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1. 发明申请

WO2010136551A2 CATALYST AND METHOD FOR PARTIALLY OXIDIZING HYDROCARBONS 审中-公开
标题翻译：催化剂和方法部分氧化烃
公开(公告)号：WO2010136551A2
公开(公告)日：2010-12-02
申请号：PCT/EP2010057375
申请日：2010-05-28
申请人： BASF SE , KARPOV ANDREY , HIBST HARTMUT , DEISSLER CHRISTINE , DOBNER CORNELIA KATHARINA , ROSOWSKI FRANK , BREM NADINE , SCHUNK STEPHAN
发明人： KARPOV ANDREY , HIBST HARTMUT , DEISSLER CHRISTINE , DOBNER CORNELIA KATHARINA , ROSOWSKI FRANK , BREM NADINE , SCHUNK STEPHAN
IPC分类号： C07C51/265
CPC分类号： B01J23/686 , B01J23/002 , B01J23/687 , B01J23/8993 , B01J27/199 , B01J37/0045 , B01J2523/00 , C07C51/265 , C07C63/16 , C07C63/26 , B01J2523/18 , B01J2523/305 , B01J2523/55 , B01J2523/68 , B01J2523/51 , B01J2523/3712 , B01J2523/53 , B01J2523/54 , B01J2523/17 , B01J2523/69 , B01J2523/15 , B01J2523/56 , B01J2523/842
摘要： The invention relates to a catalyst for partially oxidizing hydrocarbons in the gas phase, containing a multi-metal oxide of the general formula (I), AgaMObVcMdOe * f H2O (I), wherein M stands for at least one element selected from among Li, Na, K, Rb, Cs, Be, Mg, Ca, Sr, Ba, B, AI, Ga, In, Si, Sn, Pb, P, Sb, Bi, Y, Ti, Zr, Hf, V, Nb, Ta, Cr, W, Mn, Re, Fe, Ru, Os, Co, Rh, Ir, Ni, Pd, Pt, Cu, Au, Zn, Cd, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, and U, a has a value of 0.5 to 1.5, b has a value of 0.5 to 1.5, c has a value of 0.5 to 1.5, a+b+c has the value 3, d has a value of less than 1, e means a number that is determined by the valence and frequency of the elements other than oxygen in the formula (I), f has a value of 0 to 20, which multi-metal oxide exists in a crystal structure, the X-ray powder diffractogram of which is characterized by diffraction reflections at a minimum of 5 lattice distances selected from among d = 4.53, 3.38, 3.32, 3.23, 2.88, 2.57, 2.39, 2.26, 1.83, 1.77 Å (± 0.04 Å).
摘要翻译：一种用于烃的气相部分氧化催化剂包括通式（I）的多金属氧化物，AgaMObVcMdOe * F H 2 O（I）其中M是其中锂，钠，钾，铷，铯，铍，镁，钙的至少一个，锶，钡，硼，铝，镓，铟，硅，锡，铅，磷，锑，铋，Y，钛，锆，铪，钒，铌，钽，铬，钨，锰，RE，铁，钌，锇，钴，铑，铱，镍，钯，铂，铜，金，锌，镉，镧，铈，镨，钕，钐，铕，钆，铽，镝，钬，铒，铥，镱，路， U被选择的元素，一个具有0.5至1.5的值; b为0.5〜1.5的值，c具有从0.5至1.5，A + b + C的值是3，D具有小于1的值，例如确定由其中，F为0至20的值，式（I）中氧以外的元素的化合价和频率定义的一个数，在的晶体结构存在，其粉末X至少为5，在D的特征在于衍射峰= 4.53，3.38，3.32，3.23，2.88，2.57，2.39，2.26，1， 83，1.77埃（±0.04 A）中的晶面间距。

2. 发明申请

WO2010072723A3 CATALYST AND METHOD FOR PRODUCING MALEIC ANHYDRIDE 审中-公开
标题翻译：催化剂和生产马来酸酐的方法
公开(公告)号：WO2010072723A3
公开(公告)日：2010-09-10
申请号：PCT/EP2009067661
申请日：2009-12-21
申请人： BASF SE , DOBNER CORNELIA KATHARINA , ALTWASSER STEFAN , WILMER HAGEN , ROSOWSKI FRANK
发明人： DOBNER CORNELIA KATHARINA , ALTWASSER STEFAN , WILMER HAGEN , ROSOWSKI FRANK
IPC分类号： B01J27/198 , B01J35/02 , B01J35/10 , C07C51/215
CPC分类号： B01J35/023 , B01J27/198 , B01J35/002 , B01J35/02 , B01J35/026 , B01J35/1038 , B01J35/1042 , B01J37/0009 , B01J37/0018 , C07C51/215 , Y10T428/2975 , C07C57/145
摘要： The invention relates to a catalyst molded body for producing maleic anhydride by gas-phase oxidation of a hydrocarbon having at least four carbon atoms, comprising a catalytically active mass, which contains vanadium, phosphorus, and oxygen. The catalyst molded body comprises a substantially cylindrical body having at least two, preferably four, inner through-bores substantially parallel to the cylinder axis of the body. The catalyst molded body has a large outer surface area, a lower pressure loss, and sufficient mechanical stability.
摘要翻译：用于通过气相氧化具有至少四个碳原子的烃来生产马来酸酐的成型催化剂体包含含有钒，磷和氧的催化活性材料。该催化剂成型体具有基本上圆柱形的本体，该本体具有至少两个，优选四个与本体的圆柱轴线基本上平行的连续的内孔。催化剂成型体具有较大的外表面，较低的压降和足够的机械稳定性。

3. 发明申请

WO2010072721A3 CATALYST MOLDED BODIES AND METHOD FOR PRODUCING MALEIC ACID ANHYDRIDE 审中-公开
标题翻译：催化剂整形体和生产马来酸酐的方法
公开(公告)号：WO2010072721A3
公开(公告)日：2010-10-28
申请号：PCT/EP2009067657
申请日：2009-12-21
申请人： BASF SE , DOBNER CORNELIA KATHARINA , ALTWASSER STEFAN , WILMER HAGEN , ROSOWSKI FRANK
发明人： DOBNER CORNELIA KATHARINA , ALTWASSER STEFAN , WILMER HAGEN , ROSOWSKI FRANK
IPC分类号： B01J27/198 , B01J35/02 , B01J35/10 , C07C51/215
CPC分类号： B01J27/198 , B01J35/002 , B01J35/0026 , B01J35/026 , B01J35/1038 , B01J35/1066 , B01J35/1071 , B01J35/1076 , B01J35/108 , B01J37/0018 , C07C51/215 , C07C57/145
摘要： The catalytically active mass of a catalyst molded body comprises a multi-element oxide containing vanadium and phosphorus. The specific pore volume PV (in ml/g) of the catalyst molded body, the bulk density p of the catalyst molded body (in kg/l), the geometric surface area Ageo (in mm2), and the geometric volume Vgeo (in mm3) of the catalyst molded body satisfy the condition: 0.275 geo/Vgeo. In a method for producing maleic acid anhydride by heterogeneously catalytic gas phase oxidation of a hydrocarbon, the catalyst molded body allows a lower pressure loss and a high yield.
摘要翻译：成形催化剂体的催化活性组合物包含含钒和含磷的多元素氧化物。比孔体积PV（以ml / g）的催化剂成型的，该催化剂成型体的催化剂成型体的体积密度ρ（单位为kg /升），则几何表面积地理（以mm 2）和所述几何体积VGEo（以mm 3）满足条件：0.275地理 / VGEo。在通过催化剂成型体的烃的非均相催化气相氧化制备马来酸酐的方法允许较低的压力损失和较高的产率。

4. 发明申请

WO2012049246A3 METHOD FOR LONG-TERM OPERATION OF A HETEROGENEOUSLY CATALYZED PARTIAL GAS PHASE OXIDATION OF PROPENE TO OBTAIN ACROLEIN 审中-公开
标题翻译：方法长期运行丙烯到丙烯醛的非均相催化部分气相氧化
公开(公告)号：WO2012049246A3
公开(公告)日：2012-06-14
申请号：PCT/EP2011067887
申请日：2011-10-13
申请人： BASF SE , MACHT JOSEF , MUELLER-ENGEL KLAUS JOACHIM , ROSOWSKI FRANK
发明人： MACHT JOSEF , MUELLER-ENGEL KLAUS JOACHIM , ROSOWSKI FRANK
IPC分类号： C07C47/22 , C07C45/35
CPC分类号： C07C45/35 , C07C47/22
摘要： Disclosed is a method for long-term operation of a heterogeneously catalyzed partial gas phase oxidation of propene to obtain acrolein, in which the propene contained in the fed reaction gas mixture is partially oxidized when said gas mixture penetrates the fixed catalyst bed that is accommodated in two spatially successive temperature zones A, B, and in order to prevent the quality of the fixed catalyst bed from deteriorating during long-term operation, the temperature in at least one of the two temperature zones is raised in such a way that the difference TB- TA becomes greater and greater, where TB is the temperature in temperature zone B and TA is the temperature in temperature zone A.
摘要翻译：一种用于丙烯的非均相催化部分气相氧化成丙烯醛，其中部分氧化的通过固定催化剂床，其被容纳在两个空间上连续的温度区A，B传递时该气体混合物中，并且，在长期运转中所含的反应气体输入混合物的丙烯的长期操作方法，作为针对一个测量减少在固定催化剂床的质量，两个温度区中的至少一个的温度提高，以使差TB TA变得越来越大，TB温度区B的温度，和TA是温度区中的温度。

5. 发明申请

WO2007135104A8 PRODUCTION OF PHTHALIC ANHYDRIDE BY GAS PHASE OXIDATION OF O-XYLOL 审中-公开
标题翻译：通过邻二甲苯的气相氧化制备邻苯二甲酸酐
公开(公告)号：WO2007135104A8
公开(公告)日：2008-06-12
申请号：PCT/EP2007054841
申请日：2007-05-18
申请人： BASF SE , MACKEWITZ THOMAS , ROSOWSKI FRANK , TENTEN ANDREAS
发明人： MACKEWITZ THOMAS , ROSOWSKI FRANK , TENTEN ANDREAS
IPC分类号： C07D307/89
CPC分类号： C07D307/89 , C07C51/265 , C07C63/16
摘要： The invention relates to a method for producing phthalic anhydride by catalytic gas phase oxidation of o-xylol. According to said method, a gaseous mixture of o-xylol and an oxygen-containing gas is guided through at least two reaction zones in a main reactor, the temperature of said reaction zones being adjustable independently of each other, and is reacted to give a gaseous intermediate reaction product which contains unreacted o-xylol, phthalic anhydride reaction products with a lower oxidation state and phthalic anhydride, and the intermediate reaction product is introduced into a secondary reactor. The temperature in the reaction zones in the primary reactor is controlled in such a manner that the concentration of the unreacted o-xylol in the intermediate reaction product is at least 0.5% by weight. The method according to the invention allows an increase in total yield of phthalic anhydride without any or without substantial decrease in product quality.
摘要翻译：用于通过邻二甲苯，其中其将通过至少两个反应区，其是独立温度可控地转发所描述的，含有氧的气体邻二甲苯的气体混合物，并在主反应器的催化气相氧化制备邻苯二甲酸酐，于气态中间反应产物的方法反应含有未反应的邻二甲苯，邻苯二甲酸酐欠氧化产品和邻苯二甲酸酐，以及将所述中间反应产物分离成二级反应器，其特征在于，它调节在主反应器中的反应区的温度，即未转化的邻二甲苯中的中间反应产物中的浓度为至少0 ，5重量％（重量）。该方法允许增加邻苯二甲酸酐的总产没有或没有在产品质量上显著恶化。

6. 发明申请

WO2007135102A2 PRODUCTION OF PHTHALIC ANHYDRIDE BY GAS PHASE OXIDATION OF o-XYLOL IN A PRIMARY AND A SECONDARY REACTOR 审中-公开
标题翻译：制备通过邻二甲苯的气相氧化邻苯二甲酸酐IN头部和Nachreaktor
公开(公告)号：WO2007135102A2
公开(公告)日：2007-11-29
申请号：PCT/EP2007054839
申请日：2007-05-18
申请人： BASF AG , MACKEWITZ THOMAS , ROSOWSKI FRANK , TENTEN ANDREAS
发明人： MACKEWITZ THOMAS , ROSOWSKI FRANK , TENTEN ANDREAS
IPC分类号： C07D307/89
CPC分类号： C07D307/89 , C07C51/265 , C07C63/16
摘要： The invention relates to a method for producing phthalic anhydride by catalytic gas phase oxidation of o-xylol. According to said method, a gaseous mixture of o-xylol and an oxygen-containing gas is reacted in a primary reactor to give a gaseous intermediate reaction product which contains unreacted o-xylol, phthalic anhydride reaction products with a lower oxidation state and phthalic anhydride, the reaction heat produced in the primary reactor being at least partially carried off by indirect cooling with a heat exchange medium, and introducing the intermediate reaction product to a secondary reactor. The concentration of the unreacted o-xylol in the intermediate reaction product is at least 1% by weight, and the sum of the concentrations of phthalic anhydride of the lower oxidation state in the intermediate reaction product is at least 0.5% by weight. The method according to the invention allows an increase in total yield of phthalic anhydride without any or without substantial decrease in product quality.
摘要翻译：公开了一种用于由邻二甲苯，其包含邻二甲苯的含氧气体中的主反应器中的气体混合物，并以气态中间反应产物，其包含未转化的邻二甲苯，邻苯二甲酸酐欠氧化产物反应的催化气相氧化制备邻苯二甲酸酐的方法和邻苯二甲酸酐，所述一个至少部分地耗散由间接冷却用载热介质，并导入中间反应产物分离成二级反应器在主反应器的反应热产生的热。未反应的邻二甲苯中的中间反应产物中的浓度为至少1重量％，邻苯二甲酸酐产品欠氧化浓度的在中间反应产物中的总和为至少0.5重量％。该方法允许增加邻苯二甲酸酐的总产没有或没有在产品质量上显著恶化。

7. 发明申请

WO2010009021A2 PROCESS FOR MAKING ETHYLENE OXIDE USING MICROCHANNEL PROCESS TECHNOLOGY 审中-公开
标题翻译：使用微通道工艺制造乙烯氧化物的方法
公开(公告)号：WO2010009021A2
公开(公告)日：2010-01-21
申请号：PCT/US2009050342
申请日：2009-07-13
申请人： VELOCYS INC , MAZANEC TERRY , MAURER TORSTEN , ABDALLAH RADWAN , DESHMUKH SOUMITRA , SILVA LAURA J , ROSOWSKI FRANK
发明人： MAZANEC TERRY , MAURER TORSTEN , ABDALLAH RADWAN , DESHMUKH SOUMITRA , SILVA LAURA J , ROSOWSKI FRANK
IPC分类号： C07D301/10 , C07B41/04 , C07C29/10
CPC分类号： C07D301/10
摘要： This invention relates to a process comprising reacting ethylene and oxygen or a source of oxygen in a process microchannel in the presence of a catalyst to form a product comprising ethylene oxide.
摘要翻译：本发明涉及一种方法，其包括在催化剂存在下在工艺微通道中使乙烯和氧气或氧源反应，形成包含环氧乙烷的产物。

8. 发明申请

WO2007122090A3 METHOD FOR PRODUCTION OF ETHYLENE OXIDE IN A MICROCHANNEL REACTOR 审中-公开
标题翻译：用于在微通道反应器生产乙烯
公开(公告)号：WO2007122090A3
公开(公告)日：2008-02-07
申请号：PCT/EP2007053363
申请日：2007-04-05
申请人： BASF AG , MAEURER TORSTEN , GITTER MARKUS , ROSOWSKI FRANK
发明人： MAEURER TORSTEN , GITTER MARKUS , ROSOWSKI FRANK
IPC分类号： C07D301/10
CPC分类号： C07D301/10 , B01J2219/00781
摘要： Method for production of ethylene oxide in a microchannel reactor, wherein an ethylene-containing material stream and an oxygen- or oxygen-source-containing material stream are fed to the microchannel reactor and the reaction to give ethylene oxide takes place in the catalyst-containing microchannel reactor. Alkyl halides are continuously fed to the microchannel reactor at a concentration of 0.3 to 50 ppm by volume with respect to the total volume stream of all material streams fed to the reactor.
摘要翻译：一种生产在微通道反应器中的环氧乙烷，其中，一个流和含有氧或含氧流的源的乙烯进料，所述微通道反应器中，并在含催化剂的微通道反应器中，转化为环氧乙烷，得到微通道反应器的烷基卤在O的浓度的过程， 3至50ppm，相对于所有的引入到反应器中的总电流体积连续地供给材料流动。

9. 发明申请

WO2005011862A8 CATALYST FOR GAS PHASE OXIDATIONS 审中-公开
标题翻译：催化剂的气相氧化
公开(公告)号：WO2005011862A8
公开(公告)日：2006-11-16
申请号：PCT/EP2004008596
申请日：2004-07-30
申请人： BASF AG , NETO SAMUEL , ZUEHLKE JUERGEN , STORCK SEBASTIAN , ROSOWSKI FRANK
发明人： NETO SAMUEL , ZUEHLKE JUERGEN , STORCK SEBASTIAN , ROSOWSKI FRANK
IPC分类号： B01J31/06 , B01J21/06 , B01J23/22 , B01J27/198 , B01J37/02 , C07C51/215 , C07C51/265
CPC分类号： B01J23/22 , B01J21/063 , B01J23/002 , B01J27/198 , B01J37/0219 , B01J37/0221 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/51 , B01J2523/53 , B01J2523/55
摘要： Disclosed is a catalyst for gas phase oxidations, comprising an inert carrier and a catalytically active material that is applied thereupon and contains transition metal oxides, or a precatalyst. Said (pre)catalyst is obtained by processing the inert carrier with an aqueous suspension or solution of the transition metal oxides or the precursor compounds thereof. The suspension contains a binder dispersion while the binder is a copolymer of an a-olefin and a vinyl-C 2 -C 4 -carboxylate, the vinyl-C 2 -C 4 -carboxylate content of which amounts to at least 62 mole percent.
摘要翻译：公开的是用于在惰性载体的气相氧化催化剂和包含施加于其上的含有催化活性物质5，或预催化剂的过渡金属氧化物。（预）催化剂通过治疗惰性载体获得的，用含水悬浮液或上或它们的前体化合物的溶液，其中所述悬浮液包含粘合剂分散液和粘合剂的过渡金属氧化物是α-烯烃和乙烯基-C _{2 <的共聚物 / SUB> -C _{4 - 羧酸叔丁酯，其乙烯基ç_{2 -C _{4 - 羧酸叔丁酯为至少62摩尔％。}}}}

10. 发明申请

WO2005030380A2 DEVICE FOR THE MIXING, DRYING AND COATING OF POWDERED, GRANULAR OR MOULDED BULK MATERIAL IN A FLUID BED AND METHOD FOR PRODUCTION OF SUPPORTED CATALYSTS WITH SUCH A DEVICE 审中-公开
标题翻译：装置进行搅拌，流化床和工艺干燥和涂敷粉末状，颗粒状或形状BULK生产负载型催化剂使用这种装置
公开(公告)号：WO2005030380A2
公开(公告)日：2005-04-07
申请号：PCT/EP2004010748
申请日：2004-09-24
申请人： BASF AG , NETO SAMUEL , RUMMEL WOLFGANG , STORCK SEBASTIAN , ZUEHLKE JUERGEN , ROSOWSKI FRANK
发明人： NETO SAMUEL , RUMMEL WOLFGANG , STORCK SEBASTIAN , ZUEHLKE JUERGEN , ROSOWSKI FRANK
IPC分类号： B01J2/16 , B01J8/18 , B01J23/00 , B01J23/22 , B01J27/199 , B01J35/02 , B01J37/02 , F26B3/08 , F26B3/092 , B01J
CPC分类号： B01J23/002 , B01J2/16 , B01J23/22 , B01J27/199 , B01J35/023 , B01J37/0219 , B01J37/0221 , B01J37/0232 , B01J2523/00 , F26B3/0926 , B01J2523/15 , B01J2523/47 , B01J2523/51 , B01J2523/53 , B01J2523/55
摘要： The invention relates to a device for the mixing, drying and coating of powdered, granular or moulded bulk material in a fluid bed, in particular, a method for the production of supported catalysts for gas phase oxidations, with a container (10), for holding the bulk goods, whereby a dished recess (17) is provided in a lower region (13) of the container (10), a central tube (27) for the introduction of a gas, whereby the central tube enters in an upper region (12) of the container (10), extending essentially axially downwards into the container (10) and opens out in the recess (17), an essentially annular deflector screen (29), fixed to the central tube (27) in the upper region (12) of the container (10), a guide ring (31), arranged in the lower region (13) of the container (10), which surrounds the central tube (27) over a part of the length thereof essentially concentrically with a separation (L) such that a first passage (34) is formed between the wall of the container (10) at the upper edge of the recess and the lower end (33) of the guide ring (31) and a second outlet (36) is formed between the deflector screen (29) and the upper edge (35) of the guide ring (31) and means for introduction of a fluid into the container (10), such as, for example, nozzles (21). Said device is characterised in that the external wall of the central tube (27) is at least partly provided with a non-stick coating (38). In a preferred embodiment the separation (L) between the wall of the central tube (27) and the wall of the guide ring (27) is greater than the open height (H3) of the first passage (34). The invention further relates to a method for the production of supported catalysts using such a device.
摘要翻译：本发明涉及一种用于一过程混合，干燥和涂层的粉状，粒状或成形松散物料在流化床中，特别是用于气相氧化的负载型催化剂的制备方法，包括容器（10），用于接收散装材料，其中，（在其下部13 ）的容器（10）的具有用于供给气体，其中，所述中心管（在该容器的上部12）（10）进入所述容器中的碗状凹部（17）在前置式所看到的，中心管（27），位于所述一个容器（10）基本上延伸轴向向下并进入凹槽（17）打开时，基本上环形的偏转防护罩（29）在容器（10）的上部区域（12）至所述中心管（27）是固定的，布置成一个在所述容器的下部部分（13）的中心管（27）（10）导向环（31）在其长度的一部分基本上以一定距离（L），以便COLL同心 IBT，在凹部的上边缘（22）的容器（10）的壁和所述导向环（31），第一通路（34）的下端（33）（29）35之间以及Abweisschirrn之间和顶边（）所述导向环（31）的第二通道（36）的形成，以及用于将流体引入所述容器（10），例如喷嘴（21）。本发明的装置的特征在于，所述中心管（27）的外壁至少部分地设置有减少附着的涂层（38）。在一个优选的实施例中，中心管（27）和导向环（27）的所述壁的所述壁之间的距离（L）大于所述第一通道（34）的净高（H3）更大。本发明还涉及一种使用这种装置的负载型催化剂的制备方法。

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