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1. 发明申请

WO2016142228A1 PROCESS FOR MAKING MIXTURES OF ENANTIOMERS, AND MIXTURES OF ENANTIOMERS 审中-公开
标题翻译：制造增效剂混合物的方法和制剂的混合物
公开(公告)号：WO2016142228A1
公开(公告)日：2016-09-15
申请号：PCT/EP2016/054375
申请日：2016-03-02
申请人： BASF SE
发明人： FRANZKE, Constanze , REINOSO GARCIA, Marta , BAUMANN, Robert , GREINDL, Thomas
IPC分类号： C07C229/16 , C07C229/24 , C11D3/33
CPC分类号： C11D3/33 , C07C227/18 , C07C253/00 , C07C253/06 , C07C255/25 , C07C229/16 , C07C229/24
摘要： Process for preparation of a mixture of methyl glycine diacetic acid (MGDA) or its respective mono-, di-, trialkali metal salt or its respective mono-, di- or tri-ammonium salt or mixtures thereof, and glutamic acid diacetic acid (GLDA) or its respective mono-, di-, tri-, or tetra-alkali metal or mono-, di-, tri- or tetra-ammonium salt or mixtures thereof, wherein said process com- prises the steps of: (a) dissolution in water of (a1) alanine in its L- or D-enantiomeric form or its respective monoalkali metal salt or mixtures thereof, and (a2) glutamic acid as L- or D-enantiomer or its respective mono-, or dialkali metal or mixtures thereof, wherein the molar ratio of alanine to glutamic acid is in the range of from1:9 to 9:1, (b) converting the mixture obtained in step (a) with formaldehyde and hydrocyanic acid or alkali metal cyanide to the corresponding dinitriles, (c) saponification of the dinitriles resulting from step (b).
摘要翻译：制备甲基甘氨酸二乙酸（MGDA）或其相应的单，二，三碱金属盐或其相应的单 - ，二 - 或三 - 铵盐或其混合物和谷氨酸二乙酸（GLDA）的混合物的方法）或其相应的单 - ，二 - ，三 - 或四 - 碱金属或单 - ，二 - ，三 - 或四 - 铵盐或其混合物，其中所述方法包括以下步骤：（a）溶解（a1）丙氨酸以其L-或D-对映体形式或其相应的单碱金属盐或其混合物的水，和（a2）谷氨酸作为L-或D-对映异构体或其相应的单或二碱金属或混合物其中丙氨酸与谷氨酸的摩尔比在1:9至9:1的范围内，（b）将甲醛和氢氰酸或碱金属氰化物转化为相应的二腈，步骤（a）中得到的混合物与甲醛和氢氰酸或碱金属氰化物反应，（c）由步骤（b）产生的二腈的皂化。

2. 发明申请

WO2016058872A1 CONTAINER COMPRISING A DETERGENT COMPOSITION CONTAINING GLDA 审中-公开
标题翻译：包含GLDA的洗涤剂组合物的容器
公开(公告)号：WO2016058872A1
公开(公告)日：2016-04-21
申请号：PCT/EP2015/073082
申请日：2015-10-07
申请人： BASF SE
发明人： HARTMANN, Markus , JAEKEL, Frank , FRANZKE, Constanze
IPC分类号： C11D17/04 , C11D3/33
CPC分类号： C11D17/045 , C11D3/33 , C11D17/043 , C11D17/046
摘要： Container comprising a single unit dose of a detergent composition containing at least one complexing agent (A) dissolved in an aqueous medium, said complexing agent (A) being a mixture of the L- and D-enantiomers of glutamic acid diacetic acid (GLDA) or its respective mono-, di-, tri- or tetraalkali metal salts or its mono-, di-, tri- or tetraammonium salts, said mixture containing predominantly the respective L-isomer with an enantiomeric excess (ee) in the range of from 5 to 90 %, wherein said container is made from a polymer.
摘要翻译：包含单一单位剂量的含有溶解在水性介质中的至少一种络合剂（A）的洗涤剂组合物的容器，所述络合剂（A）是谷氨酸二乙酸（GLDA）的L-和D-对映异构体的混合物，或其相应的单 - ，二 - ，三 - 或四 - 碱金属盐或其单 - ，二 - ，三 - 或四 - 铵盐，所述混合物主要含有相应的L-异构体，其对映异构体过量（ee） 5至90％，其中所述容器由聚合物制成。

3. 发明申请

WO2017102483A1 PROCESS FOR MAKING A CRYSTALLINE ALKALI METAL SALT OF A COMPLEXING AGENT, AND CRYSTALLINE COMPLEXING AGENT 审中-公开
标题翻译：制备复合剂结晶碱金属盐的方法和结晶复合剂
公开(公告)号：WO2017102483A1
公开(公告)日：2017-06-22
申请号：PCT/EP2016/080001
申请日：2016-12-07
申请人： BASF SE
发明人： FRANZKE, Constanze , FRANZKE, Axel , STAMM, Armin , HARTMANN, Markus , BAUMANN, Robert
IPC分类号： C07C227/42 , C07C229/04
CPC分类号： C07C227/18 , C07C227/10 , C11D3/33 , C07C227/42 , C07C229/36
摘要： Process for manufacturing a crystalline alkali metal salt of the general formula (I) [R 1 -CH(COO)-N(CH 2 -COO) 2 ]M 1 3 (I) wherein M 1 is selected from alkali metal cations, same or different, R 1 is selected from C 1 -C 4 -alkyl and CH 2 CH 2 COOM 1 , comprising the step of (b) crystallizing said alkali metal salt from an aqueous solution containing in the range of from 5 to 30% by weight of alkali metal hydroxide, referring to said aqueous solution.
摘要翻译：制备通式（I）的结晶碱金属盐的方法[R 1 -CH（COO）-N（CH 2）2] -COO）2 M 1 M 3（I）其中M 1选自碱金属阳离子，相同的或者不同，R 1选自C 1 -C 4 - 烷基和CH 2 CH 2 - 包括以下步骤：（b）使所述碱金属盐从含有5至30重量％的碱金属氢氧化物的水溶液中结晶出来，指的是所述水溶液。

4. 发明申请

WO2016142220A1 MIXTURES OF CHELATING AGENTS, AND PROCESS FOR MAKING SUCH MIXTURES 审中-公开
标题翻译：麻醉剂混合物，以及制备这种混合物的方法
公开(公告)号：WO2016142220A1
公开(公告)日：2016-09-15
申请号：PCT/EP2016/054329
申请日：2016-03-01
申请人： BASF SE
发明人： FRANZKE, Constanze , JAEKEL, Frank , SUELING, Carsten
IPC分类号： C07C227/18 , C07C229/16 , C07C229/36 , C11D3/33
CPC分类号： C07C227/18 , C07B2200/07 , C07C229/16 , C11D3/0047 , C11D3/33
摘要： The present invention is directed towards mixtures comprising (A) 90 to 99.9 % by weight of a mixture of L- and D-enantiomers of methyl glycine diacetic acid (MGDA) or its respective mono-, di- or trialkali metal or mono-, di- or triammonium salts, said mixture containing predominantly the respective L-enantiomer with an enantiomeric excess (ee) in the range of from 10 to 99 %, and (B) in total 0.1 to 10 % by weight of the diacetic acid derivative of at least one amino acid selected from valine, leucine, isoleucine, and tyrosine, as free acids or respective mono-, di- or trialkali metal or mono-, di- or triammonium salts, percentages referring to the sum from (A) and (B).
摘要翻译：本发明涉及包含（A）90-99.9重量％的甲基甘氨酸二乙酸（MGDA）的L-和D-对映异构体或其相应的单 - ，二 - 或三 - 碱金属或单 - ，二或三铵盐，所述混合物主要含有对映异构体过量（ee）为10-99％范围内的相应L-对映异构体，和（B）总计0.1-10重量％的二乙酸衍生物至少一种选自缬氨酸，亮氨酸，异亮氨酸和酪氨酸的氨基酸，作为游离酸或相应的单 - ，二 - 或三 - 碱金属或单 - ，二 - 或三 - 铵盐，百分比指的是（A）和（ B）。

5. 发明申请

WO2016058875A1 SOLUTIONS OF TRIALKALI METAL SALTS OF AMINOCARBOXYLIC ACIDS, THEIR MANUFACTURE AND USE 审中-公开
标题翻译：氨基羧酸的试剂金属盐的溶液及其制备和使用
公开(公告)号：WO2016058875A1
公开(公告)日：2016-04-21
申请号：PCT/EP2015/073103
申请日：2015-10-07
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , FRANZKE, Constanze , STAMM, Armin
IPC分类号： C07C227/26 , C07C229/24 , C11D1/10
CPC分类号： C07C229/16 , C07C227/26 , C11D3/044 , C11D3/046 , C11D3/10 , C11D3/2079 , C11D3/2082 , C11D3/33
摘要： Aqueous solution containing in the range of from 60.5 to 75 % by weight of a mixture of trialkalimetal salts of the L-and D-enantiomers of methyl glycine diacetic acid (MGDA), said mixture containing predominantly the respective L-isomer with an enantiomeric excess (ee) in the range of from 3 to 97%, wherein said trialkali metal salts have the general formula (I) [CH 3 -CH(COO)-N(CH 2 -COO) 2 ]K 3-x Na x (I) wherein x is in the range of from zero to 2.9.
摘要翻译：含有60.5至75重量％的甲基甘氨酸二乙酸的L-和D-对映异构体的三碱金属盐（MGDA）的混合物的水溶液，所述混合物主要含有相应的L-异构体和对映体过量的（ee）的范围为3-97％，其中所述三碱金属盐具有通式（I）[CH3-CH（COO）-N（CH2-COO）2] K3-xNax（I）其中x为范围从零到2.9。

6. 发明授权

EP3207025B1 SOLUTIONS OF TRIALKALI METAL SALTS OF AMINOCARBOXYLIC ACIDS, THEIR MANUFACTURE AND USE 有权
公开(公告)号：EP3207025B1
公开(公告)日：2019-07-10
申请号：EP15774933.4
申请日：2015-10-07
申请人： BASF SE
发明人： REINOSO GARCIA, Marta , FRANZKE, Constanze , STAMM, Armin
IPC分类号： C07C227/26 , C07C229/16 , C11D3/33

7. 发明公开

EP3216781A1 MIXTURES CONTAINING POTASSIUM SALTS OF METHYL GLYCINE DIACETIC ACID 审中-公开
标题翻译：含有甲基甘氨酸二乙酸钾盐的混合物
公开(公告)号：EP3216781A1
公开(公告)日：2017-09-13
申请号：EP16159453.6
申请日：2016-03-09
申请人： BASF SE
发明人： JAEKEL, Frank , FRANZKE, Constanze , MORMUL, Verena
IPC分类号： C07C227/26 , C07C229/16 , C07C253/00 , C11D3/10 , C11D3/33
CPC分类号： C11D3/33 , C07B2200/07 , C07C227/26 , C07C229/16 , C07C253/00 , C11D3/044 , C11D3/10 , C07C255/24
摘要： Aqueous solution containing
(A) in the range of from 55 to 75 % by weight of a mixture of tripotassium salts of the L- and D-enantiomers of methyl glycine diacetic acid (MGDA), said mixture containing predominantly the respective L-enantiomer with an enantiomeric excess (ee) in the range of from 5 to 98 %, and
(B) in the range of from 0.01 to 4.0 % by weight, referring to (A), potassium hydroxide or potassium (hydrogen)carbonate or of a combination therefrom.
摘要翻译：含有（A）55-75重量％的甲基甘氨酸二乙酸（MGDA）的L-和D-对映体的三钾盐混合物的水溶液，所述混合物主要含有各自的L-对映体与（A），氢氧化钾或碳酸氢钾或其组合的对映体过量（ee）为5至98％，和（B）为0.01至4.0重量％由此。

8. 发明公开

EP3390349A1 PROCESS FOR MAKING A CRYSTALLINE ALKALI METAL SALT OF A COMPLEXING AGENT, AND CRYSTALLINE COMPLEXING AGENT 有权
公开(公告)号：EP3390349A1
公开(公告)日：2018-10-24
申请号：EP16806138.0
申请日：2016-12-07
申请人： BASF SE
发明人： FRANZKE, Constanze , FRANZKE, Axel , STAMM, Armin , HARTMANN, Markus , BAUMANN, Robert
IPC分类号： C07C227/42 , C07C229/04
CPC分类号： C07C229/36 , C07C227/02 , C07C227/10 , C07C227/18 , C07C227/42 , C11D3/33
摘要： Process for manufacturing a crystalline alkali metal salt of the general formula (I) [R1—CH(COO)—N(CH2—COO)2]M13 (I) wherein M1 is selected from alkali metal cations, same or different, R1 is selected from C1-C4-alkyl and CH2CH2COOM1, comprising the step of (b) crystallizing said alkali metal salt from an aqueous solution containing in the range of from 5 to 30% by weight of alkali metal hydroxide, referring to said aqueous solution.

9. 发明公开

EP3268348A1 PROCESS FOR MAKING MIXTURES OF ENANTIOMERS, AND MIXTURES OF ENANTIOMERS 有权
标题翻译：用于制造混合物的混合物的过程以及混合物的混合物
公开(公告)号：EP3268348A1
公开(公告)日：2018-01-17
申请号：EP16707147.1
申请日：2016-03-02
申请人： BASF SE
发明人： FRANZKE, Constanze , REINOSO GARCIA, Marta , BAUMANN, Robert , GREINDL, Thomas
IPC分类号： C07C229/16 , C07C229/24 , C11D3/33
CPC分类号： C11D3/33 , C07C227/18 , C07C253/00 , C07C253/06 , C07C255/25 , C07C229/16 , C07C229/24
摘要： Process for preparation of a mixture of methyl glycine diacetic acid (MGDA) or its respective mono-, di-, trialkali metal salt or its respective mono-, di- or tri-ammonium salt or mixtures thereof, and glutamic acid diacetic acid (GLDA) or its respective mono-, di-, tri-, or tetra-alkali metal or mono-, di-, tri- or tetra-ammonium salt or mixtures thereof, wherein said process com-prises the steps of: (a) dissolution in water of (a1) alanine in its L- or D-enantiomeric form or its respective monoalkali metal salt or mixtures thereof, and (a2) glutamic acid as L- or D-enantiomer or its respective mono-, or dialkali metal or mixtures thereof, wherein the molar ratio of alanine to glutamic acid is in the range of from 1:9 to 9:1, (b) converting the mixture obtained in step (a) with formaldehyde and hydrocyanic acid or alkali metal cyanide to the corresponding dinitriles, (c) saponification of the dinitriles resulting from step (b).

10. 发明公开

EP3207113A1 CONTAINER COMPRISING A DETERGENT COMPOSITION CONTAINING GLDA 审中-公开
标题翻译：包含含有GLDA的洗涤剂组合物的容器
公开(公告)号：EP3207113A1
公开(公告)日：2017-08-23
申请号：EP15775213.0
申请日：2015-10-07
申请人： BASF SE
发明人： HARTMANN, Markus , JAEKEL, Frank , FRANZKE, Constanze
IPC分类号： C11D17/04 , C11D3/33
CPC分类号： C11D17/045 , C11D3/33 , C11D17/043 , C11D17/046
摘要： Container comprising a single unit dose of a detergent composition containing at least one complexing agent (A) dissolved in an aqueous medium, said complexing agent (A) being a mixture of the L- and D-enantiomers of glutamic acid diacetic acid (GLDA) or its respective mono-, di-, tri- or tetraalkali metal salts or its mono-, di-, tri- or tetraammonium salts, said mixture containing predominantly the respective L-isomer with an enantiomeric excess (ee) in the range of from 5 to 90%, wherein said container is made from a polymer.
摘要翻译：包含单一剂量的含有至少一种溶解在水性介质中的络合剂（A）的洗涤剂组合物的容器，所述络合剂（A）是谷氨酸二乙酸（GLDA）的L-和D-对映体的混合物，或其各自的一，二，三或四碱金属盐或其单盐，二盐，三盐或四铵盐，所述混合物主要含有各自的L-异构体，其对映体过量（ee）为 5至90％，其中所述容器由聚合物制成。

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