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1. 发明申请

WO2004007436A1 VERFAHREN ZUR KONTINUIERLICHEN HERSTELLUNG VON TETRASUBSTITUIERTEN HARNSTOFFEN 审中-公开
标题翻译：工艺为TETRA取代脲连续生产
公开(公告)号：WO2004007436A1
公开(公告)日：2004-01-22
申请号：PCT/EP2003/007083
申请日：2003-07-03
申请人： BASF AKTIENGESELLSCHAFT , HENKELMANN, Jochem , WEBER, Theodor , ROHDE, Thorsten , BUSCH, Ralph
发明人： HENKELMANN, Jochem , WEBER, Theodor , ROHDE, Thorsten , BUSCH, Ralph
IPC分类号： C07C273/18
CPC分类号： C07C273/1809 , C07C275/06
摘要： Verfahren zur Herstellung von tetrasubstituierten Harnstoffen durch Umsetzung der entsprechenden Amine mit Phosgen in Gegenwart einer wässrigen anorganischen Base bei einer Temperatur im Bereich von 0 bis 150 Grad Celsius bei dem man das entsprechende Amin, das Phosgen und die wässrige anorganische Base dem Reaktionsapparat im Mittel kontinuierlich zuführt,durch die Auswahl der herzustellenden tetrasubstituierten Harnstoffe, durch die Mengenverhältnisse der zuzuführenden Stoffe und Stoffgemische, durch die Temperatur während der Umsetzung und gegebenenfalls durch die Zufuhr eines organischen, mit Wasser nicht vollständig mischbaren Lösungsmittels im Reaktionsapparat ein Zweiphasensystem bildet, und das Reaktionsgemisch aus dem Reaktionsapparat im Mittel kontinuierlich abführt.
摘要翻译：一种用于通过在与光气在含水无机碱的存在下在0至150摄氏度，相应的胺，光气和含水无机碱到反应装置中的中间连续范围内的温度的供给相应的胺反应制备四取代的脲的处理通过在反应过程中所产生的四取代的脲由所供给的物质和物质混合物，通过温度的比例，并且如果合适，通过一个有机的，不完全混溶的供给与反应装置的水溶剂的选择是一个两相系统的形式，并且从反应器的反应混合物平均持续放电。

2. 发明公开

EP1259473A1 VERFAHREN ZUR HERSTELLUNG VON CHLORCARBONSÄURECHLORIDEN 有权
标题翻译： VERFAHREN ZUR HERSTELLUNG VONCHLORCARBONSÄURECHLORIDEN
公开(公告)号：EP1259473A1
公开(公告)日：2002-11-27
申请号：EP01919355.6
申请日：2001-02-28
申请人： BASF AKTIENGESELLSCHAFT
发明人： STAMM, Armin , KNEUPER, Heinz-Josef , HENKELMANN, Jochem , WEBER, Theodor , BUSCH, Ralph
IPC分类号： C07C51/60 , C07C53/50
CPC分类号： C07C51/60 , C07C53/50
摘要： The invention relates to a method for producing chlorocarboxylic acid chlorides of formula (I), wherein R?1 and R2¿, independently from one another, mean a hydrogen atom, an organic radical containing carbon, a halogen, a nitro or cyano group and Y means an alkylene chain having 1 to 10 carbon atoms in the chain which is unsubstituted or is substituted by organic radicals that contain carbon, by halogen, nitro and/or cyano groups, whereby the alkylene chain can be interrupted by an ether-, thioether-, tertiary amino- or keto group, whereby the organic radicals of Y and/or R1 and/or R2 can be connected to one another and thereby form a non-aromatic system, whereby said radicals contain carbon, by converting a lactone of formula (II), wherein R1, R2 and Y have the aforementioned meanings, using a hydrogen chloride and phosgene in the presence of a catalyst. Hydrogen chloride is added before and/or while phosgene is added. The hydrogen chloride is only introduced at a temperature of at least 60 °C. A pyridine compound is used as the catalyst.
摘要翻译：本发明涉及制备式（I）的氯代羧酸氯化物的方法，其中R 1和R 2彼此独立地表示氢原子，含碳的有机基团，卤素，硝基或氰基，和 Y表示在未被取代或被含有碳的有机基团取代的链中具有1至10个碳原子的亚烷基链，其通过卤素，硝基和/或氰基基团取代，其中亚烷基链可被醚 - ，硫醚 - 叔氨基或酮基，其中Y和/或R 1和/或R 2的有机基团可以彼此连接并由此形成非芳族体系，由此所述基团含有碳，通过将式（II）的化合物，其中R1，R2和Y具有上述含义，在催化剂存在下使用氯化氢和光气。氯化氢在加入光气之前和/或加入光气时加入。氯化氢仅在至少60℃的温度下引入。吡啶化合物用作催化剂。

3. 发明公开

EP1212281A2 VERFAHREN ZUR HERSTELLUNG VON CARBONSÄURECHLORIDEN 有权
标题翻译：用于生产羧酸酰氯
公开(公告)号：EP1212281A2
公开(公告)日：2002-06-12
申请号：EP00960571.8
申请日：2000-08-31
申请人： BASF AKTIENGESELLSCHAFT
发明人： BUSCH, Ralph , KNEUPER, Heinz-Josef , WEBER, Theodor , MÜLLER, Winfried , STAMM, Armin , HENKELMANN, Jochem
IPC分类号： C07C51/60 , C07C51/64
CPC分类号： C07C51/64 , C07C51/60
摘要： The invention relates to a method for producing acid chlorides by converting carboxylic acids with carbon oxychlorides or thionyl chloride in the presence of a catalyst adduct of an N,N-disubstituted formamide of general formula (I) and carbon oxychloride or thionyl chloride. In the formula, R?1 and R2¿, independently from one another, mean C¿1?- to C4-alkyl or R?1 and R2¿ together mean a C¿4?- or C5-alkylene chain. According to the inventive method, hydrogen chloride is added during and/or after the conversion.

4. 发明授权

EP1259473B1 VERFAHREN ZUR HERSTELLUNG VON CHLORCARBONSÄURECHLORIDEN 有权
标题翻译：用于生产氯氯化物
公开(公告)号：EP1259473B1
公开(公告)日：2005-10-26
申请号：EP01919355.6
申请日：2001-02-28
申请人： BASF Aktiengesellschaft
发明人： STAMM, Armin , KNEUPER, Heinz-Josef , HENKELMANN, Jochem , WEBER, Theodor , BUSCH, Ralph
IPC分类号： C07C51/60 , C07C53/50
CPC分类号： C07C51/60 , C07C53/50
摘要： The invention relates to a method for producing chlorocarboxylic acid chlorides of formula (I), wherein R?1 and R2¿, independently from one another, mean a hydrogen atom, an organic radical containing carbon, a halogen, a nitro or cyano group and Y means an alkylene chain having 1 to 10 carbon atoms in the chain which is unsubstituted or is substituted by organic radicals that contain carbon, by halogen, nitro and/or cyano groups, whereby the alkylene chain can be interrupted by an ether-, thioether-, tertiary amino- or keto group, whereby the organic radicals of Y and/or R1 and/or R2 can be connected to one another and thereby form a non-aromatic system, whereby said radicals contain carbon, by converting a lactone of formula (II), wherein R1, R2 and Y have the aforementioned meanings, using a hydrogen chloride and phosgene in the presence of a catalyst. Hydrogen chloride is added before and/or while phosgene is added. The hydrogen chloride is only introduced at a temperature of at least 60 °C. A pyridine compound is used as the catalyst.

5. 发明授权

EP1212281B1 VERFAHREN ZUR HERSTELLUNG VON CARBONSÄURECHLORIDEN 有权
标题翻译：用于生产羧酸酰氯
公开(公告)号：EP1212281B1
公开(公告)日：2004-08-11
申请号：EP00960571.8
申请日：2000-08-31
申请人： BASF AKTIENGESELLSCHAFT
发明人： BUSCH, Ralph , KNEUPER, Heinz-Josef , WEBER, Theodor , MÜLLER, Winfried , STAMM, Armin , HENKELMANN, Jochem
IPC分类号： C07C51/60 , C07C51/64
CPC分类号： C07C51/64 , C07C51/60
摘要： The invention relates to a method for producing acid chlorides by converting carboxylic acids with carbon oxychlorides or thionyl chloride in the presence of a catalyst adduct of an N,N-disubstituted formamide of general formula (I) and carbon oxychloride or thionyl chloride. In the formula, R and R , independently from one another, mean C1- to C4-alkyl or R and R together mean a C4- or C5-alkylene chain. According to the inventive method, hydrogen chloride is added during and/or after the conversion.

6. 发明公开

EP1212273A2 VERFAHREN ZUR REINIGUNG VON CARBONSÄURECHLORIDEN 有权
标题翻译：清理方法碳酰氯
公开(公告)号：EP1212273A2
公开(公告)日：2002-06-12
申请号：EP00972657.1
申请日：2000-08-31
申请人： BASF AKTIENGESELLSCHAFT
发明人： BUSCH, Ralph , KNEUPER, Heinz-Josef , WEBER, Theodor , MÜLLER, Winfried , STAMM, Armin , HENKELMANN, Jochem
IPC分类号： C07C51/00
CPC分类号： C07C51/64 , C07C53/42
摘要： The invention relates to a method for purifying acid chlorides which have been produced by converting carboxylic acids with carbon oxychloride or thionyl chloride in the presence of a catalyst adduct. The acid chlorides are treated with a hydro halide of carboxylic acid amides of general formula (I), wherein R1 stands for hydrogen or C¿1?- to C3-alkyl; R?2 and R3¿, independently from one another, mean C¿1?- to C4-alkyl or R?2 and R3¿ together mean a C¿4?- or C5-alkylene chain. The thus purified acid chloride is isolated by separation said acid chloride from the carboxylic acid amide hydro halide-phase.

7. 发明公开

EP1521739A1 VERFAHREN ZUR KONTINUIERLICHEN HERSTELLUNG VON TETRASUBSTITUIERTEN HARNSTOFFEN 有权
标题翻译：工艺为TETRA取代脲连续生产
公开(公告)号：EP1521739A1
公开(公告)日：2005-04-13
申请号：EP03763693.3
申请日：2003-07-03
申请人： BASF AKTIENGESELLSCHAFT
发明人： HENKELMANN, Jochem , WEBER, Theodor , ROHDE, Thorsten , BUSCH, Ralph
IPC分类号： C07C273/18 , C07C275/06
CPC分类号： C07C273/1809 , C07C275/06
摘要： The invention relates to a method for producing tetra-substituted ureas by reacting the corresponding amines with phosgene in the presence of an aqueous inorganic base at a temperature ranging of from 0 to 150 °C. According to the inventive method, the corresponding amine, the phosgene and the aqueous inorganic base are on average continuously fed to the reactor, a two-phase system is formed in the reactor by selecting the tetra-substituted ureas to be produced, by selecting the quantitative ratio of the substances and substance mixtures to be added, by selecting the temperature during reaction and optionally by adding an organic solvent that is not completely miscible with water, and the reaction mixture is discharged from the reactor in an on average continuous manner.

8. 发明授权

EP1212273B1 VERFAHREN ZUR REINIGUNG VON CARBONSÄURECHLORIDEN 有权
标题翻译：清理方法碳酰氯
公开(公告)号：EP1212273B1
公开(公告)日：2005-02-02
申请号：EP00972657.1
申请日：2000-08-31
申请人： BASF AKTIENGESELLSCHAFT
发明人： BUSCH, Ralph , KNEUPER, Heinz-Josef , WEBER, Theodor , MÜLLER, Winfried , STAMM, Armin , HENKELMANN, Jochem
IPC分类号： C07C51/00
CPC分类号： C07C51/64 , C07C53/42
摘要： The invention relates to a method for purifying acid chlorides which have been produced by converting carboxylic acids with carbon oxychloride or thionyl chloride in the presence of a catalyst adduct. The acid chlorides are treated with a hydro halide of carboxylic acid amides of general formula (I), wherein R1 stands for hydrogen or C¿1?- to C3-alkyl; R?2 and R3¿, independently from one another, mean C¿1?- to C4-alkyl or R?2 and R3¿ together mean a C¿4?- or C5-alkylene chain. The thus purified acid chloride is isolated by separation said acid chloride from the carboxylic acid amide hydro halide-phase.

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