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1. 发明专利

JPH0710961B2 失效
公开(公告)号：JPH0710961B2
公开(公告)日：1995-02-08
申请号：JP50071589
申请日：1988-11-02
申请人： BASF LACKE & FARBEN
发明人： GEIST MICHAEL , CIBURA KLAUS , JOUCK WALTER , OTT GUENTHER , SADLOWSKI JUERGEN , DANGSCHAT MANDRED , REIMANN MANFRED
IPC分类号： C08G18/58 , C08G18/64 , C08G18/80 , C08G59/14 , C08G59/52 , C08J3/07 , C09D5/44 , C09D163/00 , C09D175/00

2. 发明申请

WO8909794A3 PROCESS FOR PRODUCING POLYESTER RESINS 审中-公开
标题翻译：生产聚酯树脂的方法
公开(公告)号：WO8909794A3
公开(公告)日：1989-11-16
申请号：PCT/EP8900162
申请日：1989-02-22
申请人： BASF LACKE & FARBEN
发明人： SADLOWSKI JUERGEN , DANGSCHAT MANFRED , DIEFENBACH HORST , LASAR THEO , SCMITT DIETER
IPC分类号： C08G63/78 , C08G63/22
CPC分类号： C08G63/78
摘要： In a process for producing polyester and alkyde resins from bi- and/or higher functional carboxylic acids and/or their derivatives and from bi- and/or higher functional alcohols, the reaction is carried ont intermittently in stirred boiler reactors with rectifying columns. To improve the transport of the condensation products, an entrainer is introduced throughtout the reaction into the reaction mixture below the surface and uniformly distributed by a delivery device. In addition, the condensation reaction is carried out at an absolute pressure of 1.5 to 10 bar until the peak reaction rate is attained. The pressure is then reduced to atmospheric pressure at a gradient of -0.05 bar/h to -5 bar/h in a second reaction phase. The reaction is continued at standard pressure until the product exhibits the desired properties. The reaction temperature lies between 180 and 320°C. This results in shorter processing times, and the products are accordingly subjected to lower thermal stresses and possess improved properties.

3. 发明专利

CA1329292C PROCESS FOR THE PREPARATION OF BINDER DISPERSIONS CAPABLE OF BEING CATHODICALLY DEPOSITED USING CROSSLINKING AGENTS BASED ON POLYISOCYANATES BLOCKED BY HYDROXYL GROUPS 未知
公开(公告)号：CA1329292C
公开(公告)日：1994-05-03
申请号：CA582706
申请日：1988-11-10
申请人： BASF LACKE & FARBEN
发明人： GEIST MICHAEL , CIBURA KLAUS , JOUCK WALTER , OTT GUENTHER , SADLOWSKI JUERGEN , DANGSCHAT MANFRED , REIMANN MANFRED
IPC分类号： C08G18/58 , C08G18/64 , C08G18/80 , C08G18/81 , C08G59/14 , C08J3/07 , C09D5/44 , C09D163/00 , C09D175/00
摘要： Process for the preparation of binder dispersions capable of being cathodically deposited using crosslinking agents based on polyisocyanates blocked by hydroxyl groups The invention relates to a process for the preparation of aqueous dispersions to be further processed to electrocoating paints with baking temperatures below 160.degree.C and baking times ? 30 minutes, which dispersions contain modified epoxide-amine adducts as binders and polyisocyanates blocked by hydroxyl groups as crosslinking agents. In this process polyepoxides and compounds containing one or more, preferably 2, hydroxyl groups per molecule are reacted at elevated temperatures in the presence of catalysts to furnish epoxide-containing intermediates. A solvent or a mixture of solvents is then added with external cooling and the solution is boiled under reflux, if necessary in vacuo, until the temperature of the solution drops to 95.degree.C to 20.degree.C. Amines are then added onto the epoxide groups which are still present in a free state in the epoxy resin and a dispersion is prepared by adding a water/acid mixture after adding the crosslinking agent or the dispersion is first prepared and the crosslinking agent is added subsequently.

4. 发明专利

DE58904651D1 未知
公开(公告)号：DE58904651D1
公开(公告)日：1993-07-15
申请号：DE58904651
申请日：1989-02-22
申请人： BASF LACKE & FARBEN
发明人： SADLOWSKI JUERGEN , DANGSCHAT MANFRED , DIEFENBACH HORST , LASAR THEO , SCMITT DIETER
IPC分类号： C08G63/78
摘要： PCT No. PCT/EP89/00162 Sec. 371 Date Nov. 15, 1990 Sec. 102(e) Date Nov. 15, 1990 PCT Filed Feb. 22, 1989 PCT Pub. No. WO89/09794 PCT Pub. Date Oct. 19, 1989.The invention relates to a process for the preparation of polyester and alkyd resins from bifunctional and/or polyfunctional carboxylic acids and/or derivatives thereof and from bifunctional and/or polyfunctional alcohols. The reaction is carried out in stirred kettle reactors which are operated discontinuously and equipped with rectifying columns. During the entire reaction an entraining agent is introduced into the reaction mixture below surface level, with thorough distribution, by means of a delivery device in order to improve the transport of the products of the condensation reaction. In addition, the condensation reaction is carried out under an absolute pressure of 1.5 to 10 bar at least until the maximum reaction rate has been reached. The pressure is then reduced to atmospheric pressue at a gradient of -0.05 bar/hour to -5 bar/hour in a second reaction phase. The reaction is continued under normal pressure until the product exhibits the desired properties. The reaction temperature is between 180 and 320 DEG C. The process times, in particular, are shortened as a result of this process, and the process products, which are exposed to heat for a correspondingly shorter time, are distinguished by imprved properties.

5. 发明专利

BR8907369A 未知
公开(公告)号：BR8907369A
公开(公告)日：1991-04-16
申请号：BR8907369
申请日：1989-02-22
申请人： BASF LACKE & FARBEN
发明人： SADLOWSKI JUERGEN , DANGSCHAFT MANFRED , DIEFENBACH HORST , SCHMITT DIETER , LASAR THEO
IPC分类号： C08G63/78
摘要： PCT No. PCT/EP89/00162 Sec. 371 Date Nov. 15, 1990 Sec. 102(e) Date Nov. 15, 1990 PCT Filed Feb. 22, 1989 PCT Pub. No. WO89/09794 PCT Pub. Date Oct. 19, 1989.The invention relates to a process for the preparation of polyester and alkyd resins from bifunctional and/or polyfunctional carboxylic acids and/or derivatives thereof and from bifunctional and/or polyfunctional alcohols. The reaction is carried out in stirred kettle reactors which are operated discontinuously and equipped with rectifying columns. During the entire reaction an entraining agent is introduced into the reaction mixture below surface level, with thorough distribution, by means of a delivery device in order to improve the transport of the products of the condensation reaction. In addition, the condensation reaction is carried out under an absolute pressure of 1.5 to 10 bar at least until the maximum reaction rate has been reached. The pressure is then reduced to atmospheric pressue at a gradient of -0.05 bar/hour to -5 bar/hour in a second reaction phase. The reaction is continued under normal pressure until the product exhibits the desired properties. The reaction temperature is between 180 and 320 DEG C. The process times, in particular, are shortened as a result of this process, and the process products, which are exposed to heat for a correspondingly shorter time, are distinguished by imprved properties.

6. 发明专利

AT90370T VERFAHREN ZUR HERSTELLUNG VON POLYESTERHARZEN. 未知
公开(公告)号：AT90370T
公开(公告)日：1993-06-15
申请号：AT89902517
申请日：1989-02-22
申请人： BASF LACKE & FARBEN
发明人： SADLOWSKI JUERGEN , DANGSCHAT MANFRED , DIEFENBACH HORST , LASAR THEO , SCMITT DIETER
IPC分类号： C08G63/78

7. 发明专利

BR8807784A 未知
公开(公告)号：BR8807784A
公开(公告)日：1990-10-16
申请号：BR8807784
申请日：1988-11-02
申请人： BASF LACKE & FARBEN
发明人： GEIST MICHAEL , CIBURA KLAUS , JOUCK WALTER , OTT GUENTHER , SADLOWSKI JUERGEN , DANGSCHAT MANDRED , REIMANN MANFRED
IPC分类号： C08G18/58 , C08G18/64 , C08G18/80 , C08G59/14 , C08G59/52 , C08J3/07 , C09D5/44 , C09D163/00 , C09D175/00 , C08J3/10

8. 发明专利

CA1329675C PROCESS FOR THE PREPARATION OF POLYESTER RESINS 未知
公开(公告)号：CA1329675C
公开(公告)日：1994-05-17
申请号：CA596560
申请日：1989-04-13
申请人： BASF LACKE & FARBEN
发明人： SADLOWSKI JUERGEN , DIEFENBACH HORST , DANGSCHAT MANFRED , LASAR THEO , SCHMITT DIETER
IPC分类号： C08G63/78 , C08G63/123 , C08G63/49
摘要： Process for the preparation of polyester resins The invention relates to a process for the preparation of polyester and alkyd resins from bifunctional and/or polyfunctional carboxylic acids and/or derivatives thereof and from bifunctional and/or polyfunctional alcohols. The reaction is carried out in stirred kettle reactors which are operated discontinuously and equipped with rectifying columns. During the entire reaction an entraining agent is introduced into the reaction mixture below surface level, with thorough distribution, by means of a delivery device in order to improve the transport of the products of the condensation reaction. In addition, the condensation reaction is carried out under an absolute pressure of 1.5 to 10 bar at least until the maximum reaction rate has been reached. The pressure is then reduced to atmospheric pressure at a gradient of -0.05 bar/ hour to -5 bar/hour in a second reaction phase. The reaction is continued under normal pressure until the product exhibits the desired properties. The reaction temperature is between 180 and 320.degree.C. The process times, in particular are shortened as a result of this process, and the process products, which are exposed to heat for a correspondingly shorter time, are distinguished by improved properties.

9. 发明专利

CA1329291C PROCESS FOR THE PREPARATION OF BINDER DISPERSIONS CAPABLE OF BEING CATHODICALLY DEPOSITED USING CROSSLINKING AGENTS BASED ON POLYISOCYANATES BLOCKED BY AMINO GROUPS 未知
公开(公告)号：CA1329291C
公开(公告)日：1994-05-03
申请号：CA582703
申请日：1988-11-10
申请人： BASF LACKE & FARBEN
发明人： GEIST MICHAEL , CIBURA KLAUS , JOUCK WALTER , OTT GUENTHER , SADLOWSKI JUERGEN , DANGSCHAT MANFRED , REIMANN MANFRED
IPC分类号： C08G18/58 , C08G18/64 , C08G18/80 , C08G59/14 , C08G59/52 , C08J3/07 , C09D5/44 , C09D163/00 , C09D175/00
摘要： Process for the preparation of binder dispersions capable of being cathodically deposited using crosslinking agents based on polyisocyanates blocked by amino groups The invention relates to a process for the preparation of aqueous dispersions to be further processed to electrocoating paints with baking temperatures below 160.degree.C and baking times of ? 30 minutes, which dispersions contain modified epoxide-amine adducts as binders and polyisocyanates blocked by amino groups as crosslinking agents. In this process, polyepoxides and compounds which contain one or more, preferably 2, hydroxyl groups per molecule are converted at higher temperatures and in the presence of catalysts to epoxide-containing intermediates. A solvent or a mixture of solvents is then added with external cooling and the solution is then caused to boil under reflux, if necessary by application of a vacuum, until the temperature of the solution drops to 95.degree.C to 20.degree.C. Amines are then added onto the epoxide groups which are still present in a free state in the epoxide resin and either a dispersion is prepared after the addition of the crosslinking agent by adding a water-acid mixture or the products are first dispersed and the crosslinking agent is added subsequently.

10. 发明专利

BR8807786A 未知
公开(公告)号：BR8807786A
公开(公告)日：1990-10-09
申请号：BR8807786
申请日：1988-11-03
申请人： BASF LACKE & FARBEN
发明人： GEIST MICHAEL , CIBURA KLAUS , JOUCK WALTER , OTT GUENTHER , SADLOWSKI JUERGEN , DANGSCHAT MANFRED , REIMANN MANFRED
IPC分类号： C08G18/58 , C08G18/64 , C08G18/80 , C08G18/81 , C08G59/14 , C08J3/07 , C09D5/44 , C09D163/00 , C09D175/00
摘要： PCT No. PCT/EP88/00998 Sec. 371 Date Jun. 13, 1990 Sec. 102(e) Date Jun. 13, 1990 PCT Filed Nov. 3, 1988 PCT Pub. No. WO89/04353 PCT Pub. Date May 18, 1989.The invention relates to a process for the preparation of aqueous dispersions to be further processed to electrocoating paints with baking temperatures below 160 DEG C. and baking times

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