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1. 发明授权

KR820000739B1 PROCESS FOR PREPARING BENZOTHIAZOLYL SULPEHNIC ACID MORPHOLIDE 失效
公开(公告)号：KR820000739B1
公开(公告)日：1982-05-03
申请号：KR790000846
申请日：1979-03-20
申请人： BAYER AG
发明人： WICKE M , HULLSTRUNG D , SCHERHAG B
IPC分类号： C07D413/12
摘要： Title compds., useful as vulcanization accelerators, was prepd. by the reaction of morpholine with 1,2-benzothiazolyl disulfite, mercaptobenzothiazole and their sodium salt in the presence of oxidizing agent. Thus,27.5 kg 2,6-dimethylmorpholide was prepd. from 138 kg compd. of 20 % 2-benzothiazolylsulfenic acid-2,6-dimethylmorpholide, 20 % 2,6-dimethylmorpholine, 7.5 % NaCl, 51 % H2O and 1.5 % by-product. The product was cooled by the scraping roller to give title compd.

2. 发明专利

AU517673B2 2-BENZOTHIAZOLYL SULPHENIC ACID MORPHOLIDE 未知
公开(公告)号：AU517673B2
公开(公告)日：1981-08-20
申请号：AU4593079
申请日：1979-04-11
申请人： BAYER AG
发明人： HULLSTRIIG D , WICKE M , SCHERHAG B
IPC分类号： C07D277/00 , C07D277/80 , C07D417/12

3. 发明专利

BR7902255A 未知
公开(公告)号：BR7902255A
公开(公告)日：1979-12-11
申请号：BR7902255
申请日：1979-04-11
申请人： BAYER AG
发明人： SCHERHAG B , WICKE M , HULLSTRUNG D
IPC分类号： C07D277/00 , C07D277/80 , C07D417/12 , C07D413/12

4. 发明专利

ZA755230B CONTINUOUS SOLVENT-FREE POLYMERISATION OF VINYL DERIVATIVES 未知
公开(公告)号：ZA755230B
公开(公告)日：1976-07-28
申请号：ZA755230
申请日：1975-08-15
申请人： BAYER AG
发明人： MUELLER E , WICKE M
IPC分类号： C08F2/00 , C08F2/02 , C08F12/00 , C08F12/08 , C08F212/00 , C08F220/00 , C08F220/10 , C08F
摘要： A process for the polymerization of aromatic vinyl compounds and their copolymerization with alkyl esters or nitriles of acrylic and/or methacrylic acid, wherein 1. IN A FIRST STAGE, THE MONOMER OR MONOMERS IS OR ARE CONTINUOUSLY INTRODUCED AT EXCESS PRESSURE INTO A FIRST REACTION ZONE AND POLYMERIZED THERE TO A DEGREE OF CONVERSION OF 5 - 40% BY WEIGHT AT A TEMPERATURE OF FROM 80 DEG TO 170 DEG C; 2. in a second stage, the reaction mixture is conducted at constant pressure into a second reaction zone designed for conducting highly viscous melts, the mixture flowing through this reaction zone at a rate which is 1.1 to 5 times the intrinsic rate, and polymerized there to a degree of conversion of 40 to 95% at temperatures of from 120 DEG to 250 DEG C, the excess pressure in the first and second stage being chosen so that the monomer or monomers is or are liquid, and the polymer is continuously removed from this zone with release of the pressure; and 3. IN A THIRD STAGE, UNREACTED MONOMER IS REMOVED BY EVAPORATION, THE PRESSURE BEING CHOSEN SO THAT THE MONOMER OR MONOMERS IS OR ARE EVAPORATED, AND THE POLYMER IS DISCHARGED AS A MELT.

5. 发明专利

ZA7505230B CONTINUOUS SOLVENT-FREE POLYMERISATION OF VINYL DERIVATIVES 未知
公开(公告)号：ZA7505230B
公开(公告)日：1976-07-28
申请号：ZA7505230
申请日：1975-08-15
申请人： BAYER AG
发明人： MUELLER E , WICKE M
IPC分类号： C08F2/00 , C08F2/02 , C08F12/00 , C08F12/08 , C08F212/00 , C08F220/00 , C08F220/10 , C08F
CPC分类号： C08F12/08 , C08F2/02

6. 发明专利

ZA791766B PROCESS FOR THE PREPARATION OF BENZOTHIAZOLYL SULPHENIC ACID MORPHOLIDE 未知
公开(公告)号：ZA791766B
公开(公告)日：1980-05-28
申请号：ZA791766
申请日：1979-04-12
申请人： BAYER AG
发明人： WICKE M , SCHERHAG B , HUELLSTRUNG D
IPC分类号： C07D277/00 , C07D277/80 , C07D417/12 , C07D413/12 , B01D

7. 发明专利

BR7505238A 未知
公开(公告)号：BR7505238A
公开(公告)日：1976-08-03
申请号：BR7505238
申请日：1975-08-15
申请人： BAYER AG
发明人： MUELLER E , WICKE M
IPC分类号： C08F2/00 , C08F2/02 , C08F12/00 , C08F12/08 , C08F212/00 , C08F220/00 , C08F220/10
摘要： A process for the polymerization of aromatic vinyl compounds and their copolymerization with alkyl esters or nitriles of acrylic and/or methacrylic acid, wherein 1. IN A FIRST STAGE, THE MONOMER OR MONOMERS IS OR ARE CONTINUOUSLY INTRODUCED AT EXCESS PRESSURE INTO A FIRST REACTION ZONE AND POLYMERIZED THERE TO A DEGREE OF CONVERSION OF 5 - 40% BY WEIGHT AT A TEMPERATURE OF FROM 80 DEG TO 170 DEG C; 2. in a second stage, the reaction mixture is conducted at constant pressure into a second reaction zone designed for conducting highly viscous melts, the mixture flowing through this reaction zone at a rate which is 1.1 to 5 times the intrinsic rate, and polymerized there to a degree of conversion of 40 to 95% at temperatures of from 120 DEG to 250 DEG C, the excess pressure in the first and second stage being chosen so that the monomer or monomers is or are liquid, and the polymer is continuously removed from this zone with release of the pressure; and 3. IN A THIRD STAGE, UNREACTED MONOMER IS REMOVED BY EVAPORATION, THE PRESSURE BEING CHOSEN SO THAT THE MONOMER OR MONOMERS IS OR ARE EVAPORATED, AND THE POLYMER IS DISCHARGED AS A MELT.

8. 发明专利

ZA7901766B PROCESS FOR THE PREPARATION OF BENZOTHIAZOLYL SULPHENIC ACID MORPHOLIDE 未知
公开(公告)号：ZA7901766B
公开(公告)日：1980-05-28
申请号：ZA7901766
申请日：1979-04-12
申请人： BAYER AG
发明人： WICKE M , SCHERHAG B , HUELLSTRUNG D
IPC分类号： C07D277/00 , C07D277/80 , C07D417/12 , C07D413/12 , B01D
CPC分类号： C07D277/80

9. 发明专利

IN142506B CONTINUOUS SOLVENT-FREE POLYMERISATION OF VINYL DERIVATIVES 未知
公开(公告)号：IN142506B
公开(公告)日：1977-07-23
申请号：IN1392CA1975
申请日：1975-07-16
申请人： BAYER AG
发明人： MULLER E-W , WICKE M
IPC分类号： C08F2/00 , C08F2/02 , C08F12/00 , C08F12/08 , C08F212/00 , C08F220/00 , C08F220/10 , C08F3/54 , C08F3/56
摘要： A process for the polymerization of aromatic vinyl compounds and their copolymerization with alkyl esters or nitriles of acrylic and/or methacrylic acid, wherein 1. IN A FIRST STAGE, THE MONOMER OR MONOMERS IS OR ARE CONTINUOUSLY INTRODUCED AT EXCESS PRESSURE INTO A FIRST REACTION ZONE AND POLYMERIZED THERE TO A DEGREE OF CONVERSION OF 5 - 40% BY WEIGHT AT A TEMPERATURE OF FROM 80 DEG TO 170 DEG C; 2. in a second stage, the reaction mixture is conducted at constant pressure into a second reaction zone designed for conducting highly viscous melts, the mixture flowing through this reaction zone at a rate which is 1.1 to 5 times the intrinsic rate, and polymerized there to a degree of conversion of 40 to 95% at temperatures of from 120 DEG to 250 DEG C, the excess pressure in the first and second stage being chosen so that the monomer or monomers is or are liquid, and the polymer is continuously removed from this zone with release of the pressure; and 3. IN A THIRD STAGE, UNREACTED MONOMER IS REMOVED BY EVAPORATION, THE PRESSURE BEING CHOSEN SO THAT THE MONOMER OR MONOMERS IS OR ARE EVAPORATED, AND THE POLYMER IS DISCHARGED AS A MELT.

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