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1. 发明申请

US20120022287A1 Spray Process for Selective Oxidation 有权
标题翻译：选择氧化喷涂工艺
公开(公告)号：US20120022287A1
公开(公告)日：2012-01-26
申请号：US13258159
申请日：2010-03-23
申请人： Bala Subramaniam , Daryle H. Busch , Fenghul Niu
发明人： Bala Subramaniam , Daryle H. Busch , Fenghul Niu
IPC分类号： C07C51/265
CPC分类号： C07C51/255 , B01J4/002 , B01J10/007 , B01J2219/00006 , B01J2219/00063 , B01J2219/00065 , B01J2219/00162 , C07C51/265 , C07C63/00
摘要： Oxidation process can include: introducing small droplets of liquid reaction mixture having oxidizable reactant, catalyst, and solvent into a reaction zone containing oxygen and diluent gas; and oxidizing the reactant with the oxygen at a suitable reaction temperature and a suitable reaction pressure to produce an oxidized product. The liquid reaction mixture can have an aromatic feedstock having an oxidizable substituent as the oxidizable reactant. The oxidized product can include an aromatic compound having at least one carboxylic acid. For example, the aromatic feedstock can include a benzene ring having at least one oxidizable alkyl substituent, furan hetero-ring having at least one oxidizable alkyl substituent, a naphthalene poly-ring having at least one oxidizable alkyl substituent, derivatives thereof, and mixtures thereof.
摘要翻译：氧化过程可以包括：将具有可氧化反应物，催化剂和溶剂的小液滴的液体反应混合物引入含有氧气和稀释气体的反应区; 并在合适的反应温度和合适的反应压力下用氧氧化反应物以产生氧化产物。液体反应混合物可具有具有可氧化取代基的芳族原料作为可氧化反应物。氧化产物可以包括具有至少一个羧酸的芳族化合物。例如，芳族原料可以包括具有至少一个可氧化烷基取代基的苯环，具有至少一个可氧化烷基取代基的呋喃异环，具有至少一个可氧化烷基取代基的萘多环，其衍生物及其混合物。

2. 发明授权

US09238608B2 Spray process for selective oxidation 有权
标题翻译：用于选择性氧化的喷涂工艺
公开(公告)号：US09238608B2
公开(公告)日：2016-01-19
申请号：US13258159
申请日：2010-03-23
申请人： Bala Subramaniam , Daryle H. Busch , Fenghul Niu
发明人： Bala Subramaniam , Daryle H. Busch , Fenghul Niu
IPC分类号： C07C51/265 , C07C51/255 , B01J4/00 , B01J10/00
CPC分类号： C07C51/255 , B01J4/002 , B01J10/007 , B01J2219/00006 , B01J2219/00063 , B01J2219/00065 , B01J2219/00162 , C07C51/265 , C07C63/00
摘要： Oxidation process can include: introducing small droplets of liquid reaction mixture having oxidizable reactant, catalyst, and solvent into a reaction zone containing oxygen and diluent gas; and oxidizing the reactant with the oxygen at a suitable reaction temperature and a suitable reaction pressure to produce an oxidized product. The liquid reaction mixture can have an aromatic feedstock having an oxidizable substituent as the oxidizable reactant. The oxidized product can include an aromatic compound having at least one carboxylic acid. For example, the aromatic feedstock can include a benzene ring having at least one oxidizable alkyl substituent, furan hetero-ring having at least one oxidizable alkyl substituent, a naphthalene poly-ring having at least one oxidizable alkyl substituent, derivatives thereof, and mixtures thereof.
摘要翻译：氧化过程可以包括：将具有可氧化反应物，催化剂和溶剂的小液滴的液体反应混合物引入含有氧气和稀释气体的反应区; 并在合适的反应温度和合适的反应压力下用氧氧化反应物以产生氧化产物。液体反应混合物可具有具有可氧化取代基的芳族原料作为可氧化反应物。氧化产物可以包括具有至少一个羧酸的芳族化合物。例如，芳族原料可以包括具有至少一个可氧化烷基取代基的苯环，具有至少一个可氧化烷基取代基的呋喃异环，具有至少一个可氧化烷基取代基的萘多环，其衍生物及其混合物。

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