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1. 发明授权

US5679147A Water-based organic polysiloxane-containing compositions, processes for their preparation and their use 失效
标题翻译：含水基有机聚硅氧烷的组合物，其制备方法及其应用
公开(公告)号：US5679147A
公开(公告)日：1997-10-21
申请号：US569900
申请日：1995-12-08
申请人： Burkhard Standke , Christine Fliedner , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Hans-Guenther Srebny
发明人： Burkhard Standke , Christine Fliedner , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Hans-Guenther Srebny
IPC分类号： C08L83/08 , B01F17/54 , C08G77/26 , C08G77/28 , C08L83/04 , C09D183/08
CPC分类号： C09D183/08 , C08G77/26
摘要： Water-based organopolysiloxane-containing compositions which are essentially free from organic solvents, have a flashpoint above 80.degree. C., and essentially liberate no alcohols by hydrolysis on dilution with water are obtainable by mixing water-soluble aminoalkylalkoxysilanes with alkyltrialkoxysilanes and/or dialkyldialkoxysilanes and/or mixtures of alkyltrialkoxysilanes and dialkyldialkoxysilanes which are not water-soluble, adding water to the mixture, adjusting the pH of the reaction mixture to a value of between 1 and 8 and removing any alcohol already present and/or formed during the reaction. Such compositions are especially useful for hydrophobicizing the surface of building materials such as brick, concrete, lime sand brick, and mortar.
摘要翻译：基本上不含有机溶剂的含水基的含有机基聚硅氧烷的组合物的闪点高于80℃，通过水稀释基本上不通过水解释放醇，可通过将水溶性氨基烷基烷氧基硅烷与烷基三烷氧基硅烷和/或二烷基二烷氧基硅烷混合而获得， /或不是水溶性的烷基三烷氧基硅烷和二烷基二烷氧基硅烷的混合物，向混合物中加入水，将反应混合物的pH调节至1至8的值，并除去反应中已经存在和/或形成的任何醇。这样的组合物特别可用于将建筑材料的表面疏水化，例如砖，混凝土，石灰砂砖和砂浆。

2. 发明授权

US5646325A Process for the preparation of 3-acryloyloxypropylalkoxysilanes 失效
标题翻译： 3-丙烯酰氧基丙基烷氧基硅烷的制备方法
公开(公告)号：US5646325A
公开(公告)日：1997-07-08
申请号：US533313
申请日：1995-09-25
申请人： Jaroslaw Monkiewicz , Albert Frings , Michael Horn , Peter Jenkner , Hans-Joachim Koetzsch , Frank Kropfgans , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
发明人： Jaroslaw Monkiewicz , Albert Frings , Michael Horn , Peter Jenkner , Hans-Joachim Koetzsch , Frank Kropfgans , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
IPC分类号： B01J31/12 , C07B61/00 , C07F7/18 , C07F7/08
CPC分类号： C07F7/1876
摘要： 3-Acryloyloxypropylalkoxysilanes of formula I:CH.sub.2 .dbd.C(R)C(O)O(CH.sub.2).sub.3 Si(R.sup.1).sub.a (OR.sup.2).sub.3-a (I)are prepared by reacting a hydridosilane of formula II:HSi(R.sup.1).sub.a (OR.sup.2).sub.3-a (II)with an allyl ester of formula III:CH.sub.2 .dbd.C(R)C(O)OCH.sub.2 CH.dbd.CH.sub.2 (III),where R is a hydrogen atom or a methyl group, R.sup.1 and R.sup.2 are each C.sub.1 to C.sub.6 alkyl groups or phenyl groups, and a is 0, 1 or 2, in the presence of a platinum catalyst.
摘要翻译：通式I的氢化硅烷：HSi（R1）a（I）通过使式II的氢化硅烷反应来制备式I的3-丙烯酰氧基丙基烷氧基硅烷：CH 2 = C（R）C（O）O（CH 2）3 Si （OR 2）3-a（II）与式III的烯丙基酯：CH 2 = C（R）C（O）OCH 2 CH = CH 2（III），其中R是氢原子或甲基， C1-C6烷基或苯基，a是0,1或2，在铂催化剂的存在下。

3. 发明授权

US5616762A Process for the preparation of 3-halo-and pseudohalo-alkylsilane esters 失效
标题翻译： 3-卤代 - 和拟卤代烷基硅烷酯的制备方法
公开(公告)号：US5616762A
公开(公告)日：1997-04-01
申请号：US548131
申请日：1995-10-25
申请人： Frank Kropfgans , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
发明人： Frank Kropfgans , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
IPC分类号： B01J31/02 , C07B61/00 , C07F7/08 , C07F7/10 , C07F7/18
CPC分类号： B01J31/02 , C07B61/00 , C07F7/08 , C07F7/10 , C07F7/18
摘要： 3-Halo- and pseudohalo-alkylsilane esters are prepared by reacting an allyl X compound or a compound containing an allyl X structure with a hydridosilane ester in the presence of an iridium catalyst prepared under specific conditions and/or the reaction medium containing a 0.01-100 mol % excess of the allyl X compound or compound containing the allyl X unit relative to the amount of hydridosilane ester reactant.
摘要翻译： 3-卤代和假卤代烷基硅烷酯是通过烯丙基X化合物或含有烯丙基X结构的化合物与氢化硅烷酯在特定条件下制备的铱催化剂和/或含有0.01- 100摩尔％过量的烯丙基X化合物或含有烯丙基X单元的化合物相对于氢硅烷酯反应物的量。

4. 发明授权

US5527937A Process for preparing hydrogenalkoxysilanes 失效
标题翻译：制备氢烷氧基硅烷的方法
公开(公告)号：US5527937A
公开(公告)日：1996-06-18
申请号：US538636
申请日：1995-10-04
申请人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny
发明人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny
IPC分类号： B01J27/122 , C07B61/00 , C07F7/02 , C07F7/04 , C07F7/18
CPC分类号： C07F7/025
摘要： Hydrogenalkoxysilanes are prepared by direct reaction of finely divided metallic silicon with alcohols in the presence of copper-containing catalysts in a heat-transfer oil comprising tritoluenes, tetratoluenes or mixtures thereof at from 100.degree. to 350.degree. C.
摘要翻译：在含铜催化剂存在下，在100-350℃的含三木聚四烯或其混合物的传热油中，通过细分的金属硅与醇的直接反应来制备氢烷氧基硅烷。

5. 发明授权

US5654459A Process for preparing alkylhydrogenchlorosilanes 失效
标题翻译：制备烷基氢氯硅烷的方法
公开(公告)号：US5654459A
公开(公告)日：1997-08-05
申请号：US659819
申请日：1996-06-07
申请人： Frank Kropfgans , Albert Frings , Michael Horn , Peter Jenkner , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
发明人： Frank Kropfgans , Albert Frings , Michael Horn , Peter Jenkner , Hans-Joachim Koetzsch , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
IPC分类号： B01J21/04 , B01J21/06 , B01J27/08 , C07B61/00 , C07F7/12 , C07F7/08
CPC分类号： C07F7/125
摘要： Alkylhydrogenchlorosilanes of formula I:R.sub.x HSiCl.sub.y (I)wherein R are identical or different alkyl radicals, x is 1 or 2 and y is 1 or 2 and the sum of x and y is equal to 3, are prepared by comproportionating alkylchlorosilanes of formula II:R.sub.a SiCl.sub.n (II)wherein R denotes identical or different alkyl radicals, a is 1 or 2 and n is 2 or 3 and the sum of a and n is equal to 4 with hydrogenchlorosilanes of formula III:R.sub.b H.sub.c SiCl.sub.4-b-c (III)wherein R denotes identical or different alkyl radicals, b is 0, 1, 2 or 3 and c is 1, 2, 3 or 4 and the sum of b and c is equal to or smaller than 4, in the presence of a catalyst saturated with a hydrogen halide.
摘要翻译：式I的烷基氢氯硅烷：RxHSiCly（I）其中R是相同或不同的烷基，x是1或2，y是1或2，x和y的和等于3，是通过对式II的烷基氯代硅烷进行配比制备的： RaSiCln（II）其中R表示相同或不同的烷基，a为1或2，n为2或3，a和n之和等于4与式III的氢氯硅烷：RbHcSiCl4-bc（III）其中R表示相同或不同的烷基，b为0,1,2或3，c为1,2,3或4，b和c的总和等于或小于4，在饱和氢气的催化剂存在下卤化物。

6. 发明授权

US5536860A Process for preparing aminopropylalkoxysilanes in the presence of shaped polymeric rhodium complex catalysts and their use 失效
标题翻译：在形成聚合物铑配合物催化剂存在下制备氨基丙基烷氧基硅烷的方法及其应用
公开(公告)号：US5536860A
公开(公告)日：1996-07-16
申请号：US538634
申请日：1995-10-04
申请人： Jaroslaw Monkiewicz , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Frank Kropfgans , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
发明人： Jaroslaw Monkiewicz , Albert Frings , Michael Horn , Hans-Joachim Koetzsch , Frank Kropfgans , Claus-Dietrich Seiler , Hans-Guenther Srebny , Burkhard Standke
IPC分类号： B01J31/24 , C07B61/00 , C07F7/18 , C07F7/10
CPC分类号： C07F7/1876
摘要： Aminopropylalkoxysilanes of formula (I):R.sup.2 R.sup.3 NCH.sub.2 CHR.sup.4 CH.sub.2 Si(OR).sub.3-n (R.sup.1).sub.n(I)are prepared by reacting hydrogensilanes of formula (II):HSi(OR).sub.3n (R.sup.1).sub.n (II)with an amine of formula (III):R.sup.2 R.sup.3 NCH.sub.2 CR.sup.4 .dbd.CH.sub.2 (III),where R and R.sup.1 are alkyl radicals having from 1 to 8 carbon atoms and n is equal to 0, 1 or 2 andR.sup.2 and R.sup.3 are hydrogen, alkyl radicals having from 1 to 8 carbon atoms, .omega.-alkenyl radicals having from 3 to 8 carbon atoms or combinations thereof, andR.sup.4 is hydrogen or an alkyl radical having from 1 to 8 carbon atoms, in the presence of a shaped polymeric rhodium complex catalyst containing organosiloxanemonophenylphosphine ligands.
摘要翻译：式（I）的氨基丙基烷氧基硅烷：R2R3NCH2CHR4CH2Si（OR）3-n（R1）n（I）是通过使式（II）的氢硅烷：HSi（OR）3n（R1）n（II） III）：R2R3NCH2CR4 = CH2（III），其中R和R1是具有1至8个碳原子的烷基，n等于0,1或2，R2和R3是氢，具有1至8个碳原子的烷基，具有3至8个碳原子的ω-链烯基或其组合，R4是氢或具有1至8个碳原子的烷基，在含有有机硅氧烷基苯基膦配体的成形聚合铑配合物催化剂的存在下。

7. 发明授权

US5629400A Water-based organopolysiloxane-containing compositions, processes for their preparation and their use 失效
标题翻译：含水基的含有机聚硅氧烷的组合物，其制备方法及其用途
公开(公告)号：US5629400A
公开(公告)日：1997-05-13
申请号：US568384
申请日：1995-12-06
申请人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Kotzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Jim Steinmetz
发明人： Burkhard Standke , Albert Frings , Michael Horn , Hans-Joachim Kotzsch , Frank Kropfgans , Jaroslaw Monkiewicz , Claus-Dietrich Seiler , Jim Steinmetz
IPC分类号： C08L83/08 , B01F17/54 , C08G77/26 , C08G77/28 , C08L83/04 , C09D183/04 , C09D183/08 , C09J183/00 , C09J183/08
CPC分类号： C09D183/08 , C08G77/26
摘要： The invention relates to water-based organopolysiloxane containing compositions which are essentially free from organic solvents, have a flash point above 70.degree. C. and essentially liberate no alcohols by hydrolysis on dilution with water. The organopolysiloxane-containing compositions according to the invention are obtainable by mixing M mol of water-insoluble organotrialkoxysilanes with Q mol of water-soluble aminoalkylalkoxysilanes in a molar ratio of 0
摘要翻译：本发明涉及基本上不含有机溶剂的含水基有机聚硅氧烷的组合物，其闪点高于70℃，并且在用水稀释时基本上不通过水解释放醇。根据本发明的含有机聚硅氧烷的组合物可通过将M摩尔不溶于水的有机三烷氧基硅烷与摩尔比为0

8. 发明授权

US5932757A Mixture of oligomers of condensed alkylalkoxysilanes 失效
标题翻译：缩合的烷基烷氧基硅烷的低聚物的混合物
公开(公告)号：US5932757A
公开(公告)日：1999-08-03
申请号：US877556
申请日：1997-06-17
申请人： Burkhard Standke , Roland Edelmann , Albert Frings , Michael Horn , Peter Jenkner , Ralf Laven , Jaroslaw Monkiewicz , Lothar Elfenthal , Hans-Hermann Luginsland
发明人： Burkhard Standke , Roland Edelmann , Albert Frings , Michael Horn , Peter Jenkner , Ralf Laven , Jaroslaw Monkiewicz , Lothar Elfenthal , Hans-Hermann Luginsland
IPC分类号： C07F7/18 , B01J2/30 , C07F7/08 , C07F7/21 , C08G77/04 , C09D183/04
CPC分类号： B01J2/30 , C07F7/0859 , C07F7/21 , C08G77/045 , C09D183/04
摘要： A mixture of oligomers of alkylalkoxysilanes condensed in the chain and/or cyclic form, said mixture of oligomers containing less than 2% by weight of free alcohols and the condensed alkoxysilanes satisfying formula I: ##STR1## wherein R is an alkyl group having 3 to 18 carbon atoms, and each R' is a member (i) selected from the group consisting of methyl, ethyl or hydrogen, or is (ii) methyl or hydrogen, or is (iii) ethyl or hydrogen, the degree of oligomerization being in the range 2.ltoreq.x.ltoreq.20 and the quotient of the molar ratio �Si/alkoxy group!.gtoreq.1; and/orsatisfying formula II: ##STR2## in which R is an alkyl group having 3 to 18 carbon atoms, and each R' is a member (i) selected from the group consisting of methyl, ethyl or hydrogen, or is (ii) methyl or hydrogen or is (iii) ethyl or hydrogen, the degree of oligomerization being x.gtoreq.3 and the quotient of the molar ratio �Si/alkoxy group!.gtoreq.1.
摘要翻译：以链和/或环状缩合的烷基烷氧基硅烷的低聚物的混合物，所述含低于2重量％游离醇的低聚物混合物和满足式I的缩合烷氧基硅烷：其中R是具有3至18个碳原子的烷基，并且每个R'是选自甲基，乙基或氢的成员（i），或（ii）甲基或氢，或（iii）乙基或氢，低聚度的范围为2 = 1的商; 和/或满足式II：其中R是具有3至18个碳原子的烷基，并且每个R'是选自甲基，乙基或氢的成员（i），或者是（ⅱ）甲基或氢或是（ⅲ）乙基或氢，低聚度为x≥3，摩尔比[Si /烷氧基]> = 1的商。

9. 发明授权

US6020448A N-[.omega.-(methyl),.omega.-(silyl)] alkyl-N-organocarboxamides, oligomeric and polycondensed Si-containing compounds thereof, processes for their preparation, and their use 失效
标题翻译： N-（ω-（甲基），ω-（甲硅烷基）]烷基-N-有机碳酰胺，其低聚和缩聚的含Si化合物，其制备方法及其用途
公开(公告)号：US6020448A
公开(公告)日：2000-02-01
申请号：US98530
申请日：1998-06-17
申请人： Peter Jenkner , Albert Frings , Michael Horn , Jaroslaw Monkiewicz , Burkhard Standke
发明人： Peter Jenkner , Albert Frings , Michael Horn , Jaroslaw Monkiewicz , Burkhard Standke
IPC分类号： C07F7/18 , C08G77/26 , C09D183/08 , C09J183/08 , C08G77/04
CPC分类号： C08G77/26 , C07F7/1836
摘要： N-[.omega.-(methyl),.omega.-(silyl)]alkyl-N-organocarboxamides, oligomeric and polycondensed Si-containing compounds thereof, or mixtures of the corresponding monomeric, oligomeric and polycondensed Si-containing compounds. These materials are useful as, for example, adhesion promoters and for coating surfaces.
摘要翻译： N-（ω-（甲基），ω-（甲硅烷基）]烷基-N-有机碳酰胺，其低聚和缩聚的含Si化合物，或相应的单体，低聚和缩聚的含Si化合物的混合物。这些材料可用作例如粘合促进剂和涂层表面。

10. 发明授权

US07371881B2 Process for the preparation of organosilicon compounds 有权
标题翻译：制备有机硅化合物的方法
公开(公告)号：US07371881B2
公开(公告)日：2008-05-13
申请号：US11497633
申请日：2006-08-02
申请人： Albert Frings , Louis Janssens , Stefan Lotter , Ulrich Deschler , Alfred Alig
发明人： Albert Frings , Louis Janssens , Stefan Lotter , Ulrich Deschler , Alfred Alig
IPC分类号： C07F7/08
CPC分类号： C07F7/1892
摘要： A process for the preparation of an organosilicon compound of the formula (I) (R1R2R3SiR4)2Sx (I) by reacting haloalkoxysilanes of the general formula (II) R1R2R3SiR4X (II) with a dry polysulphide of the general formula (III) M2Sz (III) and/or dry sulphide of the general formula IV M2S (IV) and optionally sulphur in an organic solvent, the organic solvent being removed from the resulting suspension, the mixture containing the organosilicon compound of the general formula (I) and the solid MX being mixed with water containing at least one buffer, and the resulting phases being separated.
摘要翻译：制备式（I）的有机硅化合物的方法<？in-line-formula description =“In-line Formula”end =“lead”→>（R 1） > 2 3 S S S 通过使通式（II）的卤代烷氧基硅烷与式（II）中的<？in-line-formula description =“In-Line Formulas”end =“lead”→> R X（II）<β在线公式描述=“In” 用“通式（III）”表示的干燥多硫化物“-line”=“尾”→“in-line-formula description =”In-line Formulas“end =”lead“？> M＆（III）<？in-line-formula description =“In-line Formulas”end =“tail”？>和/或通式IV <β的干硫化物 -line-formula description =“In-line Formulas”end =“lead”？> M 2 S（IV）<？in-line-formula description =“In-line Formulas”end =“ 尾“→和有机溶剂中的硫，有机溶剂从所得悬浮液中除去含有通式（I）的有机硅化合物和固体MX的混合物与含有至少一种缓冲液的水混合，并将所得相分离。

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