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1. 发明申请

WO2012059716A1 CARBON MATERIALS COMPRISING CARBON NANOTUBES AND METHODS OF MAKING CARBON NANOTUBES 审中-公开
标题翻译：包含碳纳米管的碳材料和制备碳纳米管的方法
公开(公告)号：WO2012059716A1
公开(公告)日：2012-05-10
申请号：PCT/GB2011/001549
申请日：2011-11-02
申请人： CAMBRIDGE ENTERPRISE LIMITED. , SUNDARAM, Rajyashree , KOZIOL, Krzysztof Kazimierz , LEKAWA-RAUS, Agnieszka Ewa , WINDLE, Alan
发明人： SUNDARAM, Rajyashree , KOZIOL, Krzysztof Kazimierz , LEKAWA-RAUS, Agnieszka Ewa , WINDLE, Alan
IPC分类号： C01B31/02 , B01J23/745 , B01J37/08 , D01F9/12
CPC分类号： C01B32/162 , B01J23/745 , B01J35/006 , B01J37/086 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B2202/22 , C01B2202/30 , C01B2202/36 , D01F9/127 , D01F9/1272 , D01F9/133 , D01F11/14 , Y10T428/268 , Y10T428/2927 , Y10T428/2982
摘要： The present invention relates to carbon materials comprising carbon nanotubes, powders comprising carbon nanotubes and methods of making carbon nanotubes. In the methods of the present invention, the size and/or formation of floating catalyst particles is closely controlled. The resulting carbon nanotubes typically exhibit armchair chirality and typically have metallic properties. The carbon nanotubes produced by this method readily form bulk materials, which typically have a conductivity of at least 0.7 x 106 Sm"1 in at least one direction. The invention has particular application to the manufacture of components such as electrical conductors. Suitable electrical conductors include wires (e.g. for electrical motors) and cables (e.g. for transmitting electrical power).
摘要翻译：本发明涉及包含碳纳米管的碳材料，包含碳纳米管的粉末和制造碳纳米管的方法。在本发明的方法中，浮动催化剂颗粒的尺寸和/或形成受到严格控制。所得碳纳米管通常具有扶手椅手性，并且通常具有金属性质。通过该方法制造的碳纳米管容易形成散装材料，其通常在至少一个方向上具有至少0.7×10 6 Sm -1的导电性，本发明特别适用于制造诸如电导体的部件，合适的电导体包括电线（例如用于电动机）和电缆（例如用于发送电力）。

2. 发明申请

WO2013190252A1 HEATING USING CARBON NANOTUBE-BASED HEATER ELEMENTS 审中-公开
标题翻译：使用碳纳米管加热器元件加热
公开(公告)号：WO2013190252A1
公开(公告)日：2013-12-27
申请号：PCT/GB2012/051435
申请日：2012-06-21
申请人： CAMBRIDGE ENTERPRISE LIMITED , JANAS, Dawid , KOZIOL, Krzysztof Kazimierz
发明人： JANAS, Dawid , KOZIOL, Krzysztof Kazimierz
IPC分类号： H05B3/14
CPC分类号： H05B3/145 , H01C17/06 , H01C17/28 , H05B3/08 , H05B3/34 , H05B2203/01 , H05B2203/013 , H05B2214/04 , Y10T29/49085
摘要： A heater element for generating heat via Joule heating, the heater element having a layer of aligned carbon nanotubes and electrical terminals located to allow, in use, an electrical current to be passed along the layer of aligned carbon nanotubes. The direction of the electrical current in use is substantially perpendicular to the alignment direction of the aligned carbon nanotubes. Also disclosed is a method of manufacturing a heater element, the method including growing carbon nanotubes in a CVD reactor and forming the layer of aligned carbon nanotubes by pulling a carbon nanotube yarn from the CVD reactor, the alignment direction being the direction of pulling from the CVD reactor.
摘要翻译：一种用于通过焦耳加热产生热量的加热器元件，该加热器元件具有一对排列的碳纳米管层和电气端子，这些电极位于允许在使用中沿着对准的碳纳米管层通过的电流。所使用的电流的方向基本上垂直于排列的碳纳米管的排列方向。还公开了一种制造加热器元件的方法，该方法包括在CVD反应器中生长碳纳米管并通过从CVD反应器中拉动碳纳米管纱线形成排列的碳纳米管层，该取向方向是从 CVD反应器。

3. 发明申请

WO2015189643A1 APPARATUS AND METHOD FOR PLASMA SYNTHESIS OF GRAPHITIC PRODUCTS INCLUDING GRAPHENE 审中-公开
标题翻译：用于等离子体合成包括石墨的石墨产品的装置和方法
公开(公告)号：WO2015189643A1
公开(公告)日：2015-12-17
申请号：PCT/GB2015/051745
申请日：2015-06-12
申请人： FGV CAMBRIDGE NANOSYSTEMS LIMITED , PENNINGTON, Dale Andrew , CLAYTON, Aaron Robert , JUDA, Katarzyna Luiza , PAUKNER, Catharina , KURZEPA, Lukasz , ST. JOHN COOPER, Robert Henry , KOZIOL, Krzysztof Kazimierz , JOAUG, Jerome Yi-Zhe
发明人： PENNINGTON, Dale Andrew , CLAYTON, Aaron Robert , JUDA, Katarzyna Luiza , PAUKNER, Catharina , KURZEPA, Lukasz , ST. JOHN COOPER, Robert Henry , KOZIOL, Krzysztof Kazimierz , JOAUG, Jerome Yi-Zhe
IPC分类号： H05H1/46 , C01B31/04
CPC分类号： B01J19/126 , B01J19/088 , B01J19/129 , B01J2219/0869 , B01J2219/0875 , B01J2219/0892 , C01B32/184 , C01B32/20 , C01B2204/04 , H05H1/46 , H05H2001/4622
摘要： Apparatus for plasma synthesis of graphitic products including graphene, comprising:a plasma nozzle coupled to a reaction chamber; means for supplying a process gas to the plasma nozzle, the process gas comprising a carbon- containing species; and means for supplying radio frequency radiation to the process gas within the plasma nozzle, so as to produce a plasma within the nozzle in use, and thereby cause cracking of the carbon-containing species;wherein the plasma nozzle is arranged such that an afterglow of the plasma extends into the reaction chamber, the cracked carbon-containing species also passes into the reaction chamber, and the cracked carbon-containing species recombines within the afterglow, so as to form graphitic products including graphene. A method of plasma-synthesising graphitic products including graphene is also provided.
摘要翻译：用于等离子体合成包括石墨烯在内的石墨产品的装置，包括：连接到反应室的等离子体喷嘴; 用于向等离子体喷嘴提供工艺气体的装置，所述工艺气体包含含碳物质; 以及用于向等离子体喷嘴内的处理气体提供射频辐射的装置，以便在使用中在喷嘴内产生等离子体，从而引起含碳物质的裂解;其中等离子体喷嘴被布置成使得等离子体喷嘴的余辉等离子体延伸到反应室中，含裂解的含碳物质也进入反应室，裂化的含碳物质在余辉内重新组合，形成包括石墨烯在内的石墨产物。还提供了包括石墨烯在内的等离子体合成石墨产品的方法。

4. 发明申请

WO2015040371A2 METHOD, SYSTEM AND INJECTION SUBSYSTEM FOR PRODUCING NANOTUBES 审中-公开
标题翻译：用于生产纳米管的方法，系统和注入子系统
公开(公告)号：WO2015040371A2
公开(公告)日：2015-03-26
申请号：PCT/GB2014/052792
申请日：2014-09-15
申请人： FGV CAMBRIDGE NANOSYSTEMS LIMITED , KOZIOL, Krzysztof Kazimierz , JOAUG, Jerome Yi-Zhe , PAUKNER, Catharina , KURZEPA, Lukasz
发明人： KOZIOL, Krzysztof Kazimierz , JOAUG, Jerome Yi-Zhe , PAUKNER, Catharina , KURZEPA, Lukasz
IPC分类号： C01B31/02
CPC分类号： C01B31/024 , B82Y30/00 , B82Y40/00 , C01B21/0646 , C01B32/162 , C01B32/164 , C01P2002/82 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/13 , C23C16/4557 , C23C16/45574 , C23C16/45578 , C30B25/00 , C30B29/403 , C30B29/602 , D01F9/08 , D01F9/133
摘要： A floating catalyst chemical vapour deposition method for producing nanotubes, the method including: supplying a nanotube-material precursor and a catalyst precursor, heating said precursors and injecting said precursors into a heated reaction chamber containing a process gas; pyrolysing the catalyst precursor within the reaction chamber to produce catalyst particles; and pyrolysing the nanotube-material precursor within the reaction chamber in the presence of the catalyst particles in order to produce nanotubes; wherein the method further comprises controlling the size of the catalyst particles at the point of pyrolysis of the nanotube-material precursor by controlling the operational parameters of the reaction chamber and/or of the precursor supplies. A corresponding system for producing nanotubes is also provided. Further provided is an injector subsystem for attachment to a reaction chamber, the injector subsystem comprising: a first portion having a first set of injection pipes for receiving species for delivery into the reaction chamber; and an interface portion that is removably attachable between the first portion and the reaction chamber in use, the interface portion comprising at least one injection pipe arranged to receive the species provided by the first set of injection pipes and to inject said species into the reaction chamber in use;the injector subsystem being operable in use such that, with the interface portion removed, said first set of injection pipes are operable to individually inject their respective species into the reaction chamber, and with the interface portion attached, a pre-mixing chamber is defined by the interface portion in combination with the first portion, for pre-mixing the species provided by the first set of injection pipes prior to the species entering the at least one injection pipe of the interface portion.
摘要翻译：一种用于制备纳米管的浮动催化剂化学气相沉积方法，所述方法包括：供应纳米管材料前体和催化剂前体，加热所述前体并将所述前体注入含有工艺气体的加热反应室中; 在反应室内热解催化剂前体以产生催化剂颗粒; 并在催化剂颗粒的存在下在反应室内热解纳米管材料前体以产生纳米管; 其中所述方法还包括通过控制所述反应室和/或所述前体供应的操作参数来控制所述纳米管材料前体热分解时所述催化剂颗粒的尺寸。还提供了一种生产纳米管的相应系统。还提供了一种用于连接到反应室的注射器子系统，所述注射器子系统包括：第一部分，其具有第一组注射管，用于接收用于递送到反应室中的物质; 以及接口部分，其在使用中可移除地附接在所述第一部分和所述反应室之间，所述界面部分包括至少一个注入管，所述至少一个注入管布置成接纳由所述第一组注射管提供的物种，并将所述物质注入所述反应室喷射器子系统在使用中是可操作的，使得在去除了界面部分的情况下，所述第一组喷射管可操作以将它们各自的物质单独地喷射到反应室中，并且在界面部分附接有预混合室由所述界面部分与所述第一部分组合限定，用于在所述物质进入所述界面部分的所述至少一个注射管之前，预先混合由所述第一组注射管提供的物种。

5. 发明申请

WO2015004467A3 MATERIALS AND METHODS FOR SOLDERING, AND SOLDERED PRODUCTS 审中-公开
公开(公告)号：WO2015004467A3
公开(公告)日：2015-01-15
申请号：PCT/GB2014/052105
申请日：2014-07-10
申请人： CAMBRIDGE ENTERPRISE LIMITED
发明人： BURDA, Marek , LEKAWA-RAUS, Agnieszka , KOZIOL, Krzysztof Kazimierz , GRUSZCZYK, Andrzej , GÓRKA, Jacek
IPC分类号： B23K35/26 , B23K35/36 , B23K35/02 , C22C13/00 , C22C13/02
摘要： A tin-based alloy consists essentially of: (i) matrix components comprising two or more of Ag, Cu, Sb, Bi, Pb, In, Zn, Cd, Ga, Au, Ge, Si, P, Al, each matrix component being present in an amount 0.01-6.0wt%; (ii) a transition metal active component comprising one or more of Cr, Ni, Ti, Co, Fe, Mn, Nb, Mo, Hf, Ta, W, the total amount of all said transition metal active components being more than 1.0 wt% and not more than 10wt%; (iii) C present in an amount 0.01-1.0wt%, and (iv) balance Sn and incidental impurities. Preferred compositions include Sn-(Ag, Cu, Sb, Bi, Pb)-(Cr, Ni)-C. The alloy is of use for soldering carbon-based materials such as carbon nanotubes.

6. 发明公开

EP3019303A2 MATERIALS AND METHODS FOR SOLDERING, AND SOLDERED PRODUCTS 审中-公开
标题翻译：用于焊接和产品材料和方法钎焊
公开(公告)号：EP3019303A2
公开(公告)日：2016-05-18
申请号：EP14739534.7
申请日：2014-07-10
申请人： Cambridge Enterprise Limited
发明人： BURDA, Marek , LEKAWA-RAUS, Agnieszka , KOZIOL, Krzysztof Kazimierz , GRUSZCZYK, Andrzej , GÓRKA, Jacek
IPC分类号： B23K35/26 , B23K35/36 , B23K35/02 , C22C13/00 , C22C13/02
CPC分类号： B23K35/0222 , B23K35/262 , B23K35/36 , C22C13/00 , C22C13/02 , H01B1/02 , H01B1/04
摘要： A tin-based alloy consists essentially of: (i) matrix components comprising two or more of Ag, Cu, Sb, Bi, Pb, In, Zn, Cd, Ga, Au, Ge, Si, P, Al, each matrix component being present in an amount 0.01-6.0 wt %; (ii) a transition metal active component comprising one or more of Cr, Ni, Ti, Co, Fe, Mn, Nb, Mo, Hf, Ta, W, the total amount of all said transition metal active components being more than 1.0 wt % and not more than 10 wt %; (iii) C present in an amount 0.01-1.0 wt %, and (iv) balance Sn and incidental impurities. Preferred compositions include Sn—(Ag, Cu, Sb, Bi, Pb)—(Cr, Ni)—C. The alloy is of use for soldering carbon-based materials such as carbon nanotubes.

7. 发明授权

EP2635523B1 METHOD OF MAKING CARBON NANOTUBES 有权
公开(公告)号：EP2635523B1
公开(公告)日：2018-11-28
申请号：EP11785758.1
申请日：2011-11-02
申请人： Cambridge Enterprise Limited
发明人： SUNDARAM, Rajyashree , KOZIOL, Krzysztof Kazimierz , LEKAWA-RAUS, Agnieszka Ewa , WINDLE, Alan
IPC分类号： C01B32/16 , C01B32/162 , B01J23/745 , B01J37/08 , D01F9/12 , D01F11/14 , D01F9/133 , D01F9/127 , B82Y40/00 , B82Y30/00 , B01J35/00
CPC分类号： C01B32/162 , B01J23/745 , B01J35/006 , B01J37/086 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B2202/22 , C01B2202/30 , C01B2202/36 , D01F9/127 , D01F9/1272 , D01F9/133 , D01F11/14 , Y10T428/268 , Y10T428/2927 , Y10T428/2982
摘要： The present invention relates to carbon materials comprising carbon nanotubes, powders comprising carbon nanotubes and methods of making carbon nanotubes. In the methods of the present invention, the size and/or formation of floating catalyst particles is closely controlled. The resulting carbon nanotubes typically exhibit armchair chirality and typically have metallic properties. The carbon nanotubes produced by this method readily form bulk materials, which typically have a conductivity of at least 0.7×106 Sm−1 in at least one direction. The invention has particular application to the manufacture of components such as electrical conductors. Suitable electrical conductors include wires (e.g. for electrical motors) and cables (e.g. for transmitting electrical power).

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