method for the hydrorefining of a gas oil that exhibits excellent effects of high hydrogenation capability, high desulfurization activity and the like in a catalytic refining reaction of a light cycle oil and the like including a difficult-to-desulfurize substance such as an alkyl dibenzothiophene or the like, and uses a base metal catalyst free from the deterioration in catalytic activity due to poisoning by hydrogen sulfide or the like generated during the hydrodesulfurization reaction of the gas oil.
SOLUTION: The method for the hydrorefining of a gas oil is a method for hydrorefining by bringing a gas oil fraction into contact with a catalyst under hydrorefining conditions in a vertically elongated reactor of a fixed-bed type wherein a first reaction zone of the vertically elongated reactor of the fixed-bed type is filled with a cobalt/molybdenum catalyst and a second reaction zone of the vertically elongated reactor of the fixed-bed type is filled with a nickel/molybdenum catalyst, which comprises feeding the gas oil to the vertically elongated reactor of the fixed-bed type from the upper part of the first reaction zone thereof and introducing hydrogen into the vertically elongated reactor of a fixed-bed type from the lower part of the second reaction zone thereof.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种在轻循环油等的催化精炼反应中显示优异的氢化能力高，脱硫活性等的优异的瓦斯油加氢精制方法，其包括困难的脱硫物质如烷基二苯并噻吩等，并且使用不会由于在瓦斯油的加氢脱硫反应期间产生的硫化氢等而引起的催化活性劣化的贱金属催化剂。解决方案：瓦斯油的加氢精制方法是通过在固定床型的垂直伸长的反应器中，在加氢精制条件下使粗柴油馏分与催化剂接触来加氢精制的方法，其中第一反应区固定床类型的垂直伸长的反应器填充有钴/钼催化剂，并且固定床类型的垂直伸长的反应器的第二反应区填充有镍/钼催化剂，其包括将瓦斯油固定床类型的垂直伸长的反应器，从其第一反应区的上部引入，并将氢气从其第二反应区的下部引入固定床类型的垂直伸长的反应器中。版权所有（C）2007，JPO＆INPIT

9. 发明专利

JP2000178565A METHOD FOR HYDROTREATMENT OF HYDROCARBON OIL 失效
公开(公告)号：JP2000178565A
公开(公告)日：2000-06-27
申请号：JP37801998
申请日：1998-12-18
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN , KIYOFUJI HIROYUKI
IPC分类号： C10G45/08 , C10G65/04
摘要： PROBLEM TO BE SOLVED: To decrease the deposition of coke on a catalyst thereby prolonging the life of the catalyst and extending the operation time for hydrotreatment by subjecting a topped crude containing kerosene and gas oil fractions having a boiling point within a specific range in a specific ratio to hydrotreatment in the presence of a catalyst. SOLUTION: A topped crude containing at least 15 vol.% of kerosene and gas oil fractions having a boiling point within the range of 165-370 deg.C is subjected to hydrotreatment in the presence of a catalyst. The content of the kerosene and gas oil fractions is preferably 15-50 vol.%, more preferably 20-40 vol.%. The hydrotreatment can be carried out using an ordinary direct hydrotreatment apparatus and an ordinary hydrotreatment catalyst. A product oil obtained by the hydrotreatment is fractionated through a fractionator or the like into gas fractions, naphtha fractions, kerosene and gas oil fractions, heavy oil fractions and the like. The separatively recovered kerosene and gas oil fractions having a boiling point ranging from 165-370 deg.C has been usually desulfurized to have a sulfur content of not more than 500 wt. ppm, and yet it can be subjected to further hydrotreatment, if required.

10. 发明专利

JPH10183142A CONTINUOUS DEHYDROGENATING DESULFURIZATION FOR HYDROCARBON OIL 失效
公开(公告)号：JPH10183142A
公开(公告)日：1998-07-14
申请号：JP35623596
申请日：1996-12-25
申请人： CATALYSTS & CHEM IND CO
发明人： FUCHIGAMI JUN , ONO KENJI , TOMOKIYO KENJI
IPC分类号： C10G45/02 , C10G45/72
摘要： PROBLEM TO BE SOLVED: To continuously hydrogenate and desulfurize a hydrocarbon oil for a long period of time, by temporarily lowering the reaction temperature of hydrogenating desulfurization to remove coke adsorbed and deposited on a catalyst without stopping operation in the middle of the reaction and to regenerate the catalyst deactivated by the coke. SOLUTION: In continuously supplying (A) a hydrocarbon oil to (B) a catalyst bed and continuously hydrogenating and desulfurizing the hydrocarbon oil (A) at a reaction temperature to make a sulfur concentration in (C) a formed oil into a fixed value, the reaction temperature is temporarily lowered, for example, to a reaction temperature at which a sulfur concentration in the component C when the reaction temperature is dropped is reduced to a sulfur concentration [Sr (wt.%)] satisfying the equation [Sp is a sulfur concentration (wt.%) in the component B before lowering the reaction temperature] and the reaction is carried out.

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