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1. 发明申请

WO2008151269A2 PALLADIUM CATALYZED HYDROGENATION OF BIO-OILS AND ORGANIC COMPOUNDS 审中-公开
标题翻译：生物油和有机化合物的钯催化氢化
公开(公告)号：WO2008151269A2
公开(公告)日：2008-12-11
申请号：PCT/US2008/065884
申请日：2008-06-05
申请人： BATTELLE MEMORIAL INSTITUTE , ELLIOTT, Douglas, C. , HU, Jianli , HART, Todd, R. , NEUENSCHWANDER, Gary, G.
发明人： ELLIOTT, Douglas, C. , HU, Jianli , HART, Todd, R. , NEUENSCHWANDER, Gary, G.
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

2. 发明申请

WO2007075428A3 ALCOHOL SYNTHESIS FROM CO OR CO2 审中-公开
公开(公告)号：WO2007075428A3
公开(公告)日：2007-07-05
申请号：PCT/US2006/047935
申请日：2006-12-16
申请人： BATTELLE MEMORIAL INSTITUTE , HU, Jianli , WANG, Yong , DAGLE, Robert, A. , CAO, Chunshe , ELLIOTT, Douglas, C. , STEVENS, Don, J. , WHITE, James, F. , HOLLADAY, Jamelyn, D.
发明人： HU, Jianli , WANG, Yong , DAGLE, Robert, A. , CAO, Chunshe , ELLIOTT, Douglas, C. , STEVENS, Don, J. , WHITE, James, F. , HOLLADAY, Jamelyn, D.
IPC分类号： C07C29/151 , C07C29/157 , C07C29/32 , B01J19/00 , C07C1/24
摘要： Methods for producing alcohols from CO or CO 2 and H 2 utilizing a palladium- zinc on alumina catalyst are described. Methods of synthesizing alcohols over various catalysts in microchannels are also described. Ethanol, higher alcohols, and other C 2+ oxygenates can produced utilizing Rh-Mn or a Fisher-Tropsch catalyst.

3. 发明申请

WO2008054804A2 HYDROXYMETHYL FURFURAL OXIDATION METHODS 审中-公开
标题翻译：羟丙基氧化氧化方法
公开(公告)号：WO2008054804A2
公开(公告)日：2008-05-08
申请号：PCT/US2007/023063
申请日：2007-10-31
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA, Michael, A. , HALLEN, Richard, T. , HU, Jianli , WHITE, James, F. , GARY, Michel, J.
发明人： LILGA, Michael, A. , HALLEN, Richard, T. , HU, Jianli , WHITE, James, F. , GARY, Michel, J.
IPC分类号： C07D307/44 , C07D307/48 , B01J23/00
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O 2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50°C to about 200°C A method of producing an oxidation catalyst where ZrO 2 is provided and is calcined. The ZrO 2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O 2 .
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O 2 2中的至少一个提供到反应器中。使起始材料与载体材料上的Pt催化剂接触，在载体材料上进行接触，反应器温度为约50℃至约200℃的制备氧化催化剂的方法，其中ZrO 2 并被煅烧。将ZrO 2 2与乙酰丙酮酸铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2 2的流下被钝化。

4. 发明申请

WO2007075432A3 METHODS OF PRODUCING HYDROGEN VIA THE WATER-GAS SHIFT REACTION OVER A PD-ZN CATALYST 审中-公开
公开(公告)号：WO2007075432A3
公开(公告)日：2007-07-05
申请号：PCT/US2006/047939
申请日：2006-12-14
申请人： BATTELLE MEMORIAL INSTITUTE , DAGLE, Robert, A. , WANG, Yong , HU, Jianli
发明人： DAGLE, Robert, A. , WANG, Yong , HU, Jianli
IPC分类号： C01B3/16 , B01J23/60
摘要： Methods for producing hydrogen via the water-gas shift reaction utilizing a palladium-zinc on alumina catalyst are described.

5. 发明申请

WO2005030390A1 ALCOHOL STEAM REFORMING CATALYSTS AND METHODS OF ALCOHOL STEAM REFORMING 审中-公开
标题翻译：醇醇蒸汽重整催化剂及醇酒蒸汽重整方法
公开(公告)号：WO2005030390A1
公开(公告)日：2005-04-07
申请号：PCT/US2004/013853
申请日：2004-05-03
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY, Jamelyn, D. , WANG, Yong , HU, Jianli , CHIN, Ya-Huei , DAGLE, Robert, A. , XIA, Guanguang , BAKER, Eddie, G. , PALO, Daniel, R. , PHELPS, Max, R. , JUNG, Heon
发明人： HOLLADAY, Jamelyn, D. , WANG, Yong , HU, Jianli , CHIN, Ya-Huei , DAGLE, Robert, A. , XIA, Guanguang , BAKER, Eddie, G. , PALO, Daniel, R. , PHELPS, Max, R. , JUNG, Heon
IPC分类号： B01J23/60
CPC分类号： F23C13/00 , B01J19/0093 , B01J21/04 , B01J21/066 , B01J23/60 , B01J23/63 , B01J37/03 , B01J2219/00783 , B01J2219/00835 , B01J2219/00862 , B01J2219/00867 , B01J2219/00873 , B01J2219/00891 , C01B3/326 , C01B2203/0233 , C01B2203/04 , C01B2203/066 , C01B2203/0816 , C01B2203/0822 , C01B2203/0827 , C01B2203/1064 , C01B2203/1076 , C01B2203/1223 , F23C2900/03001 , Y02P20/128 , Y02P20/52
摘要： The present invention provides steam reforming catalyst compositions containing Pd and Zn, and methods of steam reforming alcohols over a catalyst. Surprisingly superior results and properties of the present invention, including low temperature activity and/or low carbon monoxide output, are also described. Methods of making a steam reforming catalyst are also provided.
摘要翻译：本发明提供含有Pd和Zn的蒸汽重整催化剂组合物，以及在催化剂上蒸汽重整醇的方法。还描述了包括低温活性和/或低一氧化碳输出的本发明的令人惊奇的优异结果和性质。还提供了制备蒸汽重整催化剂的方法。

6. 发明申请

WO2007089527A2 METHOD OF FORMING A DIANHYDROSUGAR ALCOHOL 审中-公开
标题翻译：形成二氢化AR醇的方法
公开(公告)号：WO2007089527A2
公开(公告)日：2007-08-09
申请号：PCT/US2007/001996
申请日：2007-01-25
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY, Johnathan , WERPY, Todd, A. , HU, Jianli , WANG, Yong , ZHANG, Xinjie
发明人： HOLLADAY, Johnathan , WERPY, Todd, A. , HU, Jianli , WANG, Yong , ZHANG, Xinjie
IPC分类号： C07D493/04
CPC分类号： C07D307/20 , C07D493/04 , Y02P20/127
摘要： The invention includes methods of producing dianhydrosugars. A polyol is reacted in the presence of a first catalyst to form a monocyclic sugar. The monocyclic sugar is transferred to a second reactor where it is converted to a dianhydrosugar alcohol in the presence of a second catalyst. The invention includes a process of forming isosorbide. An initial reaction is conducted at a first temperature in the presence of a solid acid catalyst. The initial reaction involves reacting sorbitol to produce 1 ,4-sorbitan, 3,6-sorbitan, 2,5-mannitan and 2,5-iditan. Utilizing a second temperature, the 1 ,4-sorbitan and 3,6-sorbitan are converted to isosorbide. The invention includes a method of purifying isosorbide from a mixture containing isosorbide and at least one additional component. A first distillation removes a first portion of the isosorbide from the mixture. A second distillation is then conducted at a higher temperature to remove a second portion of isosorbide from the mixture.
摘要翻译：本发明包括生产二脱水甘油糖的方法。多元醇在第一催化剂存在下反应形成单环糖。将单环糖转移到第二反应器中，在第二反应器中，在第二催化剂的存在下将其转化为二脱水甘油醇。本发明包括形成异山梨醇的方法。在固体酸催化剂存在下，在第一温度下进行初始反应。初始反应包括使山梨糖醇反应生成1,4-脱水山梨糖醇，3,6-脱水山梨糖醇，2,5-甘露聚糖和2,5-己烷。使用第二温度，将1,4-脱水山梨醇和3,6-脱水山梨醇转化为异山梨醇。本发明包括从含有异山梨醇和至少一种另外的组分的混合物中纯化异山梨醇的方法。第一蒸馏从混合物中除去第一部分的异山梨醇。然后在较高温度下进行第二次蒸馏以从混合物中除去第二部分的异山梨醇。

7. 发明申请

WO2007089510A2 METHODS FOR DEHYDRATION OF SUGARS 审中-公开
标题翻译：蔗糖脱水方法
公开(公告)号：WO2007089510A2
公开(公告)日：2007-08-09
申请号：PCT/US2007/001945
申请日：2007-01-24
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY, Johnathan, E. , HU, Jianli , ZHANG, Xinjie , WANG, Yong
发明人： HOLLADAY, Johnathan, E. , HU, Jianli , ZHANG, Xinjie , WANG, Yong
IPC分类号： C07D493/04 , C08G63/672 , C07H1/00
CPC分类号： C07D493/04
摘要： The invention includes a method of dehydration of a sugar using a dehydration catalyst and a co-catalyst within a reactor. A sugar is introduced and H 2 is flowed through the reactor at a pressure of less than or equal to about 300 psig to convert at least some of the sugar into an anhydrosugar product. The invention includes a process for producing isosorbide. A starting material comprising sorbitol is flowed into a reactor. H 2 is counter flowed through the reactor. The starting material is exposed to a catalyst in the presence of a co- catalyst which comprises at least one metal. The exposing is conducted at a hydrogen pressure of less than or equal to 300 psig within the reactor and the hydrogen removes at least some of any water present during the exposing and inhibits formation of colored byproducts.
摘要翻译：本发明包括使用反应器内的脱水催化剂和助催化剂使糖脱水的方法。引入糖并且H 2 O 2以小于或等于约300psig的压力流过反应器，以将至少一些糖转化为脱水糖产物。本发明包括一种生产异山梨醇的方法。将含有山梨糖醇的原料流入反应器。 H 2反向流过反应器。原料在包含至少一种金属的助催化剂存在下暴露于催化剂。暴露在反应器内以小于或等于300psig的氢气压力进行，并且氢去除暴露期间存在的任何水中的至少一些并且抑制着色副产物的形成。

8. 发明申请

WO2007089526A1 METHOD OF PERFORMING SUGAR DEHYDRATION AND CATALYST TREATMENT 审中-公开
标题翻译：执行糖脱水和催化处理的方法
公开(公告)号：WO2007089526A1
公开(公告)日：2007-08-09
申请号：PCT/US2007/001995
申请日：2007-01-25
申请人： BATTELLE MEMORIAL INSTITUTE , HU, Jianli , HOLLADAY, Johnathan, E. , ZHANG, Xinjie , WANG, Yong
发明人： HU, Jianli , HOLLADAY, Johnathan, E. , ZHANG, Xinjie , WANG, Yong
IPC分类号： C07H1/00
CPC分类号： C07H1/00
摘要： The invention includes a method of treating a solid acid catalyst. After exposing the catalyst to a mixture containing a sugar alcohol, the catalyst is washed with an organic solvent and is then exposed to a second reaction mixture. The invention includes a process for production of anhydrosugar alcohol. A solid acid catalyst is provided to convert sugar alcohol in a first sample to an anhydrosugar alcohol. The catalyst is then washed with an organic solvent and is subsequently utilized to expose a second sample. The invention includes a method for selective production of an anhydrosugar. A solid acid catalyst is provided within a reactor and anhydrosugar alcohol is formed by flowing a starting sugar alcohol into the reactor. The acid catalyst is then exposed to an organic solvent which allows a greater amount of additional anhydrosugar to be produced than would occur without exposing the acid catalyst to the organic solvent.
摘要翻译：本发明包括一种处理固体酸催化剂的方法。在将催化剂暴露于含有糖醇的混合物之后，将催化剂用有机溶剂洗涤，然后暴露于第二反应混合物。本发明包括生产脱水葡萄糖醇的方法。提供固体酸催化剂以将第一样品中的糖醇转化成脱水葡萄糖醇。然后将催化剂用有机溶剂洗涤，随后用于暴露第二个样品。本发明包括选择性生产脱水糖的方法。在反应器内提供固体酸催化剂，并通过将起始糖醇流入反应器而形成脱水葡萄糖醇。然后将酸催化剂暴露于有机溶剂，其允许比不会将酸催化剂暴露于有机溶剂的情况下产生更多量的额外的脱水糖。

9. 发明申请

WO2007089524A2 TWO-STAGE DEHYDRATION OF SUGARS 审中-公开
标题翻译：糖两步脱水
公开(公告)号：WO2007089524A2
公开(公告)日：2007-08-09
申请号：PCT/US2007/001993
申请日：2007-01-25
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY, Johnathan , HU, Jianli , WANG, Yong , WERPY, Todd, A.
发明人： HOLLADAY, Johnathan , HU, Jianli , WANG, Yong , WERPY, Todd, A.
CPC分类号： C07D493/04
摘要： The invention includes methods for producing dianhydrosugar alcohol by providing an acid catalyst within a reactor and passing a starting material through the reactor at a first temperature. At least a portion of the staring material is converted to a monoanhydrosugar isomer during the passing through the column. The monoanhydrosugar is subjected to a second temperature which is greater than the first to produce a dianhydrosugar. The invention includes a method of producing isosorbide. An initial feed stream containing sorbitol is fed into a continuous reactor containing an acid catalyst at a temperature of less than 120°C. The residence time for the reactor is less than or equal to about 30 minutes. Sorbitol converted to 1 ,4-sorbitan in the continuous reactor is subsequently provided to a second reactor and is dehydrated at a temperature of at least 1200C to produce isosorbide.
摘要翻译：本发明包括通过在反应器内提供酸催化剂并使原料在第一温度下通过反应器来生产二脱水甘油的方法。在通过色谱柱期间，至少一部分起始物质被转化为单一脱氢葡萄糖异构体。单糖酐经受大于第一温度的第二温度以产生二脱水糖。本发明包括一种生产异山梨醇的方法。含有山梨糖醇的初始进料流在小于120℃的温度下进料到含有酸催化剂的连续反应器中。反应器的停留时间小于或等于约30分钟。随后将连续反应器中的山梨醇转化为1,4-脱水山梨醇至第二反应器，并在至少120℃的温度下脱水以制备异山梨醇。

10. 发明申请

WO2020055385A1 METHODS AND COMPOSITIONS FOR MICROWAVE CATALYTIC AMMONIA SYNTHESIS 审中-公开
公开(公告)号：WO2020055385A1
公开(公告)日：2020-03-19
申请号：PCT/US2018/050438
申请日：2018-09-11
申请人： WEST VIRGINIA UNIVERSITY , BATTELLE MEMORIAL INSTITUTE , FLORIDA STATE UNIVERSITY RESEARCH FOUNDATION, INC. , UNITED STATES DEPARTMENT OF ENERGY
发明人： ABDEL-SAYED, Victor , BEARDEN, Mark D. , DAGLE, Robert A. , HU, Jianli , SHEKHAWAT, Dushyant , SPENCER, Michael , STIEGMAN, Al , TIAN, Hanjing , WILDFIRE, Christina
IPC分类号： C01C1/04
摘要： In one aspect, the disclosure relates to relates to heterogeneous catalysts useful for the synthesis of ammonia under microwave irradiation, processes for preparing the disclosed heterogeneous catalysts, and processes for synthesizing ammonia using the heterogeneous catalysts with microwave irradiation. In various aspects, the disclosed heterogeneous catalysts comprise: a metal selected from Group 7, Group 8, Group 9, Group 10, Group 11, or combinations thereof; a metal oxide support; and optionally a promoter material. This abstract is intended as a scanning tool for purposes of searching in the particular art and is not intended to be limiting of the present disclosure.

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