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1. 发明授权

US4892644A Upgrading solvent extracts by double decantation and use of pseudo extract as hydrogen donor 失效
标题翻译：通过双倾析提取溶剂提取物，并使用假提取物作为氢供体
公开(公告)号：US4892644A
公开(公告)日：1990-01-09
申请号：US256095
申请日：1988-10-07
申请人： Byung; C. Choi , Grant G. Karsner , Chang-Kuei Lee , Madhava Malladi , Donald Milstein
发明人： Byung; C. Choi , Grant G. Karsner , Chang-Kuei Lee , Madhava Malladi , Donald Milstein
IPC分类号： C10G21/00 , C10G47/34 , C10G67/00
CPC分类号： C10G67/00 , C10G21/00 , C10G47/34
摘要： A solvent extract obtained from a conventional hydrocarbon oil solvent extraction process, e.g., one employing furfural as the extraction solvent, is cooled to a temperature providing, following a secondary decantation of the cooled extract, a pseudo raffinate containing most of the non-aromatics and a pseudo extract possessing a hydro-aromatic content of H.sub.alpha hydrogen of at least 20 percent of the total hydrogen content. The pseudo extract is ideally suited as a hydrogen-donor for a variety of refinery operations such as visbreaking. The pseudo raffinate is suitable as a co-feed for such catalytic cracking operations as fluidized catalytic cracking (FCC) and thermofor catalytic cracking (TCC) and can be recycled to the extraction unit to produce more lube oil.
摘要翻译：将从常规烃油溶剂萃取方法得到的溶剂萃取物，例如使用糠醛作为萃取溶剂的溶剂萃取物冷却至一个温度，在冷却的萃取物的二次倾析后，提供含有大部分非芳族化合物的假萃余液和具有氢氢原子的氢 - 芳族含量至少为总氢含量的20％的假提取物。假萃取物非常适合用于各种炼油操作如减粘裂化的氢供体。假萃余液适合作为流化催化裂化（FCC）和热反应催化裂化（TCC）等催化裂化操作的共同进料，可以再循环至萃取单元以生产更多的润滑油。

2. 发明授权

US4071574A Conversion of Fischer-Tropsch heavy product to high quality jet fuel 失效
标题翻译：费托重产品转化为高品质喷气燃料
公开(公告)号：US4071574A
公开(公告)日：1978-01-31
申请号：US671451
申请日：1976-03-29
申请人： Donald Milstein , Thomas R. Stein
发明人： Donald Milstein , Thomas R. Stein
IPC分类号： C10G65/04 , C10L1/04 , C07C1/04 , C10G34/00
CPC分类号： C10L1/04 , C10G2400/08 , Y10S208/95 , Y10S585/943
摘要： Upgrading a Fischer-Tropsch synthesis product by separating a 350.degree. to 850.degree. F product fraction thereof into a 650.degree. F minus fraction and a 650.degree. F plus fraction; separating the 650.degree. F minus fraction to provide a more narrow 350.degree. to 650.degree. F fraction; combining the 650.degree. F plus fraction with a portion of the 350.degree. to 650.degree. F fraction to form a wide boiling range feed material; contacting this formed wide boiling range feed material, together with hydrogen, with a special catalyst comprising a crystalline aluminosilicate zeolite having a silica to alumina ratio of at least 12 and a constraint index of 1 to 12, at a temperature of about 500.degree. to 800.degree. F, a hydrogen partial pressure of about 100 to 800 psia and a space velocity of about 0.5 to 5 LHSV to produce a converted product thereof separating the zeolite conversion product to recover a 350.degree. F minus fraction from a 350.degree. F plus fractions; and separating the 350.degree. F plus fraction to recover a 350.degree. to 450.degree. F jet fuel fraction having a freeze point of less than about -58.degree. F.
摘要翻译：通过将350至850°F的产物馏分分离成650°F馏分和650°F加馏分来升级费 - 托合成产物; 分离650°F负分数以提供更窄的350°至650°F馏分; 将650°F加成分与350°至650°F馏分的一部分结合形成宽沸程饲料; 使该形成的大沸点范围的原料与氢一起使用包含二氧化硅与氧化铝比至少为12且约束指数为1至12的结晶硅铝酸盐沸石的特殊催化剂在约500至800℃的温度下接触 DEG F，约100至800psia的氢分压和约0.5至5LHSV的空速，以产生其转化产物，分离沸石转化产物以从350°F加馏分回收350°F的负分馏; 并分离350°F加馏分以回收冷冻点小于约-58°F的350°至450°F喷射燃料馏分。

3. 发明授权

US4298458A Low pressure hydrotreating of residual fractions 失效
$Low pressure hydrotreating of residual fractions$
标题翻译：残余馏分的低压加氢处理
公开(公告)号：US4298458A
公开(公告)日：1981-11-03
申请号：US124017
申请日：1980-02-25
申请人： Frederick Banta , Donald Milstein , Alan W. Peters
发明人： Frederick Banta , Donald Milstein , Alan W. Peters
IPC分类号： C10G45/02 , C10G47/00 , C10G47/12 , C10G45/08
CPC分类号： C10G45/02 , C10G47/00
摘要： Cyclic hydrotreating of resids with low pressure, short term on-stream periods yields desirable products.
摘要翻译：低压，短期运行期间的循环循环加氢处理产生理想的产物。

4. 发明授权

US4016067A Process for demetalation and desulfurization of petroleum oils 失效
标题翻译：石油脱盐脱硫工艺
公开(公告)号：US4016067A
公开(公告)日：1977-04-05
申请号：US551948
申请日：1975-02-21
申请人： Ronald H. Fischer , Donald Milstein
发明人： Ronald H. Fischer , Donald Milstein
IPC分类号： B01J35/10 , C10G65/04 , C10G23/02 , C10G23/16
CPC分类号： B01J35/10 , B01J35/1038 , B01J35/1042 , B01J35/1061 , C10G2300/107
摘要： This invention is concerned with removing metal and sulfur contaminants from residual oil fractions by catalytic contact in a novel dual bed system. In this process the oil is first contacted with a catalyst comprising a Group VIB metal and an iron group metal oxide, such as a mixture of cobalt and molybdenum oxides, composited with an alumina support that contains delta or theta phase alumina, the catalyst having at least 60% of its pore volume in pores of 100A to 200A diameter, at least about 5% of its pore volume in pores having a diameter greater than 500A, and a surface area up to about 110m.sup.2 /g. The oil is then contacted with a second catalyst of the high surface-area, cobalt-molybdenum on alumina type. The second catalyst has a major fraction of its pores in the 30 to 100A diameter range.
摘要翻译：本发明涉及通过新型双床系统中的催化接触从残余油馏分中除去金属和硫污染物。在该方法中，首先将油与催化剂接触，所述催化剂包含VIB族金属和铁族金属氧化物，例如钴和钼氧化物的混合物，与含有δ或θ相氧化铝的氧化铝载体复合，所述催化剂具有孔直径为100A至200A的孔体积的至少60％，孔直径大于500A的孔体积的至少约5％，表面积高达约110m2 / g。然后将油与高表面积的氧化铝型钴 - 钼的第二催化剂接触。第二种催化剂在30至100A直径范围内具有大部分孔。

5. 发明授权

US4421633A Low pressure cyclic hydrocracking process using multi-catalyst bed reactor for heavy liquids 失效
标题翻译：用于重液体的多催化床反应器的低压循环加氢裂化方法
公开(公告)号：US4421633A
公开(公告)日：1983-12-20
申请号：US243414
申请日：1981-03-13
申请人： Stuart S. Shih , Donald Milstein
发明人： Stuart S. Shih , Donald Milstein
IPC分类号： C10G47/12 , C10G65/10 , C10G69/02 , C10G45/08 , C10G47/04
CPC分类号： C10G47/12 , C10G2300/107
摘要： Resids are hydrocracked at low pressure (600 psig and 825.degree. F.) in a solvent, while being demetalated, desulfurized, and decarbonized, by passing the solution through a dual-bed catalytic system having a large-pore catalyst as the first bed and a small-pore as the second bed. The solvent is preferably process generated and recycled, boiling at about 400.degree.-700.degree. F.
摘要翻译：将溶液在溶剂中在低压（600psig和825°F）下进行加氢裂化，同时通过使溶液通过具有大孔催化剂作为第一床的双床催化体系进行脱金属脱硫，脱硫和脱碳，以及一个小孔作为第二个床。溶剂优选在约400-700°F下进行生产和回收，沸腾。

6. 发明授权

US4271042A Process for demetalation and desulfurization of petroleum oils 失效
标题翻译：石油脱盐脱硫工艺
公开(公告)号：US4271042A
公开(公告)日：1981-06-02
申请号：US65707
申请日：1979-08-10
申请人： Stephen M. Oleck , Howard S. Sherry , Ronald H. Fischer , Donald Milstein
发明人： Stephen M. Oleck , Howard S. Sherry , Ronald H. Fischer , Donald Milstein
IPC分类号： B01J21/04 , B01J23/85 , B01J35/10 , B01J37/08 , C10G45/08 , B01J27/02 , B01J23/16
CPC分类号： B01J37/08 , B01J21/04 , B01J23/85 , B01J35/10 , B01J35/1019 , B01J35/1042 , B01J35/1061 , B01J35/109 , C10G2300/107
摘要： This invention is concerned with removing metal and sulfur contaminants from residual oil fractions by catalytic contact with an improved catalyst comprising the oxides or sulfides of a Group VIB metal and an iron group metal supported on an alumina that contains dispersed Delta and/or Theta phase alumina, the catalyst having at least 45% of its pore volume in pores 30 to 150A diameter, at least 10% of its pore volume in pores less than 30A diameter, and at least 15% of its pore volume in pores greater than 300A diameter. The process can be used to prepare feedstock for catalytic cracking.
摘要翻译：本发明涉及通过与包含第VIB族金属的氧化物或硫化物和负载在氧化铝上的铁族金属的改进的催化剂催化接触来除去残余油馏分中的金属和硫污染物，其含有分散的三角洲和/或Theta相氧化铝催化剂具有孔直径30至150A的孔中至少45％的孔体积，至少孔径小于30A直径孔隙体积的至少10％，以及孔径大于300A的孔体积的至少15％。该方法可用于制备催化裂化原料。

7. 发明授权

US4054508A Demetalation and desulfurization of residual oil utilizing hydrogen and trickle beds of catalysts in three zones 失效
标题翻译：在三个区域中利用氢气和催化剂滴液池对残油进行脱金属脱硫
公开(公告)号：US4054508A
公开(公告)日：1977-10-18
申请号：US754813
申请日：1976-12-27
申请人： Donald Milstein , Ronald H. Fischer
发明人： Donald Milstein , Ronald H. Fischer
IPC分类号： B01J35/10 , C10G65/04 , C10G23/02
CPC分类号： B01J35/10 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J35/1061 , B01J35/1066 , C10G2300/107
摘要： This invention is concerned with removing metal and sulfur contaminants from residual oil fractions by catalytic contact with two different catalysts in the presence of hydrogen. In this process, the oil is first contacted with the major fraction of a catalyst comprising a Group VIB metal and an iron group metal oxide, such as a mixture of cobalt and molybdenum oxides, composited with an alumina support, the catalyst having at least 60% of its pore volume in pores of 100A to 200A diameter and at least about 5% of its pore volume in pores having a diameter greater than 500A. The oil is then contacted with a secondcatalyst of the high surface-area, cobalt-molybdenum on alumina type having a major fraction of its pores in the 30 to 100A diameter range. Finally, the oil is contacted with the remainder of the large-pore catalyst.
摘要翻译：本发明涉及通过在氢气存在下与两种不同的催化剂进行催化接触从残留油馏分中除去金属和硫污染物。在该方法中，首先将油与主要部分与含有VIB金属和铁基金属氧化物的催化剂接触，所述催化剂包括与氧化铝载体复合的钴和钼氧化物的混合物，所述催化剂具有至少60 在100A至200A直径的孔中的孔体积的百分比以及其直径大于500A的孔中的孔体积的至少约5％。然后将油与高表面积的氧化铝型钴 - 钼的第二催化剂接触，其中孔的主要部分在30至100A直径范围内。最后，油与剩余的大孔催化剂接触。

8. 发明授权

US4044064A Conversion of Fischer-Tropsch heavy product to high quality jet fuel 失效
标题翻译：费托重产品转化为高品质喷气燃料
公开(公告)号：US4044064A
公开(公告)日：1977-08-23
申请号：US671511
申请日：1976-03-29
申请人： Donald Milstein , Thomas R. Stein
发明人： Donald Milstein , Thomas R. Stein
IPC分类号： C10G45/64 , C10G65/04 , F02B3/06 , C07C1/04
CPC分类号： C10G65/043 , C10G45/64 , F02B3/06 , Y10S208/95
摘要： Upgrading a fraction of a heavy Fischer-Tropsch oil to jet fuel by hydropretreating a 350.degree. to 850.degree. F boiling fraction; separating the hydrotreated product into a 650.degree. F minus and a 650.degree. F plus fraction, separating the650.degree. F minus fraction to provide a 350.degree. F minus naphtha boiling range fraction and a 350.degree. to 650.degree. F light distillate fraction; distilling the 350.degree. to 650.degree. F hydrotreated fraction to provide a fraction boiling in the range of 350.degree. F to 550.degree. F separate from a 550.degree. to 650.degree. F fraction processing either of the 650.degree. F plus fraction above separated or the 350.degree. to 550.degree. F boiling fraction above obtained over a catalyst comprising a crystalline aluminosilicate zeolite having a silica to alumina ratio of at least 12 and a constraint index of 1 to 12 with hydrogen, at a temperature of about 500.degree. to 800.degree. F, a hydrogen partial pressure of about 100 to 800 psig and a space velocity in the range of about 0.5 to 5 LHSV to produce a converted product comprising lower boiling hydrocarbons than the feed charged and recovering as a product of the process a reduced pour point diesel oil fraction, a 350.degree. to 550.degree. F jet fuel fraction, and a 350.degree. F minus naphtha product fraction.
摘要翻译：通过加氢分解350至850°F的沸点，将一部分重的费 - 托油升级成喷气燃料; 将加氢处理的产物分离成650°F和650°F加馏分，分离出650°F的馏分，得到350°F的减碳馏分沸点馏分和350至650°F馏分馏分。蒸馏出350°F至650°F的加氢处理馏分，以提供350°F至550°F沸点的馏分，分馏于550°F至650°F馏分，加工分离的650°F加馏分或350 通过包含二氧化硅与氧化铝之比至少为12的结晶硅铝酸盐沸石和氢的约束指数为1至12的催化剂，在约500至800°F的温度下，约100至800psig的氢分压和约0.5至5LHSV范围内的空速，以产生包含低于加入的原料的低沸点烃的转化产物，并将该还原的倾点柴油作为该方法的产物回收馏分，350〜550°F的燃油馏分和350°F的减碳馏出物馏分。

9. 发明授权

US4089774A Process for demetalation and desulfurization of petroleum oils 失效
标题翻译：石油脱盐脱硫工艺
公开(公告)号：US4089774A
公开(公告)日：1978-05-16
申请号：US807764
申请日：1977-06-17
申请人： Stephen M. Oleck , Howard S. Sherry , Ronald H. Fischer , Donald Milstein
发明人： Stephen M. Oleck , Howard S. Sherry , Ronald H. Fischer , Donald Milstein
IPC分类号： B01J21/04 , B01J23/85 , B01J27/04 , B01J35/10 , C10G45/04 , C10G45/08 , C10G23/02
CPC分类号： B01J35/10 , B01J35/1019 , B01J35/1042 , B01J35/1057 , B01J35/1061 , B01J35/109 , C10G2300/107
摘要： This invention is concerned with removing metal and sulfur contaminants from residual oil fractions by catalytic contact with an improved catalyst comprising the oxides or sulfides of a Group VIB metal and an iron group metal supported on an alumina that contains dispersed Delta and/or Theta phase alumina, the catalyst having at least 45% of its pore volume in pores 30 to 150A diameter, at least 10% of its pore volume in pores less than 30A diameter, and at least 15% of its pore volume in pores greater than 300A diameter. The process can be used to prepare feedstock for catalytic cracking.
摘要翻译：本发明涉及通过与包含第VIB族金属的氧化物或硫化物和负载在氧化铝上的铁族金属的改进的催化剂催化接触来除去残余油馏分中的金属和硫污染物，其含有分散的三角洲和/或Theta相氧化铝催化剂具有孔直径30至150A的孔中至少45％的孔体积，至少孔径小于30A直径孔隙体积的至少10％，以及孔径大于300A的孔体积的至少15％。该方法可用于制备催化裂化原料。

10. 发明授权

US3985643A Demetalation and desulfurization of oil in separate catalytic zones 失效
标题翻译：单独催化区油分离脱硫
公开(公告)号：US3985643A
公开(公告)日：1976-10-12
申请号：US501317
申请日：1974-08-28
申请人： Donald Milstein
发明人： Donald Milstein
IPC分类号： C10G65/04 , C10G23/00
CPC分类号： C10G65/04 , C10G2300/107
摘要： An improved process for desulfurization of metals and sulfur containing petroleum oils, preferably those containing residua hydrocarbon components, comprising passing the sulfur containing petroleum oils through a bed of substantially aged desulfurization catalyst at a temperature not less than 770.degree.F preceeding conventional hydrodesulfurization treatment.
摘要翻译：一种用于金属和含硫的石油，优选含有残留烃组分的脱硫的改进方法，包括在常规加氢脱硫处理之前不低于770°F使含硫油的石油进入基本老化的脱硫催化剂床。

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