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1. 发明授权

US07094368B2 Pyrano-quinolines, pyrano-quinolinones, combinations thereof, photochromic compositions and articles 失效
标题翻译：吡喹啉，吡喃 - 喹啉酮，其组合，光致变色组合物和制品
公开(公告)号：US07094368B2
公开(公告)日：2006-08-22
申请号：US10732008
申请日：2003-12-10
申请人： Beon-Kyu Kim , Anil Kumar , Barry Van Gemert
发明人： Beon-Kyu Kim , Anil Kumar , Barry Van Gemert
IPC分类号： G02B5/23 , C08K5/1545 , G02C7/10
CPC分类号： C07D491/04
摘要： Described are compositions of at least one material represented by a pyrano[3,2-c]quinoline structure, a pyrano[3,2-c]quinolinone structure or mixtures thereof. The pyrano[3,2-c]quinoline structure is characterized by having a nitrogen atom at the 6-position ring atom and an oxy-substituent at the 5-position ring atom. The pyrano[3,2-c]quinolinone structure is characterized by having a substituted nitrogen atom at the 6-position ring atom and an oxo-substituent at the 5-position ring atom, the nitrogen atom substituents being hydrogen, aliphatic substituents, cycloaliphatic substituents, aromatic substituents, heteroaromatic substituents or a combination thereof. Both of the pyrano[3,2-c]quinoline and pyrano[3,2-c]quinolinone structures are characterized by having two substituents at the 2-position ring atom. Also described are photochromic articles that contain or that have coatings or films containing at least one of the novel compositions or combinations thereof with other photochromic materials.
摘要翻译：描述了由吡喃并[3,2-c]喹啉结构，吡喃并[3,2-c]喹啉酮结构或其混合物表示的至少一种材料的组合物。吡喃并[3,2-c]喹啉结构的特征在于在6-位环原子上具有氮原子和在5位环原子上具有氧取代基。吡喃并[3,2-c]喹啉酮结构的特征在于在6位环原子上具有取代的氮原子，在5位环原子上具有氧代取代基，氮原子取代基为氢，脂族取代基，脂环族取代基，芳族取代基，杂芳族取代基或其组合。吡喃并[3,2-c]喹啉和吡喃并[3,2-c]喹啉酮结构的特征在于在2-位环原子上具有两个取代基。还描述了含有或具有包含至少一种新组合物或其组合与其它光致变色材料的涂层或膜的光致变色制品。

2. 发明申请

US20120145973A1 Photochromic Materials That Include Indeno-Fused Naphthopyrans 有权
标题翻译：包含茚诺芬萘醌的光致变色材料
公开(公告)号：US20120145973A1
公开(公告)日：2012-06-14
申请号：US13314297
申请日：2011-12-08
申请人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
发明人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
IPC分类号： G02B5/23 , C07D413/10 , C07D405/10 , C07D311/78
CPC分类号： C07D405/04 , C07D311/78 , C07D311/94 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic materials that include one or more indeno-fused naphthopyrans that have particular groups at the 7, 11, and 13 positions thereof, and at the position alpha to the oxygen of the pyran ring thereof. With some embodiments, hydrogen or an alkoxy group is bonded to the 7 position, an optionally substituted phenyl is bonded to the 11 position, two alkyl groups are bonded to the 13 position, and two optionally substituted phenyl groups are bonded to the position alpha to the oxygen of the pyran ring of the indeno-fused naphthopyran compound. The 13 position of the indeno-fused naphthopyrans is free of ether groups in which an ether oxygen is bonded to the 13 position, and hydroxyl. The present invention also relates to photochromic articles and compositions that include such indeno-fused naphthopyrans.
摘要翻译：本发明涉及光致变色材料，其包括一种或多种茚并稠合的萘并吡喃，其在其7,11和13位具有特定基团，并且在其吡喃环的氧的位置。在一些实施方案中，氢或烷氧基键合至7位，任选取代的苯基键合至11位，两个烷基键合至13位，并且两个任选取代的苯基键合至位置α 茚并稠合萘并吡喃化合物的吡喃环的氧。茚并稠合萘并吡喃的13位没有醚基，其中醚氧与13位结合，羟基。本发明还涉及包含这种茚并稠合萘并吡喃的光致变色制品和组合物。

3. 发明授权

US07556751B2 Photochromic materials having electron-withdrawing substituents 有权
标题翻译：具有吸电子取代基的光致变色材料
公开(公告)号：US07556751B2
公开(公告)日：2009-07-07
申请号：US11314141
申请日：2005-12-21
申请人： Anu Chopra , Beon-Kyu Kim , Barry Van Gemert
发明人： Anu Chopra , Beon-Kyu Kim , Barry Van Gemert
IPC分类号： G02B5/23
CPC分类号： G03C1/73 , C07D311/94 , C07D409/04 , C09K9/02 , C09K2211/1011 , C09K2211/1088
摘要： Photochromic materials comprising indeno-fused naphthopyrans having a first electron-withdrawing substituent and, in certain non-limiting embodiments, a second electron-withdrawing substituent are disclosed. The photochromic materials according to the various embodiments may display faster fade rates, bathochromic shift, and higher performance ratings compared to comparable indeno-fused naphthopyrans without the electron-withdrawing substituents. Photochromic compositions and articles, such as optical elements, incorporating the photochromic materials are also disclosed.
摘要翻译：公开了包含具有第一吸电子取代基的茚并稠合萘并吡喃的光致变色材料，在某些非限制性实施方案中为第二吸电子取代基。根据各种实施方案的光致变色材料可以显示比没有吸电子取代基的可比的茚并稠合萘并吡喃更快的褪色速率，红移偏移和更高的性能等级。还公开了掺入光致变色材料的光致变色组合物和制品，例如光学元件。

4. 发明申请

US20060228557A1 Photochromic materials having extended pi-conjugated systems and compositions and articles including the same 审中-公开
标题翻译：具有延伸的π-共轭体系的光致变色材料和包含其的组合物和制品
公开(公告)号：US20060228557A1
公开(公告)日：2006-10-12
申请号：US11102279
申请日：2005-04-08
申请人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra
发明人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra
IPC分类号： B32B9/00 , C07D498/02 , C07D491/02 , C07D493/02 , G02F1/361
CPC分类号： C09K9/02 , C07D311/78 , C07D405/04 , C07D409/04 , C07D493/04 , C07D495/04 , C09K2211/1007 , C09K2211/1022 , C09K2211/1059 , C09K2211/1088 , C09K2211/1096 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： Various non-limiting embodiments disclosed herein relate to photochromic materials having extended pi-conjugated systems. For example, various non-limiting embodiments disclosed herein provide a photochromic material, such as an indeno-fused naphthopyran, which comprises a group that extends the pi-conjugated system of the indeno-fused naphthopyran bonded at the 11-position thereof. Further, the photochromic materials according to certain non-limiting embodiments disclosed herein may display hyperchromic absorption of electromagnetic radiation as compared to conventional photochromic materials and/or may have a closed-form absorption spectrum that is bathochromically shifted as compared to conventional photochromic materials. Other non-limiting embodiments relate to photochromic compositions and photochromic articles, such as optical elements, made using the disclosed photochromic materials, and methods of making the same.
摘要翻译：本文公开的各种非限制性实施方案涉及具有延伸的π-共轭体系的光致变色材料。例如，本文公开的各种非限制性实施方案提供光致变色材料，例如茚并稠合的萘并吡喃，其包含延伸在其11位键合的茚并稠合的萘并吡喃的π-共轭体系的基团。此外，与常规光致变色材料相比，根据本文公开的某些非限制性实施方案的光致变色材料可以显示电磁辐射的超色吸收和/或可以具有与常规光致变色材料相比被红移的闭合形式的吸收光谱。其它非限制性实施方案涉及光致变色组合物和光致变色制品，例如使用所公开的光致变色材料制备的光学元件及其制备方法。

5. 发明申请

US20060226402A1 Ophthalmic devices comprising photochromic materials having extended PI-conjugated systems 审中-公开
标题翻译：眼科装置包括具有延长的PI共轭系统的光致变色材料
公开(公告)号：US20060226402A1
公开(公告)日：2006-10-12
申请号：US11102047
申请日：2005-04-08
申请人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra , Frank Molock , Shivkumar Mahadevan
发明人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra , Frank Molock , Shivkumar Mahadevan
IPC分类号： G02B5/23 , G02B1/00
CPC分类号： C09K9/02 , C09B57/02 , C09B69/109 , C09K2211/1007 , C09K2211/1011 , C09K2211/1059 , C09K2211/1088 , C09K2211/1096 , G02B1/043 , C08L101/14
摘要： Various non-limiting embodiments disclosed herein relate to ophthalmic devices comprising photochromic materials having extended pi-conjugated systems. For example, various non-limiting embodiments disclosed herein provide a photochromic material, such as an indeno-fused naphthopyran, which comprises a group that extends the pi-conjugated system of the indeno-fused naphthopyran bonded at the 11-position of thereof. Further, the photochromic materials according to certain non-limiting embodiments disclosed herein may display hyperchromic absorption of electromagnetic radiation as compared to conventional photochromic materials and/or may have a closed-form absorption spectrum that is bathochromically shifted as compared to conventional photochromic materials. Other non-limiting embodiments relate to methods of making the ophthalmic devices comprising photochromic materials.
摘要翻译：本文公开的各种非限制性实施方案涉及包含具有延伸的π-共轭体系的光致变色材料的眼科装置。例如，本文公开的各种非限制性实施方案提供光致变色材料，例如茚并稠合的萘并吡喃，其包含延伸在其11位键合的茚并稠合的萘并吡喃的π-共轭体系的基团。此外，与常规光致变色材料相比，根据本文公开的某些非限制性实施方案的光致变色材料可以显示电磁辐射的超色吸收和/或可以具有与常规光致变色材料相比被红移的闭合形式的吸收光谱。其它非限制性实施方案涉及制备包含光致变色材料的眼科装置的方法。

6. 发明申请

US20090072206A1 OPHTHALMIC DEVICES COMPRISING PHOTOCHROMIC MATERIALS HAVING EXTENDED PI-CONJUGATED SYSTEMS 审中-公开
标题翻译：包含具有扩展PI连接系统的光致变色材料的光学器件
公开(公告)号：US20090072206A1
公开(公告)日：2009-03-19
申请号：US12265842
申请日：2008-11-06
申请人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra , Frank Molock , Shivkumar Mahadevan
发明人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra , Frank Molock , Shivkumar Mahadevan
IPC分类号： G02B5/23
CPC分类号： C09K9/02 , C09B57/02 , C09B69/109 , C09K2211/1007 , C09K2211/1011 , C09K2211/1059 , C09K2211/1088 , C09K2211/1096 , G02B1/043 , C08L101/14
摘要： Various non-limiting embodiments disclosed herein relate to ophthalmic devices comprising photochromic materials having extended pi-conjugated systems. For example, various non-limiting embodiments disclosed herein provide a photochromic material, such as an indeno-fused naphthopyran, which comprises a group that extends the pi-conjugated system of the indeno-fused naphthopyran bonded at the 11-position of thereof. Further, the photochromic materials according to certain non-limiting embodiments disclosed herein may display hyperchromic absorption of electromagnetic radiation as compared to conventional photochromic materials and/or may have a closed-form absorption spectrum that is bathochromically shifted as compared to conventional photochromic materials. Other non-limiting embodiments relate to methods of making the ophthalmic devices comprising photochromic materials.
摘要翻译：本文公开的各种非限制性实施方案涉及包含具有延伸的π-共轭体系的光致变色材料的眼科装置。例如，本文公开的各种非限制性实施方案提供光致变色材料，例如茚并稠合的萘并吡喃，其包含延伸在其11位键合的茚并稠合的萘并吡喃的π-共轭体系的基团。此外，与常规光致变色材料相比，根据本文公开的某些非限制性实施方案的光致变色材料可以显示电磁辐射的超色吸收和/或可以具有与常规光致变色材料相比被红移的闭合形式的吸收光谱。其它非限制性实施方案涉及制备包含光致变色材料的眼科装置的方法。

7. 发明授权

US09028728B2 Photochromic materials that include indeno-fused naphthopyrans 有权
标题翻译：包括茚并稠合萘并吡喃的光致变色材料
公开(公告)号：US09028728B2
公开(公告)日：2015-05-12
申请号：US13314297
申请日：2011-12-08
申请人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
发明人： Kevin E. Bancroft , Anu Chopra , Xiao-Man Dai , Beon-Kyu Kim , David B. Knowles , Jason R. Lewis , Victor A. Montes , Stephen D. Straight , Massimiliano Tomasulo , Barry Van Gemert , Robert W. Walters , Wenjing Xiao , Huayun Yu , Elizabeth A. Zezinka
IPC分类号： G02B5/23 , C07D405/04 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , G03C1/73 , C07D311/78 , C07D311/94 , G03C1/00 , G03C1/685
CPC分类号： C07D405/04 , C07D311/78 , C07D311/94 , C07D405/10 , C07D407/12 , C07D409/04 , C07D493/04 , C07D495/04 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1022 , C09K2211/1033 , C09K2211/1059 , C09K2211/1088 , G02B5/23 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： The present invention relates to photochromic materials that include one or more indeno-fused naphthopyrans that have particular groups at the 7, 11, and 13 positions thereof, and at the position alpha to the oxygen of the pyran ring thereof. With some embodiments, hydrogen or an alkoxy group is bonded to the 7 position, an optionally substituted phenyl is bonded to the 11 position, two alkyl groups are bonded to the 13 position, and two optionally substituted phenyl groups are bonded to the position alpha to the oxygen of the pyran ring of the indeno-fused naphthopyran compound. The 13 position of the indeno-fused naphthopyrans is free of ether groups in which an ether oxygen is bonded to the 13 position, and hydroxyl. The present invention also relates to photochromic articles and compositions that include such indeno-fused naphthopyrans.
摘要翻译：本发明涉及光致变色材料，其包括一种或多种茚并稠合的萘并吡喃，其在其7,11和13位具有特定基团，并且在其吡喃环的氧的位置。在一些实施方案中，氢或烷氧基键合至7位，任选取代的苯基键合至11位，两个烷基键合至13位，并且两个任选取代的苯基键合至位置α 茚并稠合萘并吡喃化合物的吡喃环的氧。茚并稠合萘并吡喃的13位没有醚基，其中醚氧与13位结合，羟基。本发明还涉及包含这种茚并稠合萘并吡喃的光致变色制品和组合物。

8. 发明申请

US20090032782A1 PHOTOCHROMIC MATERIALS HAVING EXTENDED PI-CONJUGATED SYSTEMS AND COMPOSITIONS AND ARTICLES INCLUDING THE SAME 审中-公开
标题翻译：具有扩展的PI连接系统和组合物的光致变色材料和包括其的文章
公开(公告)号：US20090032782A1
公开(公告)日：2009-02-05
申请号：US12136339
申请日：2008-06-10
申请人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra
发明人： Beon-Kyu Kim , Jun Deng , Wenjing Xiao , Barry Van Gemert , Anu Chopra
IPC分类号： C07D405/14 , C07D311/78 , C07D405/10 , G02B5/23
CPC分类号： C09K9/02 , C07D311/78 , C07D405/04 , C07D409/04 , C07D493/04 , C07D495/04 , C09K2211/1007 , C09K2211/1022 , C09K2211/1059 , C09K2211/1088 , C09K2211/1096 , G03C1/685 , G03C1/73 , Y10T428/31504
摘要： Various non-limiting embodiments disclosed herein relate to photochromic materials having extended pi-conjugated systems, such as an indeno-fused naphthopyran, which comprises a group that extends the pi-conjugated system of the indeno-fused naphthopyran bonded at the 11-position thereof. Further, the photochromic materials according to certain non-limiting embodiments disclosed herein may display hyperchromic absorption of electromagnetic radiation as compared to conventional photochromic materials and/or may have a closed-form absorption spectrum that is bathochromically shifted as compared to conventional photochromic materials. Other non-limiting embodiments relate to photochromic compositions and photochromic articles, such as optical elements, made using the disclosed photochromic materials, and methods of making the same.
摘要翻译：本文公开的各种非限制性实施方案涉及具有延伸的π-共轭体系的光致变色材料，例如茚并稠合萘并吡喃，其包含延伸在其11位键合的茚并稠合萘并吡喃的π-共轭体系的基团。此外，与常规光致变色材料相比，根据本文公开的某些非限制性实施方案的光致变色材料可以显示电磁辐射的超色吸收和/或可以具有与常规光致变色材料相比被红移的闭合形式的吸收光谱。其它非限制性实施方案涉及使用所公开的光致变色材料制备的光致变色组合物和光致变色制品，例如光学元件，及其制备方法。

9. 发明申请

US20050127336A1 Pyrano-quinolines, pyrano-quinolinones, combinations thereof, photochromic compositions and articles 失效
标题翻译：吡喹啉，吡喃 - 喹啉酮，其组合，光致变色组合物和制品
公开(公告)号：US20050127336A1
公开(公告)日：2005-06-16
申请号：US10732008
申请日：2003-12-10
申请人： Beon-Kyu Kim , Anil Kumar , Barry Gemert
发明人： Beon-Kyu Kim , Anil Kumar , Barry Gemert
IPC分类号： C07D491/04 , G02B5/23
CPC分类号： C07D491/04
摘要： Described are compositions of at least one material represented by a pyrano[3,2-c]quinoline structure, a pyrano[3,2-c]quinolinone structure or mixtures thereof. The pyrano[3,2-c]quinoline structure is characterized by having a nitrogen atom at the 6-position ring atom and an oxy-substituent at the 5-position ring atom. The pyrano[3,2-c]quinolinone structure is characterized by having a substituted nitrogen atom at the 6-position ring atom and an oxo-substituent at the 5-position ring atom, the nitrogen atom substituents being hydrogen, aliphatic substituents, cycloaliphatic substituents, aromatic substituents, heteroaromatic substituents or a combination thereof. Both of the pyrano[3,2-c]quinoline and pyrano[3,2-c]quinolinone structures are characterized by having two substituents at the 2-position ring atom, each substituent being independently chosen from aliphatic substituents, cycloaliphatic substituents, aromatic substituents, heteroaromatic substituents or a combination thereof, provided that both substituents at the 2-position are not aliphatic. Alternatively, the two substituents at the 2-position can combine to form a spirocyclic group, provided that the spirocyclic group is not norbornylidene or bicyclo[3.3.1]9-nonylidene. The ring atoms have been numbered according to the International Union of Pure and Applied Chemistry rules of nomenclature starting with the 1-position ring atom being the oxygen atom of the pyran ring and numbering counterclockwise therefrom. Also described are photochromic articles that contain or that have coatings or films containing at least one of the novel compositions or combinations thereof with other photochromic materials.
摘要翻译：描述了由吡喃并[3,2-c]喹啉结构，吡喃并[3,2-c]喹啉酮结构或其混合物表示的至少一种材料的组合物。吡喃并[3,2-c]喹啉结构的特征在于在6-位环原子上具有氮原子和在5位环原子上具有氧取代基。吡喃并[3,2-c]喹啉酮结构的特征在于在6位环原子上具有取代的氮原子，在5位环原子上具有氧代取代基，氮原子取代基为氢，脂族取代基，脂环族取代基，芳族取代基，杂芳族取代基或其组合。吡喃并[3,2-c]喹啉和吡喃并[3,2-c]喹啉酮结构的特征在于在2-位环原子上具有两个取代基，每个取代基独立地选自脂族取代基，脂环族取代基，芳香族取代基，杂芳族取代基或其组合，条件是2-位上的两个取代基不是脂族的。或者，2-位上的两个取代基可以组合形成螺环基团，条件是螺环基团不是降冰片基或双环[3.3.1] 9-壬叉基。环原子根据国际纯粹和应用化学联合会的命名法编号，起始于1位环原子是吡喃环的氧原子并从其逆时针编号。还描述了含有或具有包含至少一种新组合物或其组合与其它光致变色材料的涂层或膜的光致变色制品。

10. 发明申请

US20130065056A1 PHOTOCHROMIC MATERIALS HAVING EXTENDED PI-CONJUGATED SYSTEMS AND COMPOSITIONS AND ARTICLES INCLUDING THE SAME 有权
公开(公告)号：US20130065056A1
公开(公告)日：2013-03-14
申请号：US13417662
申请日：2012-03-12
申请人： Anu Chopra , Jun Deng , Beon-Kyu Kim , David B. Knowies , Frank F. Molock, JR. , Victor A. Montes , Stephen D. Straight , Wenjing Xiao , Huayun Yu
发明人： Anu Chopra , Jun Deng , Beon-Kyu Kim , David B. Knowies , Frank F. Molock, JR. , Victor A. Montes , Stephen D. Straight , Wenjing Xiao , Huayun Yu
IPC分类号： C07D311/94 , C07D413/14 , C07D413/10 , G02B5/23 , C07D405/10
CPC分类号： G02C7/049 , C07D311/94 , C09K9/02 , C09K2211/1007 , C09K2211/1011 , C09K2211/1059 , C09K2211/1088 , C09K2211/1096 , G02B1/041 , G02B1/043 , G02C7/102 , Y10T428/31504 , C08L101/14
摘要： The present invention provides ophthalmic devices comprising at least one photochromic material which is an indeno-fused naphthopyran having a pi-conjugation extending group bonded to the 11-position of the indeno-fused naphthopyran, the pi-conjugation extending group having at least one pendent halo-substituted group bonded thereto. The pi-conjugation extending group extends the pi-conjugation system of said indeno-fused naphthopyran. The 13-position of the indeno-fused naphthopyran is substantially free of spiro-substituents. The invention further provides photochromic materials of specified structure, photochromic compositions, photochromic articles and optical elements that include the photochromic materials. Other non-limiting embodiments relate to methods of making the ophthalmic devices comprising photochromic materials.

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