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1. 发明申请

WO02090299A3 METHOD FOR THE PRODUCTION OF A PURIFIED MELT OF AT LEAST ONE MONOMER 审中-公开
标题翻译：方法一种精制熔炼至少一种单体
公开(公告)号：WO02090299A3
公开(公告)日：2003-03-27
申请号：PCT/EP0204793
申请日：2002-05-02
申请人： BASF AG , HAMMON ULRICH , ECK BERND , BAUMANN DIETER , HEILEK JOERG , MUELLER-ENGEL KLAUS JOACHIM
发明人： HAMMON ULRICH , ECK BERND , BAUMANN DIETER , HEILEK JOERG , MUELLER-ENGEL KLAUS JOACHIM
IPC分类号： C07B61/00 , C07B63/00 , C07C51/43 , C07C51/47 , C07C51/48 , C07C57/07 , C07D207/26 , C07D207/267
CPC分类号： C07D207/267 , C07C51/43 , C07C51/47 , C07C51/48 , C07C57/04
摘要： The invention relates to a method for the production of a purified melt of a monomer melt obtained by condensation, absorption or extraction in a crystallizer, wherein the inlet to the crystallizer is subjected to a mechanical solid/liquid separation operation.
摘要翻译：一种制备经缩合，吸收或萃取Monomerenschmelze在结晶回收的纯化的熔化物的，其中所述进料的机械固/液分离操作的结晶器进行处理。

2. 发明申请

WO2006111565A3 METHOD FOR THE REGULATION OF A HYDRAULIC WASH COLUMN 审中-公开
标题翻译：一种用于控制液压洗涤塔
公开(公告)号：WO2006111565A3
公开(公告)日：2007-04-19
申请号：PCT/EP2006061714
申请日：2006-04-20
申请人： BASF AG , HEILEK JOERG , MUELLER-ENGEL KLAUS JOACHIM , HAMMON ULRICH , WALTER THOMAS
发明人： HEILEK JOERG , MUELLER-ENGEL KLAUS JOACHIM , HAMMON ULRICH , WALTER THOMAS
IPC分类号： B01D11/02 , B01D9/00
CPC分类号： C07C51/43 , C07C57/04
摘要： Disclosed is a method for operating a hydraulic wash column, in which the position of the wash front in the wash column is determined by means of the rate of flow of the control liquor conducted into the wash column and/or by means of the rate of flow of the suspension conducted into the wash column, and the rate of flow is defined with the aid of the difference in pressure between points in the suspension zone located upstream of the wash front and points in the zone extending from the wash front to the end of the crystal bed in the column.
摘要翻译：进行操作的液压洗涤塔，其中积累前在洗涤塔的通过的电流的量的装置的位置，以被引导到洗涤塔控制液和/或由所述压力差的装置定位在由被引导到洗涤塔悬浮液和电流设定的量的质量流量的装置的方法，它由在位于所述堆积前悬架区和点前面在高达晶体床从堆积前区突出的端部的点之间的列。

3. 发明申请

WO0155076A3 PURIFICATION METHOD FOR (METH)ACRYLIC ACID 审中-公开
标题翻译：（甲基）丙烯酸的清洗方法
公开(公告)号：WO0155076A3
公开(公告)日：2001-12-20
申请号：PCT/EP0100743
申请日：2001-01-24
申请人： BASF AG , DECKER EMILE DE , BASTIAENSEN ERIK , BAUMANN DIETER , ECK BERND , HEILEK JOERG
发明人： DE DECKER EMILE , BASTIAENSEN ERIK , BAUMANN DIETER , ECK BERND , HEILEK JOERG
IPC分类号： C07C51/43 , C07C57/07
CPC分类号： C07C51/43 , C07C57/04
摘要： The invention concerns a method for purifying (meth)acrylic acid by means of crystallization, whereby the (meth)acrylic acid is purified by combining at least two different dynamic crystallization methods, especially a suspension crystallization method and a layer crystallization method.
摘要翻译：本发明涉及通过结晶纯化（甲基）丙烯酸的方法，其中通过至少两种不同的动态结晶过程，特别是悬浮结晶和层结晶的组合来纯化（甲基）丙烯酸。

4. 发明申请

WO0190066A3 METHOD FOR OBTAINING PURE N-VINYL PYRROLIDONE 审中-公开
标题翻译：得到纯N-乙烯基吡咯烷酮
公开(公告)号：WO0190066A3
公开(公告)日：2002-08-01
申请号：PCT/EP0106006
申请日：2001-05-25
申请人： BASF AG , ECK BERND , HEILEK JOERG , SCHMIDT-RADDE MARTIN , HELFERT HERBERT
发明人： ECK BERND , HEILEK JOERG , SCHMIDT-RADDE MARTIN , HELFERT HERBERT
IPC分类号： C07D201/16 , C07D207/26 , C07D207/267
CPC分类号： C07D207/267 , C07D201/16
摘要： The invention relates to a method for obtaining pure N-vinyl pyrrolidone from raw materials containing N-vinyl pyrrolidone, said method comprising a single or multiple-stage crystallisation method. The method is characterised in that the mother liquor of the first crystallisation stage is either purified by distillation and/or extraction or is returned to a product stream of the production process, said stream containing an N-vinyl pyrrolidone.
摘要翻译：公开了一种用于从含N乙烯基吡咯烷酮的粗产物得到纯的N-乙烯基吡咯烷酮，包括单级或多级结晶方法，其特征在于供给所述母液从所述第一结晶阶段或者是蒸馏和/或萃取纯化或在A N的方法返回制造过程的含乙烯基吡咯烷酮的产物流。

5. 发明申请

WO2004087723A3 METHOD FOR PRODUCING ACYLPHOSPHINE OXIDE SOLIDS 审中-公开
标题翻译：用于生产酰基固体
公开(公告)号：WO2004087723A3
公开(公告)日：2005-02-24
申请号：PCT/EP2004003349
申请日：2004-03-30
申请人： BASF AG , BERTLEIN GERHARD , SCHALL KARL HEINZ , MAASE MATTHIAS , HEILEK JOERG , BAUMANN DIETER , ASCHERL HERMANN
发明人： BERTLEIN GERHARD , SCHALL KARL HEINZ , MAASE MATTHIAS , HEILEK JOERG , BAUMANN DIETER , ASCHERL HERMANN
IPC分类号： C07F9/53
CPC分类号： C07F9/5337
摘要： The invention relates to a method for producing acylphosphine oxide solids consisting in transforming a molten or dispersed acylphosphine oxide into the solid aggregated state thereof by means of mechanical stress, shear force or the internal motion of the melt.
摘要翻译：本发明涉及一种方法，用于生产固体酰基膦氧化物，通过将熔体或作为分散相vorliegendes机械应力，在固体状态下的熔体的剪切/内运动下酰基膦。

6. 发明专利

JPH10323502A METHOD FOR CRYSTALLIZING MATERIAL TO BE ISOLATED BY VAPORIZATION AND VAPOR CONDENSATION 失效
公开(公告)号：JPH10323502A
公开(公告)日：1998-12-08
申请号：JP12137598
申请日：1998-04-30
申请人： BASF AG
发明人： ECK BERND , HEILEK JOERG
IPC分类号： B01D9/02 , B01D9/00 , C01D1/30 , C07C29/78 , C07C31/20 , C07C51/43 , C07C53/08
摘要： PROBLEM TO BE SOLVED: To increase the application range of crystallization and to obtain an economically advantageous method by controlling the partial pressure of the fluid component which is condensed from a liquid mixture containing a specified material to be isolated, to be lower than the partial pressure of the fluid component on a crystallization soln., and controlling the solidifying temp. of the liquid mixture to be lower than the condensation temp. in the liquid mixture. SOLUTION: The material to be isolated means inorg. salts, salts. of org. compds., solvates of these, and preferably hydrates present in a mixture with water or an org. solvent as a fluid. Or, it means a certain kind of org. component in such a mixture with water or an org. solvent that has a narrow boiling temp. range, however, the gas phase and the liquid phase in an equilibrium state under crystallization pressure and a crystallization temp. show

7. 发明专利

JPH10324681A IMIDAZOLE AND PURIFICATION OF EFFECTIVE SUBSTANCE CONTAINING THE SAME AS BASE BY CRYSTALLIZATION 失效
公开(公告)号：JPH10324681A
公开(公告)日：1998-12-08
申请号：JP1863598
申请日：1998-01-30
申请人： BASF AG
发明人： FRITZ GERHARD DR , WACHE HARRO DR , ECK BERND , HEILEK JOERG , GRUENENWALD THOMAS , GRAUENHORST KARL RAINER
IPC分类号： A61K31/415 , A61K31/495 , A61P31/04 , C07D233/28 , C07D233/54 , C07D233/58 , C07D233/60 , C07D233/62 , C07D233/64 , C07D233/92 , C07D405/06 , C07D409/12 , C07D521/00
摘要： PROBLEM TO BE SOLVED: To purify the subject compound in an industrial scale and simple and sure manner by carrying out crystallization on cooling surface on which crystals of an imidazole compound are grown. SOLUTION: In a method for purifying either one of an imidazole of formula I (R to R are each H, a halogen, acetyl, carboxyl, a 1-20C alkyl, a 6-12C aryl, etc.), and an effective substance containing the imidazole as a base by crystallization, the crystallization is carried out on at least one cooling surface on which crystals of imidazole compound grows. The effective substance containing the imidazole as a base includes e.g. secnidazole of formula II or climbazole of formula III. In the purification, crystals of imidazole compound which grows on the cooling surface are preferably brought through the cooling surface into contact with a liquid mixture (preferably containing at least 80 wt.% imidazole compound) of a substance containing an imidazole compound to be purified and the cooling surface is cooled to form the corresponding crystals.

8. 发明专利

MY143513A PROCESS FOR REMOVING METHACRYLIC ACID FROM LIQUID PHASE COMPRISING ACRYLIC ACID AS A MAIN CONSTITUENT AND TARGET PRODUCT, AND METHACRYLIC ACID AS A SECONDARY COMPONENT 未知
公开(公告)号：MY143513A
公开(公告)日：2011-05-31
申请号：MYPI20060773
申请日：2006-02-23
申请人： BASF AG
发明人： HEILEK JOERG , MUELLER-ENGEL KLAUS JOACHIM DR , ADAMI CHRISTOPH DR , DIETERLE MARTIN DR
IPC分类号： C07C51/42
摘要： A PROCESS FOR REMOVING METHACRYLIC ACID FROM LIQUID PHASE P COMPRISING ACRYLIC ACID AS A MAIN CONSTITUENT AND TARGET PRODUCT, AND METHACRYLIC ACID AS A SECONDARY COMPONENT IN WHICH THE REMOVAL IS CFFECTED BY CRYSTALLIZATION, THE ACRYLIC ACID ACCUMULATING IN THE CRYSTALS FORMED AND THE METHACRYLIC ACID IN THE REMAINING MOTHER LIQUOR.

9. 发明专利

DE102005018702A1 Process to control hydraulic wash column, comprises feeding mother liquor, conducting liquor to filter tube, feeding control liquor to wash column, purifying liquor, transporting crystal bed, removing crystal and determining flow rate 未知
公开(公告)号：DE102005018702A1
公开(公告)日：2006-10-26
申请号：DE102005018702
申请日：2005-04-21
申请人： BASF AG
发明人： HEILEK JOERG , MUELLER-ENGEL KLAUS JOACHIM , HAMMON ULRICH , WALTER THOMAS
IPC分类号： B01D9/00 , C07B63/00 , C07C57/07
摘要： Process for controlling a hydraulic wash column having a cylindrical shell (1) which delimits the column and within which filter tubes (2) in the vicinity of the second end of column and at least one filter (3) in the filter tube wall, comprises: feeding of mother liquor (7) into first end of column; conducting mother liquor into filter tube; feeding control liquor (9) into wash column (12); purifying the mother liquor and control liquor flow; transporting the crystal bed (10); continuous removing; melting; passing the melt through the crystal bed; and determining flow rates. Process for controlling a hydraulic wash column comprises: continuous feeding of a stream of a suspension comprises a substance to be purified suspended in a mother liquor (7) into the first end of the column with a pressure P2, which is greater than P1; conducting the mother liquor through the filters into the filter tube interior and out of the column through the filter tubes; feeding the control liquor (9) into the wash column (12) at the first end of the column and/or between this end and the start of the filter; purifying the mother liquor and control liquor flow in the column from the crystal bed of the substance, where the crystal bed (10) is having a buildup front faces the first end of the column and at which the crystals are added continuously to the crystal bed; transporting the crystal bed by the force resulting from the hydraulic flow pressure drop of the mother liquor and the control liquor flow in the column, where the filters into the wash zone disposed between the filters and the second end of the wash column; continuous removing of the crystals at the opposite end of the crystal bed to the buildup front; melting the removed crystals; passing the melt through the crystal bed as a wash liquid stream coming from the second end of the column against the transport direction of the crystals; and determining the flow rates of the control liquor and/or suspension conducted into the wash column by utilizing at least one pressure difference delta P s k, which exists in the column between at least one point in the zone projecting from the buildup front up to the end of the crystal bed (preferably in the concentration zone, projecting up to the start of the wash zone, of the crystal bed), where the hydraulic wash column has a cylindrical shell (1), which delimits and within which one or more filter tubes (2) extend through the column parallel to the cylinder axis and have, in the vicinity of the second end of the column, at least one filter (3) in the filter tube wall, which forms the sole direct connection between the filter tube interior under the pressure P1 and the interior of the column.

10. 发明专利

DE50304605D1 未知
公开(公告)号：DE50304605D1
公开(公告)日：2006-09-21
申请号：DE50304605
申请日：2003-10-06
申请人： BASF AG
发明人： THIEL JOACHIM , HAMMON ULRICH , BAUMANN DIETER , HEILEK JOERG , SCHROEDER JUERGEN , MUELLER-ENGEL KLAUS JOACHIM
IPC分类号： C07C51/44 , C07C57/04
摘要： In a process for preparing acrylic acid, an acrylic acid-containing product gas mixture obtained by catalytic gas phase partial oxidation of a C 3 precursor of acrylic acid, after direct cooling with a quench liquid, is fractionally condensed in a separating column provided with internals, rising into itself with sidestream takeoff of crude acrylic acid, and the acrylic acid oligomers which form are dissociated and the resulting dissociation gas is subjected to a countercurrent rectification before it is recycled.

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