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1. 发明专利

JP2010084148A Special polyether-based polyurethane composition for producing holographic medium 有权
标题翻译：用于生产全息介质的特殊聚醚基聚氨酯组合物
公开(公告)号：JP2010084148A
公开(公告)日：2010-04-15
申请号：JP2009226491
申请日：2009-09-30
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： WEISER MARC-STEPHAN , ROELLE THOMAS , BRUDER FRIEDRICH KARL , FAECKE THOMAS , HOENEL DENNIS , LORENZ KLAUS , HOFMANN JOERG DR
IPC分类号： C08G18/48
CPC分类号： C08G18/7837 , C08G18/4866 , C08G18/672 , C08G18/776 , C08G18/7887 , G03F7/001 , G03F7/027 , G03F7/035 , G11B7/24044 , G11B7/245
摘要： PROBLEM TO BE SOLVED: To provide a new polyurethane composition capable of improving a more excellent contrast ratio of a hologram and an improved brightness, without sacrificing adaptability of a matrix polymer and a writing monomer. SOLUTION: The polyurethane compositions includes: (A) a polyisocyanate component; (B) an isocyanate reactive component comprising a Y(X i -H) n type hydroxy-functional multiblock copolymer (B1) which has a number-average molecular weight of 1,000 g/mol or more; (C) a compound which is free from NCO group, having a group reacting with an ethylenic unsaturated compound via polymerization under the action of a chemical ray; (D) a radical stabilizer; and (E) a photoinitiator. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供能够改善全息图的更优异的对比度和改进的亮度的新的聚氨酯组合物，而不牺牲基质聚合物和书写单体的适应性。聚氨酯组合物包括：（A）多异氰酸酯组分; （B）包含数均分子量为1,000的Y（X H）-SSN n / SB>型羟基官能多嵌段共聚物（B1）的异氰酸酯反应性组分 g / mol以上; （C）不含NCO基团的化合物，具有通过在化学射线的作用下聚合而与烯属不饱和化合物反应的基团; （D）自由基稳定剂; 和（E）光引发剂。版权所有（C）2010，JPO＆INPIT

2. 发明专利

JP2007314787A Method for producing polyether polyol 审中-公开
标题翻译：生产聚醚多元醇的方法
公开(公告)号：JP2007314787A
公开(公告)日：2007-12-06
申请号：JP2007135074
申请日：2007-05-22
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , HOFMANN JOERG DR
IPC分类号： C08G65/26
CPC分类号： B01J27/26 , C08G18/36 , C08G18/4866 , C08G65/2663 , C08G2190/00 , Y10S521/914
摘要： PROBLEM TO BE SOLVED: To provide a method for treating a double metal cyanide (DMC) catalyst, which enables the high ratio of a starting compound measured and supplied by a method for continuously measuring and supplying the starter compound to an alkylene oxide, and enables to easily obtain a polyether polyol having an OH value exceeding 200 mg KOH/g. SOLUTION: This method for conditioning the DMC catalyst comprises dispersing the DMC catalyst in a starting solvent containing an addition product of an alkylene oxide to the starter compound having an OH value of about 5 to 500 mgKOH/g and a Zerewitinoff active hydrogen atom, under a pressure of about 1 mbar to about 10 bar at a temperature of about 0°C to about 80°C for about 5 minutes to about 4 hours. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种处理双金属氰化物（DMC）催化剂的方法，其能够通过连续测量和供应起始化合物的方法测量和提供的起始化合物的高比例与环氧烷烃并且能够容易地获得OH值超过200mg KOH / g的聚醚多元醇。解决方案：用于调节DMC催化剂的方法包括将DMC催化剂分散在含有环氧烷加成产物的起始溶剂中，其具有OH值为约5至500mgKOH / g的起始化合物和Zerewitinoff活性氢在约0℃至约80℃的温度下在约1毫巴至约10巴的压力下进行约5分钟至约4小时。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2007146163A Method for producing polyol based on natural oil 审中-公开
标题翻译：基于天然油生产多元醇的方法
公开(公告)号：JP2007146163A
公开(公告)日：2007-06-14
申请号：JP2006318146
申请日：2006-11-27
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS
IPC分类号： C08G65/04 , C08H99/00
CPC分类号： C08G65/2609 , C08G59/32 , C08G63/16 , C08G63/672 , C08G65/2696
摘要： PROBLEM TO BE SOLVED: To provide a simple method for converting non-denatured unsaturated fatty acid triglyceride into an alkylene oxide addition product having a wide OH value range compatible with normal polyether. SOLUTION: The invention relates to the method for producing polyol based on natural oil comprising, (a) a process of oxidizing unsaturated triglyceride by hydrogen peroxide catalyzed with a peroxycarboxylic acid or carboxylic acid, (b) a process of converting the product epoxide group into alcoholic group in situ, (c) a process of separating the product of the process (a) and (b) from volatile components, and (d) a process of forming a polyether polyol by alkoxylating the product alkylene oxide obtained in the processes (a)-(c). COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供将未变性的不饱和脂肪酸甘油三酯转化成具有与正常聚醚相容的宽OH值范围宽的环氧烷加成产物的简单方法。解决方案：本发明涉及用于生产基于天然油的多元醇的方法，其包括：（a）用过氧羧酸或羧酸催化的过氧化氢氧化不饱和甘油三酸酯的方法，（b）将产物环氧基团原位成醇类，（c）将方法（a）和（b）的产物与挥发性成分分离的方法，和（d）通过将获得的产物烯化氧烷氧基化形成聚醚多元醇的方法方法（a） - （c）。版权所有（C）2007，JPO＆INPIT

4. 发明专利

JP2006265553A Poly(ether-ester) polyol and method for producing the same 有权
标题翻译：聚（醚）多元醇及其制备方法
公开(公告)号：JP2006265553A
公开(公告)日：2006-10-05
申请号：JP2006073018
申请日：2006-03-16
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , HOFMANN JOERG DR , NEFZGER HARTMUT
IPC分类号： C08G63/664 , C08G18/42
CPC分类号： C08G18/4887 , C08G65/2615 , C08G65/3311
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a poly(ether-ester) by which a structure having the ester bonds equally and uniformly distributed along the polymer chain, and a well-regulated functional value is provided.
SOLUTION: The poly(ether-ester) containing an OH-functional terminal ester group or terminal carboxylic acid group is obtained by reacting a carboxylic acid ester containing an OH group and represented by the general formula of the figure with an alkylene oxide in the presence of a polyol and a dicarboxylic acid ester with ring opening, and exchanging the ester of the product. (In the formula, R is a monovalent organic group; R' is a divalent organic group; and m is 1 and n is 1, m is 2 or more and n is 1, or n is 2 or more and m is 1).
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：待解决的问题：提供一种制备聚（醚 - 酯）的方法，通过该方法，具有沿聚合物链均匀分布的酯键的结构和良好调节的功能值。解决方案：含有OH官能的末端酯基或末端羧酸基团的聚（醚 - 酯）是通过使含OH基团的羧酸酯与由通式表示的环氧烷在多元醇和具有开环性的二羧酸酯的存在下，交换该产物的酯。（式中，R为1价有机基团，R'为二价有机基团，m为1，n为1，m为2以上且n为1，n为2以上且m为1）。版权所有（C）2007，JPO＆INPIT

5. 发明专利

JP2014162925A Process for preparing polyether polyol 审中-公开
标题翻译：制备聚醚多元醇的方法
公开(公告)号：JP2014162925A
公开(公告)日：2014-09-08
申请号：JP2014031292
申请日：2014-02-21
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , EICHMANN MARKUS
IPC分类号： C08G65/26 , C08G65/10 , C08G65/28
CPC分类号： C08G65/2606 , C08G65/00 , C08G65/2609 , C08G65/2648 , C08G65/2696 , C08G65/30
摘要： PROBLEM TO BE SOLVED: To provide a process for preparing polyether polyol based on a starter which is a solid at room temperature.SOLUTION: There is provided the process for preparing polyether polyol having n Eblocks having 75 wt.% or more of an oxyethylene unit and m Pblocks having 60 wt.% or more of an oxypropylene unit and based on an active hydrogen-containing starter, where n and m are natural numbers of 1 to 10. The process for preparing polyether polyol comprises reacting an active hydrogen-containing starter having a melting point of 40°C or more with ethylene oxide (EO) and propylene oxide (PO) by adding a catalyst. The reaction with PO is conducted during addition of the Pblocks under a condition represented by the following inequality, where x(PO) is the amount of PO, x(OH) is the amount of an OH group in the polyether polyol, t(PO) is addition time of PO, OHZ is a calculated OH value of the polyether polyol, and m is the natural number of 1 to 10, and the total content of the oxyethylene unit in the polyether polyol based on the total amount of the added alkylene oxide is 5 to 90 wt.%.
摘要翻译：要解决的问题：提供一种制备基于在室温下为固体的起动剂的聚醚多元醇的方法。解决方案：提供了制备具有75重量％或更多的氧化乙烯单元的n个Eblock的聚醚多元醇的方法和具有60重量％或更多的氧化丙烯单元并且基于活性含氢起始物的m Pb嵌段，其中n和m为1至10的天然数。制备聚醚多元醇的方法包括使含活性氢的起始物通过加入催化剂与环氧乙烷（EO）和环氧丙烷（PO）的熔点为40℃以上。在POPS的添加条件下，在以下不等式表示的条件下进行与PO的反应，其中x（PO）是PO的量，x（OH）是聚醚多元醇中OH基团的量，t（PO ）为PO的添加时间，OHZ为聚醚多元醇的计算OH值，m为1〜10的自然数，基于所添加的亚烷基的总量，聚醚多元醇中的氧乙烯单元的总含量氧化物为5〜90重量％。

6. 发明专利

JP2014162924A Process for preparing polyether polyol 审中-公开
标题翻译：制备聚醚多元醇的方法
公开(公告)号：JP2014162924A
公开(公告)日：2014-09-08
申请号：JP2014031291
申请日：2014-02-21
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , EICHMANN MARKUS
IPC分类号： C08G65/26 , C08G65/10
CPC分类号： C08G65/34 , C08G65/00 , C08G65/2609 , C08G65/30
摘要： PROBLEM TO BE SOLVED: To provide a process for preparing polyether polyol based on a starter which is a solid at room temperature.SOLUTION: There is provided the process for preparing polyether polyol having n Eblocks each having at least 75 wt.% of an oxyethylene unit and m Ablocks different from the Eblock, where n and m are natural numbers of 1 to 10. The process for preparing polyether polyol comprises reacting an active hydrogen-containing starter having a melting point of 40°C or more with ethylene oxide and further alkylene oxide compound by adding a catalyst. The reaction with ethylene oxide is conducted during addition of Eblocks under a condition represented by the following inequality, where Tis an average reaction temperature, x(cat) is the amount of a catalyst, tis addition time of ethylene oxide, x(EO) is the amount of ethylene oxide, and n is a natural number of 1 to 10, and the total content of the oxyethylene unit in the polyether polyol based on the total amount of the added all alkylene oxide is 5 to 85 wt.%.
摘要翻译：要解决的问题：提供一种制备基于在室温下为固体的起动剂的聚醚多元醇的方法。解决方案：提供了制备具有n个Eblock的聚醚多元醇的方法，每个Eblock具有至少75重量％的氧化乙烯单元和m与Eblock不同的嵌合体，其中n和m为1至10的自然数。制备聚醚多元醇的方法包括使具有40℃或更高的熔点的活性氢起始物与环氧乙烷反应，环氧烷化合物。在由以下不等式表示的条件下，在加入Eblock期间进行与环氧乙烷的反应，其中T是平均反应温度，x（cat）是催化剂的量，环氧乙烷的加成时间，x（EO）为环氧乙烷的量，n为1〜10的自然数，聚醚多元醇中的氧化乙烯单元的总含量相对于所添加的全部氧化烯的总量为5〜85重量％。

7. 发明专利

JP2010095721A Method for producing polyetherester polyol 有权
标题翻译：生产聚醚多元醇的方法
公开(公告)号：JP2010095721A
公开(公告)日：2010-04-30
申请号：JP2009238002
申请日：2009-10-15
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , ALBERS REINHARD , OTTO FRANK
IPC分类号： C08G65/28 , C08G18/48 , C08G65/332
CPC分类号： C08G18/4825 , C08G18/1808 , C08G18/1816 , C08G18/1825 , C08G18/5021 , C08G65/2615 , C08G65/2696 , C08G2101/00 , C08L71/02 , C08L2666/22
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a polyetherester polyol starting from a fatty acid ester and a starter compound having a Zerewitinoff-active hydrogen atom. SOLUTION: The method for producing a first polyetherester polyol includes making the starter compound (a) having a Zerewitinoff-active hydrogen atom react with at least one alkylene oxide (b) in the presence of at least one amine (c) selected from a group composed of a tertiary amine and optionally a substituted imidazole, and in the presence of at least one fatty acid ester (d), wherein (d) is added before, during, or after measuring and adding (b), and a second polyetherester polyol (e) is mixed with the components (a), (c), and optionally (d) with an amount of 3.0-20.0 wt.% with respect to the sum total weight of components (a), (b), (c), (d) and (e), before measuring and adding (b). COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：待解决的问题：提供一种由脂肪酸酯起始的聚醚酯多元醇和具有泽维辛酯 - 活性氢原子的起始化合物的方法。解决方案：制备第一聚醚酯多元醇的方法包括在至少一种选择的胺（c）的存在下，制备具有泽维辛酯 - 活性氢原子的起始化合物（a）与至少一种烯化氧（b）反应从由叔胺和任选取代的咪唑组成的组中，并且在至少一种脂肪酸酯（d）的存在下，其中（d）在测量之前，期间或之后加入（b），和第二聚醚酯多元醇（e）与组分（a），（b）的总和重量相对于组分（a），（c）和任选地（d）与3.0-20.0重量％的量混合，，（c），（d）和（e），在测量和添加（b）之前。版权所有（C）2010，JPO＆INPIT

8. 发明专利

JP2009046675A Method for producing polyol 有权
标题翻译：生产聚醇的方法
公开(公告)号：JP2009046675A
公开(公告)日：2009-03-05
申请号：JP2008209162
申请日：2008-08-15
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , WERNER ARNULF , EICHMANN MARKUS
IPC分类号： C08G65/30 , C08G18/48
CPC分类号： C08G65/2609 , C08G65/2648 , C08G65/30 , C08G65/32
摘要： PROBLEM TO BE SOLVED: To provide an inexpensive finishing method for an ethylene oxide-containing polyol produced using an alkali metal- or alkaline earth metal-hydroxide catalyst or the like, which shows no disadvantages of the conventional art.
SOLUTION: The method for producing a polyol comprises steps of (1) carrying out basic catalyst addition of (a) an alkylene oxide to (b) a Zerewitinoff-active hydrogen atom-containing multifunctional starter compound in the presence of (c) a catalyst based on an alkali metal hydroxide or alkaline earth metal hydroxide or the like; and (2) neutralizing the alkaline polymerization activity center of a coarse alkylene oxide addition product by adding sulfuric acid.
COPYRIGHT: (C)2009,JPO&INPIT
摘要翻译：要解决的问题：为了提供使用碱金属或碱土金属氢氧化物催化剂等制备的含环氧乙烷的多元醇的廉价的整理方法，其显示出传统技术的缺点。解决方案：多元醇的制造方法包括以下步骤：（a）在（c）存在下，（a）烯化氧与（b）含有Zerewitinoff活性氢原子的多官能起始化合物进行碱性催化剂的加成反应）基于碱金属氢氧化物或碱土金属氢氧化物等的催化剂; 和（2）通过加入硫酸中和粗大的氧化烯加成产物的碱性聚合活性中心。版权所有（C）2009，JPO＆INPIT

9. 发明专利

JP2008121015A Method for manufacturing polyether-ester polyol 有权
标题翻译：制备聚酯多元醇的方法
公开(公告)号：JP2008121015A
公开(公告)日：2008-05-29
申请号：JP2007294171
申请日：2007-11-13
申请人： Bayer Materialscience Ag , バイエル・マテリアルサイエンス・アクチェンゲゼルシャフトBayer MaterialScience AG
发明人： LORENZ KLAUS , ALBERS REINHARD , OTTO FRANK , LEYRER ULRICH , WARDIUS DON S , HEADLEY KEITH J
IPC分类号： C08G65/26 , C08G18/42
CPC分类号： C08G18/4891 , C08G18/14 , C08G18/4018 , C08G18/4244 , C08G18/4804 , C08G18/482 , C08G18/5021 , C08G18/5033 , C08G63/66 , C08G63/87 , C08G65/2606 , C08G65/2609 , C08G65/2612 , C08G65/2621 , C08G65/2624 , C08G65/2627 , C08G65/2672 , C08G65/2687 , C08G65/3322 , C08G2101/0025 , C08G2101/005 , C08G2101/0083
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a polyol based on a fatty acid ester and a starter compound having Zerewitinoff-active hydrogen atoms and the use thereof for manufacturing a polyurethane material. SOLUTION: The method for manufacturing the polyether-ester polyol is characterized in that the polyether-ester polyol is obtained by reacting the starter compound having the Zerewitinoff-active hydrogen atoms according to the basic catalyst reaction with an alkylene oxide in the presence of a fatty acid ester. The polyether-ester polyol is used for manufacturing the polyurethane. COPYRIGHT: (C)2008,JPO&INPIT

10. 发明申请

WO2010127823A2 METHOD FOR PRODUCING POLYESTER POLYOLS HAVING SECONDARY OH TERMINAL GROUPS 审中-公开
标题翻译：用于生产SECONDARY聚酯多元醇与OH端基
公开(公告)号：WO2010127823A2
公开(公告)日：2010-11-11
申请号：PCT/EP2010002697
申请日：2010-05-04
申请人： BAYER MATERIALSCIENCE AG , NEFZGER HARTMUT , BAUER ERIKA , HOFMANN JOERG , LORENZ KLAUS , KLESCZEWSKI BERT
发明人： NEFZGER HARTMUT , BAUER ERIKA , HOFMANN JOERG , LORENZ KLAUS , KLESCZEWSKI BERT
CPC分类号： C08G63/914 , C08G18/4261 , C08G63/87
摘要： The invention relates to a method for producing polyester polyols having secondary hydroxyl terminal groups, comprising the step of reacting polyester comprising carboxyl terminal groups with an epoxide of the general formula (1), where R1 stands for an alkyl radical or an aryl radical, and the reaction is performed in the presence of a catalyst comprising at least one nitrogen atom per molecule. The method is characterized in that the polyester comprising carboxyl terminal groups has an acid number of = 25 mg KOH/g to = 400 mg KOH/g and a hydroxyl number of = 5 mg KOH/g, and that the polyester comprising carboxyl terminal groups is produced in that = 1.03 mol to = 1.90 mol of carboxyl groups or carboxyl group equivalents of an acid component are added per mol of hydroxyl groups of an alcohol. The polyester polyols comprising secondary hydroxyl terminal groups thus obtained can be used for producing polyurethane polymers.
摘要翻译：本发明涉及一种用于生产具有仲羟基端基的聚酯多元醇的方法，其包含含有聚酯一个羧基端基与通式的环氧化物反应的步骤（1）其中R1是烷基或芳基，并且在一个存在下的反应是每分子包含至少一个氮原子进行的催化剂。该方法的特征在于，所述羧基末端基团，其包括聚酯已到= 400毫克KOH /克的= 25毫克KOH / g的酸值和= 5毫克KOH /克，并且羧基末端基团的羟基值是制备包含聚酯通过用于= 1.90摩尔羧基或Carboxylgruppenäquivalente每醇= 1.03摩尔的羟基摩尔酸组分。包括聚酯多元醇所获得的仲羟基端基可用于聚氨酯聚合物的制备。

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