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    • 3. 发明申请
    • PROCESS FOR A CONTINUOUS SYNTHESIS OF ZEOLITIC MATERIALS
    • 连续合成沸石材料的方法
    • WO2017216236A1
    • 2017-12-21
    • PCT/EP2017/064567
    • 2017-06-14
    • BASF SE
    • MARX, StefanCLADE, StefanieARNOLD, LenaDIEHLMANN, UweMUELLER, Ulrich
    • C01B39/48C01B39/04B01J29/76
    • The present invention relates to a continuous process for preparing a zeolitic material comprising (i) preparing a mixture comprising a source of YO 2 , optionally a source of X 2 O 3 , and a liquid solvent system; (ii) continuously feeding the mixture prepared in (i) into a continuous flow reactor at a liquid hourly space velocity in the range of from 0.3 to 20 h -1 for a duration of at least 1 h; and (iii) crystallizing the zeolitic material from the mixture in the continuous flow reactor, wherein the mixture is heated to a temperature in the range of from 100 to 300°C; wherein the volume of the continuous flow reactor is in the range of from 150 cm³ to 75 m³, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.
    • 本发明涉及制备沸石材料的连续方法,所述方法包括(i)制备包含YO 2来源,任选地来源于XO 2, 2 O 3和液体溶剂体系; (ii)将(i)中制备的混合物以0.3-20h -1的液时空速连续加入连续流动反应器持续至少1小时; 和(iii)在连续流动反应器中从混合物中结晶沸石材料,其中将混合物加热至100-300℃的温度; 其中连续流动反应器的体积在150cm 3〜 到75m 3以及可根据本发明方法获得的沸石材料及其用途。