会员体验
专利管家(专利管理)
工作空间(专利管理)
风险监控(情报监控)
数据分析(专利分析)
侵权分析(诉讼无效)
联系我们
交流群
官方交流:
QQ群: 891211   
微信请扫码    >>>
现在联系顾问~
热词
    • 6. 发明专利
    • Method for crystallization for producing bisphenol
    • 用于生产双酚的结晶方法
    • JP2008179633A
    • 2008-08-07
    • JP2008001117
    • 2008-01-08
    • Bayer Materialscience Agバイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
    • MUENNICH CHRISTIANBLASCHKE ULRICHEEK ROBPREIN MICHAELAUDENAERT RAYMONDTYTGAT GERT
    • C07C29/78C07C39/16
    • C07C37/20C07C37/84C07C39/16
    • PROBLEM TO BE SOLVED: To provide a method for producing a bisphenol having >99.7% purity. SOLUTION: The method for producing a bisphenol having >99.7% purity comprises (a) reacting phenol with acetone in the presence of an acidic catalyst to form a bisphenol-containing product mixture, (b) taking out at least a portion of the bisphenol from the product mixture in a form of a bisphenol/phenol adduct by crystallization, filtration and washing, to provide bisphenol/phenol adduct crystals, and (c) removing at least a portion of the phenol from the bisphenol/phenol adduct crystals to provide the bisphenol having high purity of >99.7%, wherein the crystallization comprises continuous suspension crystallization and is carried out in at least three crystallization devices constituted so that the product mixture is first cooled in a first stage of crystallization to a temperature of 50-70°C in a first crystallization device and a second crystallization device connected in parallel, and subsequently cooled in a second stage of the crystallization to a temperature of 40-50°C in a third crystallization device connected downstream in series to the first and second crystallization devices, and wherein a total residence time of the product mixture in the crystallization is >4 hr. COPYRIGHT: (C)2008,JPO&INPIT
    • 待解决的问题:提供一种生产纯度> 99.7%的双酚的方法。 解决方案:制备纯度> 99.7%的双酚的方法包括(a)在酸性催化剂存在下使苯酚与丙酮反应以形成含双酚的产物混合物,(b)取出至少一部分 通过结晶,过滤和洗涤从双酚/苯酚加合物形式的产物混合物中提供双酚/酚加合物晶体,和(c)从双酚/苯酚加合物晶体中除去至少一部分苯酚至 提供高纯度> 99.7%的双酚,其中结晶包括连续悬浮液结晶,并且在至少三个结晶装置中进行,所述结晶装置构成使得产物混合物首先在结晶的第一阶段被冷却至50-70℃ ℃的第一结晶装置和第二结晶装置并联连接,随后在第二结晶阶段中在40-50℃的温度下在 第三结晶装置与第一和第二结晶装置串联连接下游,并且其中产物混合物在结晶中的总停留时间> 4小时。 版权所有(C)2008,JPO&INPIT
    • 8. 发明专利
    • Method for producing high-purity bisphenol a
    • 生产高纯度双酚A的方法
    • JP2006335760A
    • 2006-12-14
    • JP2006155618
    • 2006-06-05
    • Bayer Materialscience Agバイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
    • BLASCHKE ULRICHWESTERNACHER STEFANBRAUN ARNEAUDENAERT RAYMONDZANK JESKO
    • C07C37/20C07B61/00C07C37/74C07C37/82C07C37/84C07C39/16
    • C07C39/16C07C37/20C07C37/84
    • PROBLEM TO BE SOLVED: To provide a method for producing high-purity bisphenol A (BPA). SOLUTION: This method for producing the high-purity bisphenol A includes processes (a) to (k) as follows: (a) reacting phenol with acetone in the presence of an acidic ion exchanger and a sulfur-containing cocatalyst, so as to obtain a product mixture; (b) continuously obtaining crystals of a BPA-phenol adduct from the product mixture; (c) separating the adduct obtained in the process (b), so as to obtain a solid phase and a liquid phase; (d) washing the solid phase, so as to obtain a washed solid phase and a second liquid phase; (e) distilling the liquid phase and the second liquid phase, so as to obtain a dehydrated solution; (f) introducing at least 90 wt% of the dehydrated solution into the process (a); (g) adding the phenol to the washed solid phase obtained in the process (d), so as to obtain a homogeneous substance system; (h) continuously obtaining the crystals of the BPA-phenol adduct from the homogeneous substance system; (i) separating the crystals obtained in the process (h), so as to obtain a second solid phase; (j) washing the second solid phase, so as to obtain a washed adduct; and (k) heating the washed adduct, so as to remove the phenol. COPYRIGHT: (C)2007,JPO&INPIT
    • 待解决的问题:提供一种生产高纯度双酚A(BPA)的方法。 解决方案:用于生产高纯度双酚A的方法包括以下方法(a)至(k):(a)在酸性离子交换剂和含硫助催化剂存在下使苯酚与丙酮反应,因此 获得产品混合物; (b)从产物混合物中连续获得BPA-酚加合物的晶体; (c)分离方法(b)中获得的加合物,以获得固相和液相; (d)洗涤固相,以获得洗涤的固相和第二液相; (e)蒸馏液相和第二液相,得到脱水溶液; (f)将至少90重量%的脱水溶液引入到方法(a)中; (g)在方法(d)中得到的洗涤固相中加入苯酚,得到均匀物质体系; (h)从均匀物质体系连续得到BPA-苯酚加成物的晶体; (i)分离方法(h)中得到的晶体,得到第二固相; (j)洗涤第二固相,以获得洗涤的加合物; 和(k)加热洗涤的加合物,以除去苯酚。 版权所有(C)2007,JPO&INPIT