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1. 发明申请

US20120121911A1 POLYHYDROXY KETAL ESTER ADDUCTS, METHODS OF MANUFACTURE AND USES THEREOF 有权
标题翻译：聚羟基硬脂酸酯添加剂，其制备方法及其用途
公开(公告)号：US20120121911A1
公开(公告)日：2012-05-17
申请号：US13294854
申请日：2011-11-11
申请人： Brian D. Mullen , Marc D. Scholten , Dorie J. Yontz , Cora M. Leibig , Matthew J. Tjosaas
发明人： Brian D. Mullen , Marc D. Scholten , Dorie J. Yontz , Cora M. Leibig , Matthew J. Tjosaas
IPC分类号： B32B27/36 , C07D317/30 , C08J9/35 , C08K5/156 , C08G63/16 , C08G14/02 , C08G18/32 , C09K3/00 , C09D163/00 , C09D175/06 , C08G64/00 , B05D7/24 , B05D3/00 , B32B27/28 , C07D407/12
CPC分类号： C08K5/1565 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G18/3218 , C08G63/668 , C08G63/672 , C08G63/91 , C08G64/0208 , C08G64/42 , C08G2101/0025 , C08L59/00 , C08L67/00 , C09D159/00 , C09D167/00 , Y02P20/582 , Y10T428/31507 , Y10T428/31786
摘要： Disclosed herein is a polyhydroxy ketal adduct obtained by the esterification of a hydrocarbon polyol by at least 1.5 equivalents of a ketocarboxy to produce an intermediate ketocarboxylic ester. The intermediate polyketocarboxylic ester is then ketalized to produce the polyhydroxyketal adduct, which can be used to provide a polymeric composition.
摘要翻译：本文公开了通过烃多元醇通过至少1.5当量的酮羧基酯化以产生中间体酮羧酸酯而获得的多羟基缩酮加合物。然后中间体多酮羧酸酯被缩醛化以产生可用于提供聚合物组合物的多羟基缩酮加合物。

2. 发明授权

US09187598B2 Polyhydroxy ketal ester adducts, methods of manufacture and uses thereof 有权
标题翻译：多羟基缩酮酯加合物，其制备方法和用途
公开(公告)号：US09187598B2
公开(公告)日：2015-11-17
申请号：US13294854
申请日：2011-11-11
申请人： Brian D. Mullen , Marc D. Scholten , Dorie J. Yontz , Cora M. Leibig , Matthew J. Tjosaas
发明人： Brian D. Mullen , Marc D. Scholten , Dorie J. Yontz , Cora M. Leibig , Matthew J. Tjosaas
IPC分类号： C08G63/91 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G63/668 , C08G64/02 , C08G64/42 , C08L59/00 , C09D159/00 , C09D167/00 , C08G18/32 , C08L67/00 , C08G101/00
CPC分类号： C08K5/1565 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G18/3218 , C08G63/668 , C08G63/672 , C08G63/91 , C08G64/0208 , C08G64/42 , C08G2101/0025 , C08L59/00 , C08L67/00 , C09D159/00 , C09D167/00 , Y02P20/582 , Y10T428/31507 , Y10T428/31786
摘要： Disclosed herein is a polyhydroxy ketal adduct obtained by the esterification of a hydrocarbon polyol by at least 1.5 equivalents of a ketocarboxy to produce an intermediate ketocarboxylic ester. The intermediate polyketocarboxylic ester is then ketalized to produce the polyhydroxyketal adduct, which can be used to provide a polymeric composition.
摘要翻译：本文公开了通过烃多元醇通过至少1.5当量的酮羧基酯化以产生中间体酮羧酸酯而获得的多羟基缩酮加合物。然后中间体多酮羧酸酯被缩醛化以产生可用于提供聚合物组合物的多羟基缩酮加合物。

3. 发明授权

US09212176B2 Polyketal adducts, methods of manufacture and uses thereof 有权
标题翻译：聚缩酮加成物，其制造方法和用途
公开(公告)号：US09212176B2
公开(公告)日：2015-12-15
申请号：US13294690
申请日：2011-11-11
申请人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana , Matthew J. Tjosaas
发明人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana , Matthew J. Tjosaas
IPC分类号： C07D407/12 , C08K5/1565 , C08L79/08 , C08L77/00 , C08L59/02
CPC分类号： C07D407/12 , C08K5/1565 , C08L59/02 , C08L77/00 , C08L79/08 , Y02P20/582 , C08L27/06
摘要： Disclosed herein is a polyketal adduct obtained by forming an ester between a hydrocarbon polyol and a ketocarboxylic acid to produce an intermediate polyketocarboxylic ester. The intermediate polyketocarboxylic ester can be purified via crystallization to achieve purities of greater than 99.0% and then ketalized to produce the polyketal adduct, which can be used in polymer compositions. The polyketal adduct I is obtained at high purity and at high yield.
摘要翻译：本文公开了通过在烃多元醇和酮羧酸之间形成酯以产生中间体多酮羧酸酯而获得的聚缩酮加成物。可以通过结晶纯化中间体多酮羧酸酯以实现大于99.0％的纯度，然后缩醛化以产生可用于聚合物组合物中的聚缩酮加合物。以高纯度和高收率获得聚缩酮加成物I.

4. 发明授权

US08846817B2 Ionic polymers, method of manufacture, and uses thereof 有权
标题翻译：离子聚合物，制造方法及其用途
公开(公告)号：US08846817B2
公开(公告)日：2014-09-30
申请号：US13294926
申请日：2011-11-11
申请人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
发明人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
IPC分类号： C08F8/12 , C08F218/10 , B01J20/26 , C08F224/00 , B01J20/30 , C08F220/16 , B01J20/28 , C08F226/10 , C08F220/06
CPC分类号： B01J20/3042 , B01J20/264 , B01J20/267 , B01J20/2803 , B01J2220/46 , B01J2220/68 , C08F8/44 , C08F220/06 , C08F220/16 , C08F224/00 , C08F226/10 , C08F2800/10
摘要： An ionic polymer of formula VI wherein each b=0 or 1; X is hydrogen, 1/z of a metal ion of charge z, a protonated nitrogen base, or a tetrasubstituted organic ammonium compound; the molar ratio of q:r:s:t=(100-0.1):(0-99.9):(0-50):(0-30); R1, R2 and R3 are hydrogen or C1-4 alkyl; R4, R5, R6 and R7 are hydrogen, C1-4 alkyl or F, wherein F is a functional group that imparts a property to polymer VI, at least one and no more than two of R4, R5, R6 and R7 are F and F is the same or different; G is a single bond or a C1-30 hydrocarbyl group; and for each instance of t when t is not zero, c=0-5 and d=0-5, provided that c+d=1-5, and wherein q, r and s as present in c are independent of any other value of q, r and s.
摘要翻译：式VI的离子聚合物，其中每个b = 0或1; X是氢，电荷z的金属离子的1 / z，质子化的氮碱或四取代的有机铵化合物; q：r：s：t =（100-0.1）：（0-99.9）：（0-50）：（0-30）的摩尔比; R1，R2和R3是氢或C1-4烷基; R4，R5，R6和R7是氢，C1-4烷基或F，其中F是赋予聚合物VI性质的官能团，R 4，R 5，R 6和R 7中的至少一个不超过两个是F， F相同或不同; G是单键或C1-30烃基; 并且对于t的每个实例，当t不为零时，c = 0-5和d = 0-5，条件是c + d = 1-5，并且其中存在于c中的q，r和s独立于任何其它 q，r和s的值。

5. 发明申请

US20120118832A1 IONIC POLYMERS, METHOD OF MANUFACTURE, AND USES THEREOF 有权
标题翻译：离子聚合物，制造方法及其用途
公开(公告)号：US20120118832A1
公开(公告)日：2012-05-17
申请号：US13294926
申请日：2011-11-11
申请人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
发明人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
IPC分类号： B01D21/01 , B01J20/26 , C09K3/00 , C08F218/10 , C08F8/44
CPC分类号： B01J20/3042 , B01J20/264 , B01J20/267 , B01J20/2803 , B01J2220/46 , B01J2220/68 , C08F8/44 , C08F220/06 , C08F220/16 , C08F224/00 , C08F226/10 , C08F2800/10
摘要： An ionic polymer of formula VI wherein each b=0 or 1; X is hydrogen, 1/z of a metal ion of charge z, a protonated nitrogen base, or a tetrasubstituted organic ammonium compound; the molar ratio of q:r:s:t=(100-0.1):(0-99.9):(0-50):(0-30); R1, R2 and R3 are hydrogen or C1-4 alkyl; R4, R5, R6 and R7 are hydrogen, C1-4 alkyl or F, wherein F is a functional group that imparts a property to polymer VI, at least one and no more than two of R4, R5, R6 and R7 are F and F is the same or different; G is a single bond or a C1-30 hydrocarbyl group; and for each instance of t when t is not zero, c=0-5 and d=0-5, provided that c+d=1-5, and wherein q, r and s as present in c are independent of any other value of q, r and s.
摘要翻译：式VI的离子聚合物，其中每个b = 0或1; X是氢，电荷z的金属离子的1 / z，质子化的氮碱或四取代的有机铵化合物; q：r：s：t =（100-0.1）：（0-99.9）：（0-50）：（0-30）的摩尔比; R1，R2和R3是氢或C1-4烷基; R4，R5，R6和R7是氢，C1-4烷基或F，其中F是赋予聚合物VI性质的官能团，R 4，R 5，R 6和R 7中的至少一个不超过两个是F， F相同或不同; G是单键或C1-30烃基; 并且对于t的每个实例，当t不为零时，c = 0-5和d = 0-5，条件是c + d = 1-5，并且其中存在于c中的q，r和s独立于任何其它 q，r和s的值。

6. 发明申请

US20120118201A1 POLYKETAL ADDUCTS, METHODS OF MANUFACTURE AND USES THEREOF 有权
标题翻译：聚酮制剂，制造方法及其用途
公开(公告)号：US20120118201A1
公开(公告)日：2012-05-17
申请号：US13294690
申请日：2011-11-11
申请人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana
发明人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana
IPC分类号： C08K5/1565 , C08L67/04 , C08L27/06 , C08L23/00 , C08L69/00 , C08L79/08 , C08L25/06 , C08L77/00 , C08L1/02 , C08L81/04 , C08L81/06 , C07D407/12 , C08L83/04
CPC分类号： C07D407/12 , C08K5/1565 , C08L59/02 , C08L77/00 , C08L79/08 , Y02P20/582 , C08L27/06
摘要： Disclosed herein is a polyketal adduct obtained by forming an ester between a hydrocarbon polyol and a ketocarboxylic acid to produce an intermediate polyketocarboxylic ester. The intermediate polyketocarboxylic ester can be purified via crystallization to achieve purities of greater than 99.0% and then ketalized to produce the polyketal adduct, which can be used in polymer compositions. The polyketal adduct I is obtained at high purity and at high yield.
摘要翻译：本文公开了通过在烃多元醇和酮羧酸之间形成酯以产生中间体多酮羧酸酯而获得的聚缩酮加成物。可以通过结晶纯化中间体多酮羧酸酯以实现大于99.0％的纯度，然后缩醛化以产生可用于聚合物组合物中的聚缩酮加合物。以高纯度和高收率获得聚缩酮加成物I.

7. 发明授权

US10316009B2 Process to prepare hydroxymethylfurfural derivatives 有权
公开(公告)号：US10316009B2
公开(公告)日：2019-06-11
申请号：US15754060
申请日：2016-08-19
申请人： GFBIOCHEMICALS LIMITED , Brian D. Mullen , Cora M. Leibig , Roger Schoonover , Kevin Jon Bechtold
发明人： Brian D. Mullen , Cora M. Leibig , Roger Schoonover , Arie De Rijke , Kevin Jon Bechtold
IPC分类号： C07D307/50 , C07D307/48 , C07D307/54 , C07C59/185
摘要： The invention relates generally to the preparation of hydroxymethyl furfural derivatives such as 5-carboxymethyl furfural derivatives, ethers such as 5-alkoxymethyl furfural derivatives, 5-hydroxymethyl furfural, levulinic acid, levulinic acid esters, and/or formic acid, formic acid esters from sugar.

8. 发明授权

US08507718B2 Ketocarboxylic acids, methods of manufacture and uses thereof 有权
标题翻译：酮羧酸，其制备方法和用途
公开(公告)号：US08507718B2
公开(公告)日：2013-08-13
申请号：US13294751
申请日：2011-11-11
申请人： Brian D. Mullen , Cora M. Leibig , Leo E. Manzer
发明人： Brian D. Mullen , Cora M. Leibig , Leo E. Manzer
IPC分类号： C07C69/716 , C07C51/36
CPC分类号： C07C69/738 , C07C51/09 , C07C51/493 , C07C67/08 , C07C67/52 , C07C69/716 , Y02P20/582 , C07C59/185
摘要： Ketocarboxylic acids such as levulinic acid can be efficiently purified in high yield by esterification with a hydrocarbon polyol to the corresponding polyketocarboxylic ester, which can be readily purified, for example recrystallized. After purification, the ketocarboxylic ester can be hydrolyzed to provide pure ketocarboxylic acid, or a salt thereof, after removal of the esterifying hydrocarbon polyol, or used for other synthetic transformations. Advantageously, the polyketocarboxylic esters, ketocarboxylic acids, and salts thereof produced by this method are obtained in high purity.
摘要翻译：酮羧酸如乙酰丙酸可以通过用烃多元醇与相应的聚酮羧酸酯酯化而以高收率有效地纯化，其可以容易地纯化，例如重结晶。纯化后，在除去酯化烃多元醇之后，可以将酮羧酸酯水解以提供纯酮羧酸或其盐，或用于其它合成转化。有利地，以高纯度获得通过该方法制备的多酮羧酸酯，酮羧酸及其盐。

9. 发明申请

US20120035376A1 METHODS FOR THE MANUFACTURE OF ACETALS AND KETALS, AND THE ACETALS AND KETALS PRODUCED THEREBY 审中-公开
标题翻译：乙酸和乙酸乙酯的制备方法，以及生产的乙醇和乙醇
公开(公告)号：US20120035376A1
公开(公告)日：2012-02-09
申请号：US13197593
申请日：2011-08-03
申请人： Brian D. Mullen , Marc D. Scholten , Andrew J. Louwagie , Steven A. Donen , Feng Jing , Vivek Badarinarayana
发明人： Brian D. Mullen , Marc D. Scholten , Andrew J. Louwagie , Steven A. Donen , Feng Jing , Vivek Badarinarayana
IPC分类号： C07D317/30
CPC分类号： C07D317/30 , Y02P20/582
摘要： A method for producing a product that comprises glycerol ketal of ethyl levulinate or propylene glycol ketal of ethyl levulinate comprises reacting either glycerol or propylene glycol with ethyl levulinate in the presence of a homogenous or heterogeneous catalyst system in a reactor system. The ethyl levulinate and either glycerol or propylene glycol are heated to remove water, polyol, and excess ethyl levulinate. The excess ethyl levulinate and polyol is recycled back to the reactor. The product is distilled in a specific fashion and optionally treated by means of a stabilizing agent or acid species removal bed, to obtain a composition comprising glycerol ketal of ethyl levulinate or propylene glycol ketal of ethyl levulinate wherein the composition comprises less than or equal to about 2 wt % contaminants.
摘要翻译：用于生产包含乙酰乙酸乙酯乙酰丙酸乙酯或丙二醇缩酮的甘油缩酮的产物的方法包括在反应器系统中在均相或非均相催化剂体系存在下使甘油或丙二醇与乙酰乙酸乙酯反应。将乙酰乙酸乙酯和甘油或丙二醇加热以除去水，多元醇和过量乙酰乙酸乙酯。过量的乙酰丙酸乙酯和多元醇再循环回到反应器中。产物以特定方式蒸馏并任选地通过稳定剂或酸物质去除床处理，以获得组合物，其包含乙酰丙酸乙酯的乙酰丙酸乙酯或丙二醇缩酮的甘油缩酮，其中组合物包含小于或等于约 2重量％的污染物。

10. 发明授权

US09271034B2 Adding content during data stream acquisition 有权
标题翻译：在数据流采集期间添加内容
公开(公告)号：US09271034B2
公开(公告)日：2016-02-23
申请号：US12640818
申请日：2009-12-17
申请人： Yeqing Wang , Brian D. Mullen
发明人： Yeqing Wang , Brian D. Mullen
IPC分类号： H04N7/10 , H04N21/438 , H04N21/44 , H04N21/81 , H04N21/433
CPC分类号： H04N21/8126 , H04N21/4331 , H04N21/4384 , H04N21/44016 , H04N21/812
摘要： A device is provided for use with extended content data on a first data stream and second content data on a second data stream. The device includes a processing portion, an acquisition portion and a buffer. The acquisition portion is in communication with the processing portion. The acquisition portion can acquire the first data stream, can transition to the second data stream to receive the second content data and can provide the second content data to the processing portion. The buffer can receive the extended content data. The processing portion can instruct the acquisition portion to transition from the first data stream to the second data stream to receive the second content data. The buffer can further provide the extended content data to the processing portion based on the acquisition portion transitioning from the first data stream to the second data stream. The processing portion can further process the extended content data portion as received from the buffer.
摘要翻译：提供了一种用于第一数据流上的扩展内容数据和第二数据流上的第二内容数据的设备。该设备包括处理部分，获取部分和缓冲器。采集部与处理部进行通信。获取部分可以获取第一数据流，可以转换到第二数据流以接收第二内容数据，并且可以向处理部分提供第二内容数据。缓冲区可以接收扩展内容数据。处理部分可以指示采集部分从第一数据流转换到第二数据流以接收第二内容数据。缓冲器可以基于从第一数据流到第二数据流的获取部分转换，进一步向处理部分提供扩展内容数据。处理部分可以进一步处理从缓冲器接收到的扩展内容数据部分。

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