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1. 发明授权

US06168868A Process for applying a lead-free coating to untreated metal substrates via electrodeposition 失效
标题翻译：通过电沉积将未经处理的金属基材施加无铅涂层的方法
公开(公告)号：US06168868A
公开(公告)日：2001-01-02
申请号：US09309850
申请日：1999-05-11
申请人： Brian T. Hauser , Richard F. Karabin , Thor G. Lingenfelter
发明人： Brian T. Hauser , Richard F. Karabin , Thor G. Lingenfelter
IPC分类号： C23C2800
CPC分类号： C23C22/34 , C25D13/20 , Y10T428/31678
摘要： An improved process for applying a lead-free coating by electrodeposition to an untreated ferrous metal substrate is provided. The substrate need not be phosphated prior to treatment. The process includes the following steps: a) contacting the substrate surface with a group IIIB or IVB metal compound in a medium that is essentially free of accelerators needed to form phosphate conversion coatings; followed by b) electrocoating the substrate with a substantially lead-free, curable electrodepositable composition; and c) curing the electrodepositable composition. The group IIIB or IVB metal compound is preferably a zirconium compound and is typically in an aqueous medium. The process may further include initial steps of cleaning the substrate with an alkaline cleaner and rinsing with an acidic rinse. Substrates treated by the process of the present invention demonstrate excellent corrosion resistance.
摘要翻译：提供了一种通过电沉积施加到未处理的黑色金属基底上的无铅涂层的改进方法。在处理之前，基板不需要磷化。该方法包括以下步骤：a）在基本上不含形成磷酸盐转化涂层所需的促进剂的介质中使基材表面与IIIB或IVB族金属化合物接触; 随后b）用基本上无铅的可固化的可电沉积组合物电镀基材; 并且c）固化可电沉积组合物。组IIIB或IVB金属化合物优选是锆化合物，并且通常在水性介质中。该方法还可以包括用碱性清洁剂清洁基底并用酸性漂洗物冲洗的初始步骤。通过本发明的方法处理显示出优异的耐腐蚀性。

2. 发明申请

US20100187117A1 ELECTRODEPOSITABLE COATING COMPOSITION COMPRISING SILANE AND YTTRIUM 有权
标题翻译：包含硅烷和铝的电沉积涂料组合物
公开(公告)号：US20100187117A1
公开(公告)日：2010-07-29
申请号：US12693626
申请日：2010-01-26
申请人： Thor G. Lingenfelter , Amanda Foley , Edward F. Rakiewicz , Richard F. Karabin
发明人： Thor G. Lingenfelter , Amanda Foley , Edward F. Rakiewicz , Richard F. Karabin
IPC分类号： B32B15/08 , C25D9/02 , B32B15/09 , B32B15/092 , B32B15/095
CPC分类号： C09D5/448 , C08K3/105
摘要： An electrodepositable coating composition comprising (i) a film-forming polymer, (ii) a corrosion inhibitor, and (iii) a silane that does not contain an ethylenically unsaturated double bond.
摘要翻译：一种电沉积涂料组合物，其包含（i）成膜聚合物，（ii）缓蚀剂，和（iii）不含烯属不饱和双键的硅烷。

3. 发明授权

US08486538B2 Electrodepositable coating composition comprising silane and yttrium 有权
标题翻译：包含硅烷和钇的电沉积涂料组合物
公开(公告)号：US08486538B2
公开(公告)日：2013-07-16
申请号：US12693626
申请日：2010-01-26
申请人： Thor G. Lingenfelter , Amanda Foley , Edward G. Rakiewicz , Richard F. Karabin , William J. Vanooij
发明人： Thor G. Lingenfelter , Amanda Foley , Edward G. Rakiewicz , Richard F. Karabin , William J. Vanooij
IPC分类号： B32B15/08 , B32B27/18 , B32B33/00 , C09D5/08 , B32B15/092 , C25D9/02 , C25D9/04
CPC分类号： C09D5/448 , C08K3/105
摘要： An electrodepositable coating composition comprising (i) a film-forming polymer, (ii) a corrosion inhibitor, and (iii) a silane that does not contain an ethylenically unsaturated double bond.
摘要翻译：一种电沉积涂料组合物，其包含（i）成膜聚合物，（ii）缓蚀剂，和（iii）不含烯属不饱和双键的硅烷。

4. 发明授权

US08288504B2 Method of making a cyclic guanidine from dicyandiamide and coating compositions containing same 有权
标题翻译：从双氰胺制备环状胍的方法和含有它们的涂料组合物
公开(公告)号：US08288504B2
公开(公告)日：2012-10-16
申请号：US12720971
申请日：2010-03-10
申请人： Steven R. Zawacky , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Thomas C. Moriarity
发明人： Steven R. Zawacky , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Thomas C. Moriarity
IPC分类号： C08G69/00
CPC分类号： C07D471/04 , C07D487/04 , C08G59/4021 , C08G59/50 , C09D5/4461 , C09D5/4488
摘要： The present invention is directed to a method for preparing a cyclic guanidine comprising reacting (i) a cyanamide, (ii) a polyamine, and (iii) a weak acid. The present invention is also directed to a coating composition comprising the cyclic guanidine.
摘要翻译：本发明涉及一种制备环状胍的方法，包括使（ⅰ）氰胺，（ⅱ）多胺和（ⅲ）弱酸反应。本发明还涉及包含环状胍的涂料组合物。

5. 发明授权

US5074979A Cationic resin containing blocked isocyanate groups suitable for use in electrodeposition 失效
标题翻译：含阴离子异氰酸酯基团的阳离子树脂适用于电沉积
公开(公告)号：US5074979A
公开(公告)日：1991-12-24
申请号：US540991
申请日：1990-06-20
申请人： Joseph T. Valko , Richard F. Karabin
发明人： Joseph T. Valko , Richard F. Karabin
IPC分类号： C08G18/58 , C08G18/80 , C08G59/14 , C09D5/44 , C09D163/00 , C09D175/00 , C09D175/04
CPC分类号： C08G18/581 , C08G18/8048 , C08G18/8054 , C08G18/8064 , C09D5/4434
摘要： A cationic resin containing blocked isocyanate groups which is suitable for use in electrodeposition is disclosed. The cationic resin is derived from an epoxy resin and contains in the resin molecule cationic salt groups, active hydrogen groups and blocked isocyanate groups. The blocked isocyanate groups are incorporated into the resin molecule by reacting the epoxy resin with a compound selected from the class consisting of mercapto compounds and acid group-containing compounds where the compounds also contain blocked isocyanate groups. The resin can be formulated into an electrocoating composition which is free of lead and yet provides outstanding corrosion resistance when electrodeposited over steel substrates. The outstanding corrosion resistance can be attained when the substrate has not been given a chrome rinse which is conventional in pretreating the steel substrate before electrodeposition.

6. 发明授权

US08795836B2 Electrodepositable coating composition comprising a bismuth salt and a stabilizing compound 有权
标题翻译：包含铋盐和稳定化合物的电沉积涂料组合物
公开(公告)号：US08795836B2
公开(公告)日：2014-08-05
申请号：US12716305
申请日：2010-03-03
申请人： Alan J. Kaylo , Kevin J. Dufford , Steven D. Perrine , Michael J. Pawlik , Richard F. Karabin
发明人： Alan J. Kaylo , Kevin J. Dufford , Steven D. Perrine , Michael J. Pawlik , Richard F. Karabin
IPC分类号： B32B27/00 , C25D9/00 , C09D5/00 , B32B27/38 , C09D163/00
CPC分类号： C09D5/44 , Y10T428/31504
摘要： The present invention is directed to an electrodepositable coating composition comprising a bismuth salt and a stabilizing agent, and wherein the molar ratio of elemental bismuth to the stabilizing agent is not less than 1:0.25.
摘要翻译：本发明涉及包含铋盐和稳定剂的电沉积涂料组合物，其中元素铋与稳定剂的摩尔比不小于1:0.25。

7. 发明申请

US20120220770A1 PREPARATION OF BICYCLIC GUANIDINE SALTS IN AN AQUEOUS MEDIA 有权
标题翻译：水性介质中双糖类营养盐的制备
公开(公告)号：US20120220770A1
公开(公告)日：2012-08-30
申请号：US13035048
申请日：2011-02-25
申请人： Charles Robert Hickenboth , Richard F. Karabin , Christopher A. Dacko , Steven Randolph Zawacky , Thomas Charles Moriartiy , Gregory J. McCollum
发明人： Charles Robert Hickenboth , Richard F. Karabin , Christopher A. Dacko , Steven Randolph Zawacky , Thomas Charles Moriartiy , Gregory J. McCollum
IPC分类号： C07D487/04
CPC分类号： C07D487/04
摘要： Disclosed herein are bicyclic guanidine salts formed as the reaction product of reactants comprising (a) a compound having the general formula CXn, wherein X is N, O, or S and wherein n is 2 to 4; (b) an acid; (c) dipropylene triamine; and (d) water, and an associated method for forming a bicyclic guanidine salt from the same reaction ingredients.
摘要翻译：本文公开了作为反应物的反应产物形成的双环胍盐，其包含（a）具有通式CXn的化合物，其中X为N，O或S，且其中n为2至4; （b）酸; （c）二丙烯三胺; 和（d）水，以及由相同的反应成分形成双环胍盐的相关方法。

8. 发明授权

US07776959B2 Coatings comprising terpene 失效
标题翻译：包含萜烯的涂料
公开(公告)号：US07776959B2
公开(公告)日：2010-08-17
申请号：US11564570
申请日：2006-11-29
申请人： Simion Coca , James O'Dwyer , Richard F. Karabin , Stephen J. Thomas , Victoria A. Trettel , Davina Schwartzmiller , Jane N. Valenta , Gregory J. McCollum , Richard J. Sadvary
发明人： Simion Coca , James O'Dwyer , Richard F. Karabin , Stephen J. Thomas , Victoria A. Trettel , Davina Schwartzmiller , Jane N. Valenta , Gregory J. McCollum , Richard J. Sadvary
IPC分类号： C08L33/04 , C08L99/00 , C08G65/34
CPC分类号： C09D4/00 , C08F289/00 , C08F291/00 , C09D151/003 , C09D151/08 , C08L2666/02
摘要： Coatings comprising a polymer comprising a terpene and a monomer polymerized with terpene by free radical polymerization are disclosed. Coatings comprising terpene in greater than 30 wt % are also disclosed as are coatings comprising a terpene and a urea. Copolymers with terpene are also disclosed.
摘要翻译：公开了包含由萜烯和通过自由基聚合与萜烯聚合的单体的聚合物的涂料。包含大于30wt％的萜烯的涂层也被公开为包含萜烯和脲的涂层。还公开了与萜烯的共聚物。

9. 发明申请

US20100047583A1 AUTOMOTIVE SUBSTRATE HAVING A COATING LAYER SYSTEM WITH A BARRIER COATING COMPOSITION LAYER 审中-公开
标题翻译：具有涂层组合物层的涂层系统的汽车底板
公开(公告)号：US20100047583A1
公开(公告)日：2010-02-25
申请号：US12194991
申请日：2008-08-20
申请人： Michelle S. MILES , Edward F. Rakiewicz , Ken W. Niederst , Richard F. Karabin
发明人： Michelle S. MILES , Edward F. Rakiewicz , Ken W. Niederst , Richard F. Karabin
IPC分类号： B32B27/38 , C25D5/48
CPC分类号： C25D5/48 , B05D7/57 , C08G59/3218 , C08G59/50 , C08G65/24 , C08G65/2627 , C09D5/4488 , C09D163/00 , Y10T428/31511
摘要： An automotive substrate comprising an electrodepositable coating layer deposited over at least a portion of the automotive substrate and a barrier coating layer deposited over at least a portion of the electrodepositable coating layer.
摘要翻译：汽车衬底包括沉积在汽车衬底的至少一部分上的可电沉积涂层和沉积在可电沉积涂层的至少一部分上的阻挡涂层。

10. 发明申请

US20090281314A1 METHOD FOR PRODUCING BICYCLIC GUANIDINES BY USE OF A CYCLIC UREA AND A DEHYDRATING AGENT 失效
标题翻译：通过使用环状尿素和脱水剂生产双环类药物的方法
公开(公告)号：US20090281314A1
公开(公告)日：2009-11-12
申请号：US12195751
申请日：2008-08-21
申请人： Donald W. BOYD , Venkatachalam Eswarakrishnan , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Britt A. Minch , Thomas C. Moriarity , Steven R. Zawacky
发明人： Donald W. BOYD , Venkatachalam Eswarakrishnan , Charles R. Hickenboth , Richard F. Karabin , Gregory J. McCollum , Britt A. Minch , Thomas C. Moriarity , Steven R. Zawacky
IPC分类号： C07D487/04
CPC分类号： C07D487/04
摘要： The present invention is directed to a method for producing bicyclic guanidines comprising heating a reaction mixture comprising cyclic urea and a dehydrating agent to a temperature ≧90° C.
摘要翻译：本发明涉及一种制备双环胍的方法，包括将包含环脲和脱水剂的反应混合物加热至> 90℃的温度。

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