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1. 发明授权

US5173556A Fluorinated copolymer and barrier films 失效
标题翻译：氟化共聚物和阻隔膜
公开(公告)号：US5173556A
公开(公告)日：1992-12-22
申请号：US696414
申请日：1991-05-06
申请人： Frank Mares , Bryce C. Oxenrider , David J. Long , John P. Sibilia
发明人： Frank Mares , Bryce C. Oxenrider , David J. Long , John P. Sibilia
IPC分类号： C08F8/12 , C08F214/18 , C08F218/04
CPC分类号： C08F214/186 , C08F218/04 , C08F8/12 , C08J5/18 , C08F2810/50
摘要： The present invention is directed to a copolymer of a fluoromonomer having the formula R.sub.1 R.sub.2 C.dbd.CR.sub.3 F wherein R.sub.1, R.sub.2 and R.sub.3 are selected from H and F, and R.sub.3 may be Cl when R.sub.1 and R.sub.2 are F; and a vinyl monomer having the formula H.sub.2 C.dbd.CHR.sub.x, wherein R.sub.x is a radical having the formula --O.sub.2 CR.sub.y, wherein R.sub.y is a radical selected from CH.sub.3 and C.sub.2 H.sub.5.The resulting copolymer comprises fluorinated units having the formula (R.sub.1 R.sub.2 C--CR.sub.3 F) wherein R.sub.1, R.sub.2 and R.sub.3 are selected from H and F, and R.sub.3 may be Cl when R.sub.1 and R.sub.2 are F, and corresponding amounts of vinyl units having the formula (H.sub.2 C--CHR.sub.x), wherein R.sub.x is selected from --CH.sub.3 and C.sub.2 H.sub.5. In an alternate and preferred embodiment the copolymer is hydrolyzed so that R.sub.x becomes --OH.
摘要翻译：本发明涉及式R1R2C = CR3F的含氟单体的共聚物，其中R 1，R 2和R 3选自H和F，当R 1和R 2为F时，R 3可以为Cl; 和具有式H2C = CHRx的乙烯基单体，其中Rx是具有式-O2CRy的基团，其中Ry是选自CH3和C2H5的基团。所得共聚物包括具有式（R 1 R 2 C-CR 3 F）的氟化单元，其中R 1，R 2和R 3选自H和F，当R 1和R 2为F时，R 3可为Cl，并且相应量的具有式 -CHRx），其中Rx选自-CH 3和C 2 H 5。在替代和优选的实施方案中，共聚物被水解，使得Rx变成-OH。

2. 发明授权

US5194667A Fiber surface modifiers 失效
标题翻译：纤维表面改性剂
公开(公告)号：US5194667A
公开(公告)日：1993-03-16
申请号：US488201
申请日：1990-03-05
申请人： Bryce C. Oxenrider , David J. Long
发明人： Bryce C. Oxenrider , David J. Long
IPC分类号： A01N37/12 , C07C219/14 , C07F7/18 , D06M15/507 , D06M16/00 , F16H61/02 , F16H61/04
CPC分类号： D06M15/507 , A01N37/12 , C07C219/14 , C07F7/1836 , D06M16/00 , F16H61/0267 , F16H61/04 , Y10T428/2969
摘要： This invention relates to fiber surface treating agnets containing a pyromellitate nucleus which have fungicidal, anti-microbial and anti-static properties, and blends of such agents with other types of surface modifiers.
摘要翻译：本发明涉及含有具有杀真菌，抗微生物和抗静电特性的均苯四酸根核的纤维表面处理剂，以及这些试剂与其它类型表面改性剂的共混物。

3. 发明授权

US4435294A Polycyclic pyromellitates and use thereof on polyesters and polyamides 失效
标题翻译：多环苯并四唑酸酯及其在聚酯和聚酰胺上的应用
公开(公告)号：US4435294A
公开(公告)日：1984-03-06
申请号：US429945
申请日：1982-09-30
申请人： Bryce C. Oxenrider , David J. Long
发明人： Bryce C. Oxenrider , David J. Long
IPC分类号： D06M13/213 , C07C153/07 , D06M13/20
CPC分类号： D06M13/213 , Y10T428/2969
摘要： Oligomers containing pyromellitic rings, divalent linking groups, pendant fluoroalkoxy or hydrocarbon alkoxy groups and pendant polar groups of various kinds impart soil repellency to fibers that persists after repeated laundering. An exemplary material is prepared by the reaction of pyromellitic difluoroester/diacid chloride with 1,4-butanediol (the linking group) and 3-chloro-1,2-propanediol (the pendant polar group).
摘要翻译：含有均苯四甲酸环，二价连接基团，氟代烷氧基或烃烷氧基侧基和各种侧挂极性基团的低聚物，对反复洗涤后持续存在的纤维赋予疏水性。通过均苯四甲酸二氟酯/二酰氯与1,4-丁二醇（连接基）和3-氯-1,2-丙二醇（侧极基团）的反应制备示例性材料。

4. 发明授权

US4939289A Fiber surface modifiers 失效
标题翻译：纤维表面改性剂
公开(公告)号：US4939289A
公开(公告)日：1990-07-03
申请号：US190987
申请日：1988-05-06
申请人： Bryce C. Oxenrider , David J. Long
发明人： Bryce C. Oxenrider , David J. Long
IPC分类号： A01N37/12 , C07C219/14 , C07F7/18 , D06M15/507 , D06M16/00
CPC分类号： A01N37/12 , C07C219/14 , C07F7/1836 , D06M15/507 , D06M16/00 , Y10T428/31721 , Y10T428/31736
摘要： This invention relates to fiber surface treating agents containing a pyromellitate nucleus which have fungicidal, anti-microbial and anti-static properties, and blends of such agents with other types of surface modifiers.
摘要翻译：本发明涉及含有具有杀真菌，抗微生物和抗静电性能的均苯四酸根核的纤维表面处理剂，以及这些试剂与其它类型表面改性剂的共混物。

5. 发明授权

US4537728A Fluorinated and non-fluorinated terminally halogenated alkyl pyromellitates 失效
标题翻译：氟化和非氟化的末端卤代烷基苯甲酸酯
公开(公告)号：US4537728A
公开(公告)日：1985-08-27
申请号：US431452
申请日：1982-09-30
申请人： Bryce C. Oxenrider , David J. Long
发明人： Bryce C. Oxenrider , David J. Long
IPC分类号： C07C69/76 , C07C153/07 , C07C101/20 , C07C101/24 , C07C101/26
CPC分类号： C07C69/76
摘要： Novel polycarboxy benzene dianhydrides useful as surfactants are disclosed. The novel compounds of this invention are pyromellitate tetraesters wherein two ester moieties characteristically contain fluorinated alkyl groups or saturated hydrocarbon alkyl groups and wherein two ester moieties contain alkylene moieties having a terminal halogen.
摘要翻译：公开了可用作表面活性剂的新型多羧基苯二酐。本发明的新化合物是均苯四酸四丁酯，其中两个酯部分特征地含有氟化烷基或饱和烃烷基，其中两个酯部分含有具有末端卤素的亚烷基部分。

6. 发明授权

US5151477A Copolymerization of vinyl acetate and a fluoromonomer in an aqueous medium 失效
标题翻译：乙酸乙烯酯和含氟单体在水性介质中的共聚合
公开(公告)号：US5151477A
公开(公告)日：1992-09-29
申请号：US796184
申请日：1991-11-22
申请人： Bryce C. Oxenrider , David J. Long , Frank Mares
发明人： Bryce C. Oxenrider , David J. Long , Frank Mares
IPC分类号： C08F2/00 , C08F8/12 , C08F214/18 , C08F218/04
CPC分类号： C08F214/186 , C08F218/04 , C08F8/12 , C08J5/18
摘要： A process of preparing a copolymer of vinyl monomer such as vinyl acetate, vinyl propionate and vinyl trifluoroacetate, and of fluorinated monomers such as tetrafluoroethylene and trifluoroethylene, said copolymer having an alternating or substantially alternating distribution of vinyl recurring monomeric units and fluorinated recurring monomeric units in the copolymer backbone which comprises copolymerizing said monomers in an aqueous reaction medium comprising water and a water miscible organic co-solvent in an amount less than the amount sufficient to form a distinct organic co-solvent phase.
摘要翻译：一种制备乙酸乙烯酯，丙酸乙烯酯和三氟乙酸乙烯酯的乙烯基单体和氟代单体如四氟乙烯和三氟乙烯的共聚物的方法，所述共聚物具有乙烯基重复单体单元和氟化重复单体单元的交替或基本上交替的分布，所述共聚物骨架包括使所述单体在包含水和水混溶性有机助溶剂的水性反应介质中的量低于足以形成不同有机共溶剂相的量。

7. 发明授权

US5137999A Copolymerization of vinyl acetate and a fluoromonomer in an aqueous medium 失效
标题翻译：乙酸乙烯酯和含氟单体在水性介质中的共聚合
公开(公告)号：US5137999A
公开(公告)日：1992-08-11
申请号：US695677
申请日：1991-05-06
申请人： Bryce C. Oxenrider , David J. Long , Frank Mares
发明人： Bryce C. Oxenrider , David J. Long , Frank Mares
IPC分类号： C08F2/00 , C08F8/12 , C08F214/18 , C08F218/04
CPC分类号： C08F214/186 , C08F218/04 , C08F8/12 , C08J5/18 , C08F2810/50
摘要： A process of preparing a copolymer of vinyl monomer selected from the group consisting of vinyl acetate, vinyl propionate and vinyl trifluoroacetate, and of fluorinated monomer selected from the group consisting of tetrafluoroethylene and trifluoroethylene, said copolymer having an alternating or substantially alternating distribution of vinyl recurring monomeric units and fluorinated recurring monomeric units in the copolymer backbone which comprises copolymerizing said monomers in an aqueous reaction medium comprising water and a water miscible organic co-solvent in an amount less than the amount sufficient to form a distinct organic co-solvent phase.
摘要翻译：一种制备乙烯基单体的共聚物的方法，所述乙烯基单体选自乙酸乙烯酯，丙酸乙烯酯和三氟乙酸乙烯酯，以及选自四氟乙烯和三氟乙烯的氟化单体，所述共聚物具有交替或基本交替的乙烯基重复分布共聚物主链中的单体单元和氟化的重复单体单元，其包括在包含水和水混溶性有机助溶剂的水性反应介质中将所述单体共聚，其量小于足以形成不同有机共溶剂相的量。

8. 发明授权

US4447629A Fluorinated and non-fluorinated siloxy pyromellitates 失效
标题翻译：氟化和非氟化甲硅烷氧基苯甲酸酯
公开(公告)号：US4447629A
公开(公告)日：1984-05-08
申请号：US429946
申请日：1982-09-30
申请人： Bryce C. Oxenrider , David J. Long
发明人： Bryce C. Oxenrider , David J. Long
IPC分类号： C07F7/18 , D06M13/192 , C07F7/08 , C07F7/10
CPC分类号： D06M13/192 , C07F7/1836 , Y10T428/2933
摘要： Pyromellitate tetraesters are disclosed that are useful as water repellents. The pyromellitates of this invention characteristically contain two ester moieties wherein said ester moieties contain a fluorinated or saturated hydrocarbon alkyl group. Additionally, pyromellitates of this invention contain two ester moieties which contain siloxyl groups.
摘要翻译：公开了作为防水剂有用的均苯四酸四
酯。本发明的均苯四酸酯特征在于含有两个酯部分，其中所述酯部分含有氟化或饱和烃烷基。此外，本发明的均苯四酸酯含有含有硅氧烷基的两个酯部分。

9. 发明授权

US5135998A Process for forming a fluorinated copolymer 失效
标题翻译：形成含氟共聚物的方法
公开(公告)号：US5135998A
公开(公告)日：1992-08-04
申请号：US726091
申请日：1991-07-05
申请人： Frank Mares , Bryce C. Oxenrider , David J. Long , John P. Sibilia
发明人： Frank Mares , Bryce C. Oxenrider , David J. Long , John P. Sibilia
IPC分类号： C08F2/00 , C08F8/12 , C08F214/18 , C08F218/04
CPC分类号： C08F214/186 , C08F218/04 , C08F8/12 , C08J5/18 , C08F2810/50
摘要： A process of preparing a copolymer of a vinyl monomer such as vinyl acetate, vinyl propionate and vinyl trifluoroacetate, and of fluorinated monomer such as tetrafluoroethylene and trifluoroethylene, said copolymer having an alternating or substantially alternating distributing of vinyl recurring monomeric units and fluorinated recurring monomeric units in the copolymers backbone which comprises copolymerizing said monomers in a reaction medium of a chlorocarbon, a fluorocarbon a chlorofluorocarbon or a mixture thereof.
摘要翻译：制备乙烯基单体如乙酸乙烯酯，丙酸乙烯酯和三氟乙酸乙烯酯的共聚物和氟化单体如四氟乙烯和三氟乙烯的共聚物的方法，所述共聚物具有乙烯基重复单体单元和氟化重复单体单元的交替或基本上交替的分布在共聚物主链中，其包括将所述单体在氯碳化合物，氟碳化合物，氯氟烃或其混合物的反应介质中共聚。

10. 发明授权

US5070162A Copolymerization of vinyl acetate and a fluoromonomer in an aqueous medium 失效
标题翻译：乙酸乙烯酯和含氟单体在水性介质中的共聚合
公开(公告)号：US5070162A
公开(公告)日：1991-12-03
申请号：US424441
申请日：1989-10-20
申请人： Bryce C. Oxenrider , David J. Long , Frank Mares
发明人： Bryce C. Oxenrider , David J. Long , Frank Mares
IPC分类号： C08F2/00 , C08F8/12 , C08F214/18 , C08F218/04
CPC分类号： C08F214/186 , C08F218/04 , C08F8/12 , C08F2810/50
摘要： A process of preparing a copolymer of vinyl monomer selected from the group consisting of vinyl acetate, vinyl propionate and vinyl trifluoroacetate, and of fluorinated monomer selected from the group consisting of tetrafluoroethylene and trifluoroethylene, said copolymer having an alternating or substantially alternating distribution of vinyl recurring monomeric units and fluorinated recurring monomeric units in the copolymer backbone which comprises copolymerizing said monomers in an aqueous reaction medium comprising water and a water miscible organic co-solvent in an amount less than the amount sufficient to form a distinct organic co-solvent phase.
摘要翻译：一种制备乙烯基单体的共聚物的方法，所述乙烯基单体选自乙酸乙烯酯，丙酸乙烯酯和三氟乙酸乙烯酯，以及选自四氟乙烯和三氟乙烯的氟化单体，所述共聚物具有交替或基本交替的乙烯基重复分布共聚物主链中的单体单元和氟化的重复单体单元，其包括在包含水和水混溶性有机助溶剂的水性反应介质中将所述单体共聚，其量小于足以形成不同有机共溶剂相的量。

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