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    • 10. 发明申请
    • Zr/ZrO2 Electrode and Producing Method Thereof and Integrated High Temperature and High-Pressure Chemical Sensor Composed by the Same
    • Zr / ZrO2电极及其制造方法及由其组成的高温高压化学传感器
    • US20090050476A1
    • 2009-02-26
    • US11886663
    • 2006-03-21
    • Ronghua ZhangShumin HuXuetong Zhang
    • Ronghua ZhangShumin HuXuetong Zhang
    • G01N27/30G01N27/27G01N27/407
    • G01N27/30Y10T29/49117
    • The invention involves a Zr/ZrO2 electrode that consists of a piece of Zr wire and a ZrO2 film formed over the surface of the part of the Zr wire for the use of measuring end in the probe section. An insulating layer and a sealing structure are put in place on the non-probe section and the non-conducting wire connection section of said electrode, while the Zr wire at the other end is applied for circuit connection. The invention also provides a type of integrated high-temperature/high-pressure chemical sensors, which includes one Zr/ZrO2 electrode and also 2 to 5 electrodes that can combine with the Zr/ZrO2 electrode to measure pH value, H2 value, H2S value and Eh value in high-temperature/high-pressure conditions, together constructing the integrated chemical sensors capable of measuring at least two kinds of parameters. The electrode and the integrated high-temperature/high-pressure chemical sensors work properly at the temperature range between 0 and 400 under the pressure up to 60 MPa and accurately measure various electrochemical parameters of liquid, displaying working stability and long lifespan. The electrode and chemical sensors can be fitted in high pressure reactors in laboratory for measuring and marking, as well as on detectors for measuring in actual high-temperature/high-pressure environments. The invention also presents the fabrication and construct process of the Zr/ZrO2 electrode.
    • 本发明涉及一种Zr / ZrO 2电极,其由在一部分Zr线上形成的Zr线和ZrO2膜组成,用于在探针部分中使用测量端。 绝缘层和密封结构放置在所述电极的非探针部分和非导线连接部分上,而另一端的Zr线被施加于电路连接。 本发明还提供了一种集成的高温高压化学传感器,其包括一个Zr / ZrO 2电极和还可以与Zr / ZrO 2电极结合的2至5个电极,以测量pH值,H 2值,H 2 S值 和高温/高压条件下的Eh值,共同构建能够测量至少两种参数的综合化学传感器。 电极和集成高温/高压化学传感器在0至400℃的温度范围内,在高达60 MPa的压力下正常工作,可精确测量液体的各种电化学参数,显示工作稳定性和使用寿命长。 电极和化学传感器可以安装在实验室用于测量和标记的高压反应器中,以及用于在实际高温/高压环境中测量的检测器。 本发明还提出了Zr / ZrO2电极的制造和构造过程。