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1. 发明申请

WO2004024668A3 METHOD FOR PRODUCING IPDA WITH A HIGH CIS/TRANS ISOMER RATIO BY DISTILLATION 审中-公开
标题翻译：蒸馏工艺用于生产IPDA具有高顺/反式异构体
公开(公告)号：WO2004024668A3
公开(公告)日：2004-10-14
申请号：PCT/EP0308831
申请日：2003-08-08
申请人： BASF AG , FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUEDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED
发明人： FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUEDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED
IPC分类号： C07C209/86 , B01D3/14 , C07C209/84 , C07C211/36
CPC分类号： B01D3/141 , B01D3/146 , C07C209/84 , Y10S203/20 , C07C211/36
摘要： The invention relates to a method for obtaining 3-aminomethyl-3,5,5-trimethyl cyclohexylamine (isophorone diamine, IPDA) with a cis/trans isomer ratio of at least 73/27 by fractional distillation. Said method comprises the following steps: a) preparation of IPDA with a cis/trans isomer ratio /=73/27 and iv) an IPDA fraction with a cis/trans isomer ratio
摘要翻译：本发明涉及一种用于具有顺式/反式异构体中的至少73/27通过分馏，其包括以下步骤比率回收3-氨基甲基-3,5,5-三甲基环己胺（异佛尔酮二胺，IPDA）：a）提供具有IPDA顺/反异构体比率<73/27; b）将IPDA送入蒸馏塔的中间区域具有内部和在一定温度下在该蒸馏塔中蒸馏IPDA。为5〜300℃，为10〜2000毫巴的压力; c）任选地进一步纯化由步骤b）通过在至少一个另外的塔中蒸馏得到IPDA; 其中，所述步骤b）和c）需要在步骤a中使用的IPDA的分离）放置到至少五个级分IA）至iv）：IA）erunreinigungen低于一小部分的有机比例反式IPDA沸腾V，IB）的含水部分一小部分比反式IPDA沸点杂质下，ii）除了顺式IPDA沸点杂质更高的馏分，iii）具有> = 73/27的顺/反异构体比率的IPDA馏分和iv）具有顺式的IPDA馏分式/反式异构体比率<= 66/34。

2. 发明专利

CA2164688A1 PARTICLE FLUIDIZATION METHOD AND APPARATUS THEREFOR 未知
公开(公告)号：CA2164688A1
公开(公告)日：1996-06-09
申请号：CA2164688
申请日：1995-12-07
申请人： BIALLAS BERND , DUSCHEK WOLFGANG , MATTMANN WOLFGANG , HILLIGARDT KLAUS , FEINDT HANS JACOB
发明人： BIALLAS BERND , DUSCHEK WOLFGANG , MATTMANN WOLFGANG , HILLIGARDT KLAUS , FEINDT HANS-JACOB
IPC分类号： B01J8/24 , B05B7/14 , B05D1/24 , B01J8/18 , B05C19/02
摘要： Particle fluidization method in which particles are swirled up by a flow of a fluidizing gas to form a fluidized bed and pressure measurements are performed in or along the fluidized bed, and in which a parameter for the distribution of the measured values from these pressure measurements is determined and is used as a basis for regulating the flow rate of the stream of fluidizing gas.

3. 发明专利

AT343561T 未知
公开(公告)号：AT343561T
公开(公告)日：2006-11-15
申请号：AT03794858
申请日：2003-08-08
申请人： BASF AG
发明人： FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUEDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED
IPC分类号： C07C209/86 , B01D3/14 , C07C209/84 , C07C211/36
摘要： Recovery of isophoronediamine (IPDA) comprises preparation of IPDA having a cis/trans isomer ratio of less than 73/27 and separation into at least 5 fractions by distillation including an IPDA fraction having a cis/trans ratio of greater than 73/27 and a fraction having a cis/trans ratio of less than 66/34. A process for the recovery of 3-aminomethyl-3,5,5-trimethylcyclohexylamine (isophoronediamine, IPDA) comprises; (a) preparation of IPDA having a cis/trans isomer ratio of less than 73/27; (b) introduction of IPDA to the middle region of a distillation column having inserts and distillation of IPDA at 5-300 degreesC and 10-2000 mbar; (c) optionally further purification of the IPDA from (b) by distillation in at least one further column whereby the IPDA from step (b) and (c) are separated into at least 5 fractions comprising an organic fraction (1a) containing impurities having a lower b. pt. than trans-IPDA, an aqueous fraction (1b) containing impurities having a lower b. pt. than trans-IPDA, a fraction (2) containing impurities having a higher b. pt. than cis-IPDA, an IPDA fraction (3) having a cis/trans ratio of greater than 73/27 and an IPDA fraction (4) having a cis/trans ratio of less than 66/34.

4. 发明专利

AT217860T 未知
公开(公告)号：AT217860T
公开(公告)日：2002-06-15
申请号：AT98906939
申请日：1998-02-09
申请人： BASF AG
发明人： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
IPC分类号： C07C51/48 , C07C51/02 , C07C65/03 , C07C65/21 , C07C65/24
摘要： PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.

5. 发明专利

AU744848B2 Method for isolating 3-Ý2-chloro-4-(trifluoromethyl)-phenoxy¨-benzoic acid 未知
公开(公告)号：AU744848B2
公开(公告)日：2002-03-07
申请号：AU6296298
申请日：1998-02-09
申请人： BASF AG
发明人： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
IPC分类号： C07C51/48 , C07C51/02 , C07C65/03 , C07C65/21 , C07C65/24
摘要： PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.

6. 发明专利

NO992550A 未知
公开(公告)号：NO992550A
公开(公告)日：1999-11-29
申请号：NO992550
申请日：1999-05-27
申请人： BASF AG
发明人： MATTMANN WOLFGANG , KOENIG JOSEF , JONES SIMON A , EDINGER CHRISTINE , EDINGER MICHAEL , HEMMER GERD
IPC分类号： B01D53/34 , B01D53/75 , B01D53/77 , F23G5/00 , B08B9/08
CPC分类号： F23G5/006 , B01D53/34 , B01D53/75 , B01D53/77 , F23G2209/14

7. 发明专利

AU6296298A Method for isolating 3-{2-chloro-4-(trifluoromethyl)-phenoxy}-benzoic acid 未知
公开(公告)号：AU6296298A
公开(公告)日：1998-09-09
申请号：AU6296298
申请日：1998-02-09
申请人： BASF AG
发明人： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
IPC分类号： C07C51/48 , C07C51/02 , C07C65/03 , C07C65/21 , C07C65/24
摘要： PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.

8. 发明专利

ES2290546T3 METODO PARA LA PRODUCCION DE ISOFORONDIAMINA (IPDA, 3-AMINOMETIL-3,5,5-TRIMETILCICLOHEXILAMINA) QUE TIENE UNA PROPORCION ALTA DE ISOMEROS CIS/TRANS. 未知
公开(公告)号：ES2290546T3
公开(公告)日：2008-02-16
申请号：ES03790870
申请日：2003-08-06
申请人： BASF AG
发明人： FUNKE FRANK , HILL THOMAS , VON WATZDORF JOBST RUDIGER , MATTMANN WOLFGANG , HARDER WOLFGANG , HENKES ERHARD
IPC分类号： C07C209/54 , C07C209/84 , C07B61/00 , C07C29/68 , C07C209/82 , C07C209/86 , C07C211/36
摘要： Un proceso para preparar 3-aminometil-3, 5, 5-trimetilciclohexilamina (isoforonodiamina, IPDA) sustancialmente pura que tiene una proporción de isómeros cis/trans de por lo menos 73/27, y comprende la siguientes etapas: a) suministrar IPDA crudo que tenga una proporción de isómeros cis/trans de

9. 发明专利

AU2003258591A1 METHOD FOR PRODUCING IPDA WITH A HIGH CIS/TRANS ISOMER RATIO BY DISTILLATION 未知
公开(公告)号：AU2003258591A1
公开(公告)日：2004-04-30
申请号：AU2003258591
申请日：2003-08-08
申请人： BASF AG
发明人： HENKES ERHARD , LITTMANN GERD , JULIUS MANFRED , FUNKE FRANK , HILL THOMAS , WATZDORF JOBST RUDIGER VON , MATTMANN WOLFGANG , HARDER WOLFGANG
IPC分类号： C07C209/86 , B01D3/14 , C07C209/84 , C07C211/36 , C07C209/00
摘要： Recovery of isophoronediamine (IPDA) comprises preparation of IPDA having a cis/trans isomer ratio of less than 73/27 and separation into at least 5 fractions by distillation including an IPDA fraction having a cis/trans ratio of greater than 73/27 and a fraction having a cis/trans ratio of less than 66/34. A process for the recovery of 3-aminomethyl-3,5,5-trimethylcyclohexylamine (isophoronediamine, IPDA) comprises; (a) preparation of IPDA having a cis/trans isomer ratio of less than 73/27; (b) introduction of IPDA to the middle region of a distillation column having inserts and distillation of IPDA at 5-300 degreesC and 10-2000 mbar; (c) optionally further purification of the IPDA from (b) by distillation in at least one further column whereby the IPDA from step (b) and (c) are separated into at least 5 fractions comprising an organic fraction (1a) containing impurities having a lower b. pt. than trans-IPDA, an aqueous fraction (1b) containing impurities having a lower b. pt. than trans-IPDA, a fraction (2) containing impurities having a higher b. pt. than cis-IPDA, an IPDA fraction (3) having a cis/trans ratio of greater than 73/27 and an IPDA fraction (4) having a cis/trans ratio of less than 66/34.

10. 发明专利

BR9807583A 未知
公开(公告)号：BR9807583A
公开(公告)日：2000-03-21
申请号：BR9807583
申请日：1998-02-09
申请人： BASF AG
发明人： MERKLE HANS RUPERT , EVA RONALD R , FRANKE DIRK , JONES SIMON A , MATTMANN WOLFGANG , MUNZINGER MANFRED
IPC分类号： C07C51/48 , C07C51/02 , C07C65/03 , C07C65/21 , C07C65/24
摘要： PCT No. PCT/EP98/00705 Sec. 371 Date Jul. 28, 1999 Sec. 102(e) Date Jul. 28, 1999 PCT Filed Feb. 9, 1998 PCT Pub. No. WO98/37054 PCT Pub. Date Aug. 27, 1998A process for the isolation of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid of the formula I from an aqueous solution of its metal salt comprises a) reacting the metal salt of 3-[2-chloro-4-(trifluoromethyl)phenoxy]benzoic acid with an organic or inorganic acid; b) heating the reaction mixture until a liquid two-phase system of organic and aqueous phase has formed; and c) separating the organic phase from the aqueous phase.

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