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1. 发明专利

JP2009209372A Phase interface method related to production of polycarbonate 有权
标题翻译：与生产聚碳酸酯相关的相接口方法
公开(公告)号：JP2009209372A
公开(公告)日：2009-09-17
申请号：JP2009051589
申请日：2009-03-05
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： EBERT WOLFGANG , KORDS CHRISTIAN , BACHMANN ROLF , OBENDORF LARS , EYNDE JOHAN VANDEN , RUYTINX BERT , SEEBA JOHANN
IPC分类号： C08G64/24
CPC分类号： C08G64/24
摘要： PROBLEM TO BE SOLVED: To provide a method of reducing an excessive phosgene as much as possible, and capable of preventing a defect of a prior art from being generated, as to an efficient continuous production method of a polycarbonate using a phase interface method. SOLUTION: This production method of reacting a dihydroxy diaryl alkane with phosgene in the presence of a catalyst by the phase interface method includes a process for dispersing continuously an organic phase containing a solvent suitable for the phosgene and the polycarbonate, and an aqueous phase containing the dihydroxy diaryl alkane, water and an alkaline solution existing at an amount of 1.5-2.5 mol. per one mole of the dihydroxy diaryl alkane, in a disperser 1, a process for reacting a mixture therein within 0.5 or less of residence time, in the first reactor, a process for reacting further the mixture while adding an additional alkaline solution, in the second reactor, and a process for carrying out condensation by adding an additional alkaline solution, and a chain terminator when necessary, in the presence of the catalyst, in the third reactor. COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供尽可能减少过量的光气并且能够防止现有技术的缺陷产生的方法，关于使用相界面的聚碳酸酯的有效的连续制备方法方法。解决方案：通过相界面法在催化剂存在下使二羟基二芳基烷烃与光气反应的该制备方法包括连续分散含有适用于光气和聚碳酸酯的溶剂的有机相和相含有二羟基二芳基烷烃，水和碱性溶液，其量为1.5-2.5mol。在分散器1中，在其中在其中的混合物的反应时间在0.5或更小的停留时间内的方法，在第一反应器中，使进一步混合物同时加入另外的碱性溶液的方法在第二反应器，以及通过添加额外的碱性溶液进行缩合的方法，必要时在催化剂的存在下在第三反应器中进行链终止剂。版权所有（C）2009，JPO＆INPIT

2. 发明申请

WO2008052662A3 METHOD FOR TREATING METAL SURFACES 审中-公开
标题翻译：方法在金属表面的处理
公开(公告)号：WO2008052662A3
公开(公告)日：2008-07-31
申请号：PCT/EP2007009024
申请日：2007-10-18
申请人： BAYER MATERIALSCIENCE AG , EBERT WOLFGANG , MELLIS RAINER , MEYER ALEXANDER , RUYTINX BERT , KARBACH ALEXANDER , MICHALSKI-VOLLMER DETLEF
发明人： EBERT WOLFGANG , MELLIS RAINER , MEYER ALEXANDER , RUYTINX BERT , KARBACH ALEXANDER , MICHALSKI-VOLLMER DETLEF
IPC分类号： C23C22/50 , C08G64/40 , C23C8/10 , C23C22/06
CPC分类号： C23C22/06 , B29C33/00 , B29C47/0009 , B29C47/68 , B29C47/686 , B29K2069/00 , C08G64/406 , C23C8/10 , C23C22/50
摘要： The invention relates to a method for treating metal surfaces which come into contact with the polymer melt during the production of polymers, characterized in that the metal surfaces are thermally pretreated in an oxidative atmosphere.
摘要翻译：一种用于治疗落入在生产与在接触聚合物熔体的聚合物的金属表面处理，其特征在于所述金属表面在氧化气氛中热预处理。

3. 发明申请

WO2008052664A3 METHOD FOR FILTERING SUBSTRATE MATERIALS 审中-公开
标题翻译：过滤基材的方法
公开(公告)号：WO2008052664A3
公开(公告)日：2008-10-30
申请号：PCT/EP2007009026
申请日：2007-10-18
申请人： BAYER MATERIALSCIENCE AG , EBERT WOLFGANG , NIETZWETZKI BERNHARD , MELLIS RAINER , HAESE WILFRIED , RUYTINX BERT , KARBACH ALEXANDER , MEYER ALEXANDER
发明人： EBERT WOLFGANG , NIETZWETZKI BERNHARD , MELLIS RAINER , HAESE WILFRIED , RUYTINX BERT , KARBACH ALEXANDER , MEYER ALEXANDER
IPC分类号： B29C47/68 , B29C45/17
CPC分类号： B29C47/68 , B29C45/17 , B29C47/0021 , B29C47/0877 , B29C47/686 , B29K2069/00 , B29L2011/00 , B29L2017/005 , C08G64/406
摘要： The invention relates to a method for filtering polycarbonate, characterized in that the polycarbonate melt having an average molecular weight (weight-average) of 14.000 to 30.000 g/mol is filtered through at least one metal nonwoven having a thickness ranging from 5 mm to 1 mm and comprising two or more layers, at least one layer having a thickness ranging from 0,05 to 0,2 mm and a pore size from 1 to 10 µm.
摘要翻译：本发明涉及一种用于聚碳酸酯的过滤方法，其特征在于，具有14,000的平均分子量（重均）的熔融聚碳酸酯至30,000克/摩尔由厚度为5毫米至1毫米的至少一种金属羊毛，由2个或更多其中至少一层厚度为0.05至0.2毫米，孔径为1至10微米的层被过滤。

4. 发明申请

WO2008052669A3 SUBSTRATE MATERIALS FOR TRANSPARENT INJECTION MOULDINGS 审中-公开
标题翻译：透明注塑件用基材
公开(公告)号：WO2008052669A3
公开(公告)日：2008-07-17
申请号：PCT/EP2007009065
申请日：2007-10-19
申请人： BAYER MATERIALSCIENCE AG , MEYER ALEXANDER , EBERT WOLFGANG , HAESE WILFRIED , KRETSCHMAR GABRIELE , REITZE BURKHARD , WINZEN THOMAS , BRUDER FRIEDRICH-KARL , RUYTINX BERT , KARBACH ALEXANDER , VOETZ MATTHIAS , POGODA ANDREAS
发明人： MEYER ALEXANDER , EBERT WOLFGANG , HAESE WILFRIED , KRETSCHMAR GABRIELE , REITZE BURKHARD , WINZEN THOMAS , BRUDER FRIEDRICH-KARL , RUYTINX BERT , KARBACH ALEXANDER , VOETZ MATTHIAS , POGODA ANDREAS
IPC分类号： G11B7/00 , G11B7/253 , G11B7/2534
CPC分类号： C08G64/406 , G01N33/442 , G11B7/2534 , Y10T428/21 , Y10T428/269
摘要： The invention relates to polycarbonates or substrate materials, characterized by a specific distribution of the particle diameters of fluorescent particles contained, and to the use thereof for producing mouldings and extrudates.
摘要翻译：本发明涉及聚碳酸酯或基底材料，其特征在于所含荧光颗粒的粒径的一定分布，以及它们用于生产模制品和挤出物的用途。

5. 发明专利

BRPI0718262A2 未知
公开(公告)号：BRPI0718262A2
公开(公告)日：2014-01-07
申请号：BRPI0718262
申请日：2007-10-19
申请人： BAYER MATERIALSCIENCE AG
发明人： MEYER ALEXANDER , EBERT WOLFGANG , HAESE WILFRIED , KRETSCHMAR GABRIEL , REITZE BURKHARD , WINZEN THOMAS , BRUDER FRIEDRICH-KARL , RUYTINX BERT , KARBACH ALEXANDER , VOETZ MATTHIAS , POGODA ANDREAS
IPC分类号： G11B7/00 , G11B7/253 , G11B7/2534
摘要： A polycarbonate resin comprising fluorescing particles that feature a particular size distribution is disclosed. The size distribution of these particles that fluoresce upon excitation at wavelengths of 400-440 nm, 50x magnification and illumination time of 40 msec per scan was found to be critical in determining the suitability of the resin for optical, particularly optical storage, applications.

6. 发明专利

DE102006051305A1 未知
公开(公告)号：DE102006051305A1
公开(公告)日：2008-05-08
申请号：DE102006051305
申请日：2006-10-31
申请人： BAYER MATERIALSCIENCE AG
发明人： EBERT WOLFGANG , NIETZWETZKI BERNHARD , MELLIS RAINER , HAESE WILFRIED , MEYER ALEXANDER , RUYTINX BERT , KARBACH ALEXANDER
IPC分类号： C08G64/40 , B01D61/14
摘要： A process for purifying polycarbonate is disclosed. The process entails filtering molten polycarbonate having weight average molecular weight of 14,000 to 30,000 g/mol through at least one non-woven metal structure having a thickness of 5 to 1 mm, said structure including at least one dense layer, and at least one less dense layer wherein said dense layer is 0.05 to 0.2 mm thick and has pore size of 1 to 10 mum to obtain pure polycarbonate.

7. 发明专利

DE102004061715A1 未知
公开(公告)号：DE102004061715A1
公开(公告)日：2006-07-06
申请号：DE102004061715
申请日：2004-12-22
申请人： BAYER MATERIALSCIENCE AG
发明人： KAUTH HERMANN , EBERT WOLFGANG , HAESE WILFRIED , EINBERGER HELMUT , MEYER ALEXANDER , FRANKENAU ANDREAS , FRANZ ULI , EH CHRISTIAN , VOS STEFAAN DE , RUYTINX BERT
IPC分类号： C08G64/24
摘要： An improvement to the phase interface process of preparing aromatic polycarbonate is disclosed. The process is characterized in that the phosgenation is carried out at 0 to 40° C., and in that the temperature of the reaction mixture at the time of addition of the catalyst at 10 to 40° C., and in that the molar ratio of aromatic dihydroxy compounds to phosgene at 1:1.05 to 1:1.20. The polycarbonate thus produced is characterized in its low content of carbamates, making it particularly suitable for the preparation of optical storage media.

8. 发明专利

SG10201402741PA ULTRA-HIGH PURITY POLYCARBONATES HAVING GOOD INHERENT COLOR AND THERMAL RESISTANCE AND A DEVICE AND A METHOD FOR PRODUCING THE SAME 未知
公开(公告)号：SG10201402741PA
公开(公告)日：2014-07-30
申请号：SG10201402741P
申请日：2010-05-26
申请人： BAYER MATERIALSCIENCE AG
发明人： KÖNIG THOMAS , KIRCHHOFF JÖRG , BIERDEL MICHAEL , KOHLGRÜBER KLEMENS , RECHNER JOHANN , VAES JOHAN , VANDEN EYNDE JOHAN , BRUYNSEELS FRANK , RUYTINX BERT
IPC分类号： B29C48/38 , B29C48/76
摘要： Aromatic polycarbonate, comprising less than 5 ppm of aromatic chloro compounds, less than 0.5 ppm of dichloromethane, less than 5 ppm of univalent phenol and less than 0.5 ppm of aromatic compound, which is free of chlorine, is new. Independent claims are included for: (1) a device, for degassing of solvent-based polycarbonate melt, comprising a degassing extruder with at least three degassing zones, and a zone, before the degassing zones, for dispersing a stripping agent; and (2) the preparation of the polycarbonate.

9. 发明专利

ES2369326T3 PROCEDIMIENTO PARA LA PREPARACION DE POLICARBONATO SEGUN EL PROCEDIMIENTO DE INTERFASE. 未知
公开(公告)号：ES2369326T3
公开(公告)日：2011-11-29
申请号：ES09002488
申请日：2009-02-21
申请人： BAYER MATERIALSCIENCE AG
发明人： EBERT WOLFGANG , KORDS CHRISTIAN , BACHMANN ROLF , OBENDORF LARS , EYNDE JOHAN VANDEN , RUYTINX BERT , SEEBA JOHANN
IPC分类号： C08G64/24
摘要： Procedimiento para la preparación continua de policarbonatos con pesos moleculares medios Mw de 15000 - 200000 g/mol según el procedimiento de interfase a partir de por lo menos un difenol, fosgeno y por lo menos un catalizador eventualmente en presencia por lo menos un interruptor de cadena y/o ramificador, caracterizado porque (a) se genera una mezcla de la fase orgánica y acuosa, dispersándose en un dispersor de forma continua la fase orgánica en la fase acuosa o la fase acuosa en la fase orgánica, en donde la fase orgánica contiene por lo menos un disolvente apropiado para el policarbonato y contiene el fosgeno parcial o totalmente y la fase acuosa contiene el o los difenoles, agua y lejía alcalina, en donde se añaden entre 1,5 moles y 2,5 moles de lejía alcalina por mol de difenol, (b) a continuación se hace reaccionar la mezcla en un reactor con un tiempo de permanencia inferior a 0,5 s, (c) a continuación la mezcla de reacción se sigue haciendo reaccionar con adición de más lejía alcalina y eventualmente interruptores de cadena en otro reactor y (d) a continuación se lleva a cabo una posterior condensación por adición de más lejía alcalina, eventualmente interruptor(es) de cadena y en presencia de por lo menos un catalizador en por lo menos otro reactor.

10. 发明专利

AT520728T 未知
公开(公告)号：AT520728T
公开(公告)日：2011-09-15
申请号：AT09002488
申请日：2009-02-21
申请人： BAYER MATERIALSCIENCE AG
发明人： EBERT WOLFGANG , KORDS CHRISTIAN , BACHMANN ROLF , OBENDORF LARS , EYNDE JOHAN VANDEN , RUYTINX BERT , SEEBA JOHANN
IPC分类号： C08G64/24
摘要： Continuously producing polycarbonates by phase boundary process, comprises: (a) producing a mixture of organic- and aqueous-phases by continuously dispersing the organic phase in the aqueous phase or the aqueous phase in the organic phase; (b) reacting the mixture in a reactor; (c) further reacting the mixture by adding further alkali metal hydroxide solution and optionally chain terminator(s) in a further reactor; and (d) further condensing by adding further alkali metal hydroxide solution, optionally chain terminator(s) and in the presence of a catalyst in a further reactor. Continuously producing polycarbonates with an average weight average molecular weight of 15000-200000 g/mol, by phase boundary process from at least one dihydroxydiarylalkane, phosgene and at least one catalyst optionally in the presence of at least one chain terminator and/or chain-branching agent, comprises: (a) producing a mixture of organic- and aqueous-phases by continuously dispersing the organic phase in the aqueous phase or the aqueous phase in the organic phase by a disperser, where the organic phase contains at least one suitable solvent for the polycarbonate and complete or partial phosgene and the aqueous phase contains the dihydroxyalkane(s), water and an alkali metal hydroxide solution, and 1.5-2.5 moles of the alkali metal hydroxide solution are added per mole of dihydroxydiarylalkane; (b) reacting the mixture in a reactor with a dwell time of less than 0.5 second; (c) reacting the reaction mixture by adding further alkali metal hydroxide solution and optionally chain terminator(s) in an another reactor; and (d) further condensing by adding further alkali metal hydroxide solution, optionally chain terminator(s) and in the presence of at least one catalyst in at least a further reactor. An independent claim is included for use of a disperser containing a pre-disperser, a homogenizing nozzle and at least three pumps for producing the mixture of organic and aqueous phases during the production of the polycarbonate.

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