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1. 发明授权

US6111100C1 Preparation of bis(2-morpholinoethyl) ether 有权
标题翻译：双（2-吗啉代乙基）醚的制备
公开(公告)号：US6111100C1
公开(公告)日：2002-04-02
申请号：US47490699
申请日：1999-12-30
申请人： BASF AG
发明人： RIECHERS HARTMUT , SIMON JOACHIM , HENNE ANDREAS , HOEHN ARTHUR
IPC分类号： C07D295/08 , B01J23/72 , C07D295/088 , C07D413/12
CPC分类号： C07D295/088

2. 发明专利

JP2000212134A MANUFACTURE OF N-ETHYL-DIISOPROPYLAMINE 失效
公开(公告)号：JP2000212134A
公开(公告)日：2000-08-02
申请号：JP2000006835
申请日：2000-01-14
申请人： BASF AG
发明人： ELLER KARSTEN DR , FIEGE BERND , HENNE ANDREAS , KNEUPER HEINZ-JOSEF DR
IPC分类号： B01J23/44 , B01J23/46 , B01J23/68 , C07B61/00 , C07C209/26 , C07C211/06 , C07C211/08
摘要： PROBLEM TO BE SOLVED: To provide an economic method for manufacture of N-ethyl- diisopropylamine in an excellent space-time yield capable of carrying out in a discontinuous method or continuous method. SOLUTION: This method comprises the reaction of acetaldehyde, diisopropylamine and hydrogen at elevated temperature and pressurized condition in the presence of the hydrogenating catalyst, using a catalyst including oxide type supporting material selected from a group selected zirconium dioxide, titanium dioxide, aluminum oxide, silicone dioxide, zinc oxide, magnesium oxide, cerium dioxide, clay and zeolite and their mixtures.

3. 发明专利

JP2000212175A PRODUCTION OF 2,2'-MORPHOLINO DIETHYL ETHER 失效
公开(公告)号：JP2000212175A
公开(公告)日：2000-08-02
申请号：JP37063599
申请日：1999-12-27
申请人： BASF AG
发明人： RIECHERS HARTMUT , SIMON JOACHIM DR , HENNE ANDREAS , HOEHN ARTHUR
IPC分类号： C07D295/08 , B01J23/72 , C07D295/088
摘要： PROBLEM TO BE SOLVED: To obtain 2,2'-morpholino diethyl ether by using a specific catalyst before reducing diethylene glycol and ammonia with hydrogen. SOLUTION: This compound is obtained by incorporating a catalyst whose catalytic component contains aluminum oxide, zirconium dioxide, titanium dioxide, and/or silicon dioxide at 20-85 wt.%, an oxygen-containing compound of Cu at 1-70 wt.% as calculated as CuO, oxygen-containing compound(s) of Mg, Cr, Zn, Ba, and/or Ca at 0-50 wt.% as calculated as MgO, Cr2O3, ZnO, BaO, and/or CaO, respectively, and an oxygen-containing compound of Ni as calculated as NiO at less than 20 wt.% per the oxygen-containing compound of Cu before reducing diethylene glycol and ammonia with hydrogen in the presence of the obtained hydrogenation catalyst at an elevated temperature and pressure.

4. 发明专利

JPH1149733A PRODUCTION OF ANHYDROUS 2-AMINO-1-METHOXYPROPANE 失效
公开(公告)号：JPH1149733A
公开(公告)日：1999-02-23
申请号：JP14725298
申请日：1998-05-28
申请人： BASF AG
发明人： SIMON JOACHIM , HENNE ANDREAS , LINGK HEINZ
IPC分类号： C07C213/02 , C07C213/10 , C07C217/08
摘要： PROBLEM TO BE SOLVED: To provide a method for producing anhydrous 2-amino-1- methoxypropane, capable of obtaining a desired product in high yield. SOLUTION: (a) Two phases comprising a reaction mixture and sodium hydroxide solution, obtained by reaction of 1-methoxy-2-propanol with ammonia on a catalyst are formed and (b) 2-amino-1-methoxypropane-containing phase is separated from water phase and (c) 2-amino-1-methoxypropane-containing phase is subjected to azeotropic distillation to produce an azeotropic mixture at first and the azeotropic mixture is returned to a process (a) or (b), and then, anhydrous 2-amino-1-methoxypropane is produced.

5. 发明专利

JPH1072377A PROCESS FOR REACTION OF ORGANIC COMPOUNDS AND CATALYST THEREFOR 失效
公开(公告)号：JPH1072377A
公开(公告)日：1998-03-17
申请号：JP16283697
申请日：1997-06-19
申请人： BASF AG
发明人： RUEHL THOMAS DR , BREITSCHEIDEL BORIS DR , KONRAD KNOLL , WEIGUNY SABINE , HENKELMAN JOCHEM , NAEGELE PAUL , HERMANN GAUSEPOHL , NIESNER NORBERT , HENNE ANDREAS , ROLF REEPUKYUUHIYAA
IPC分类号： B01J23/44 , B01J23/46 , B01J35/10 , C07B35/02 , C07B61/00 , C07C29/141 , C07C29/149 , C07C29/20 , C07C31/12 , C07C31/135 , C07C31/20 , C07C35/08 , C07C35/21 , C07C209/72 , C07C211/35 , C08C19/02 , C08F4/70 , C08F4/80 , C08F8/04 , C08F36/06 , C08F297/04
摘要： PROBLEM TO BE SOLVED: To enable the obtaining of a process by which a high yield or a quantitative conversion rate can be achieved by reacting an organic compound in the presence of a catalyst containing a specific metal supported on a specified support. SOLUTION: An organic compound is reacted in the presence of a catalyst comprising (B) ruthenium alone or together with at least one group Ib, IIb or VIIIb as an active metal in an amount of 0.01-30wt.%, based on the total weight of the catalyst applied to (A) a support in which 50-90% of the pore volume of the support comprises mesepores having a pore diameter within the range of 2-50nm and the sum of the pores volumes is 100%. The reaction is preferably hydrogenation, dehydrogenation, hydrogenolysis, etc., especially preferably the hydrogenation. The organic compound is low molecular weight monomers and polymeric organic compounds, etc., which can be catalytically reacted. Thereby, the reaction can be carried out at a high space velocity and an ultrahigh turnover number for a long on-stream time, and a high yield and a high purity of a hydrogenation product can be expected.

6. 发明申请

WO03068784A2 ACYL- AND BISACYLPHOSPHINE DERIVATIVES 审中-公开
标题翻译：酰基和二酰基
公开(公告)号：WO03068784A2
公开(公告)日：2003-08-21
申请号：PCT/EP0301053
申请日：2003-02-04
申请人： BASF AG , NOE RALF , HENNE ANDREAS , MAASE MATTHIAS
发明人： NOE RALF , HENNE ANDREAS , MAASE MATTHIAS
IPC分类号： C07F9/30 , C07F9/32 , C07F9/34 , C07F9/36 , C07F9/40 , C07F9/42 , C08F2/50 , C08F4/00 , G03F7/029 , C07F9/50 , C07F9/52
CPC分类号： C07F9/3294 , C07F9/3252 , C07F9/34 , C07F9/36 , C07F9/4065 , C07F9/409 , C07F9/4093 , C07F9/4096 , C07F9/425 , G03F7/029
摘要： The invention relates to the acyl- and bisacylphosphine derivatives according to formula (I), wherein Y represents O, S, NR3, N-OR3 or N-NR3R4, Z represents O, S, NR3, N-OR3, N-NR3R4 or a free pair of electrons, and FG represents a leaving group and the remaining groups are defined as in the description. The invention further relates to a method for the production of the inventive derivatives and to their use.
摘要翻译：根据式I，其中Y是酰基和二酰基膦衍生物O，S，NR 3，N-OR 3或N-NR 3 R 4，Z是O，S，NR 3，N-NR 3 R 4，或自由电子对，和FG是指离去基团，并且其它基团如在所描述的刚才提到的含义，其制备方法及其用途。

7. 发明专利

AU2003205731A1 MONO- AND BIACYLPHOSPHINE DERIVATIVES 未知
公开(公告)号：AU2003205731A1
公开(公告)日：2003-09-04
申请号：AU2003205731
申请日：2003-02-04
申请人： BASF AG
发明人： NOE RALF , BECK ERICH , MAASE MATTHIAS , HENNE ANDREAS
IPC分类号： C07F9/32 , C07F9/36 , C07F9/40 , C07F9/44 , C07F9/59 , C07F9/6509 , C07F9/655 , C08F2/50 , C07F9/53

8. 发明专利

AU2003205730A1 ALKOXYLATED ACYL- AND BISACYLPHOSPHINE DERIVATIVES 未知
公开(公告)号：AU2003205730A1
公开(公告)日：2003-09-04
申请号：AU2003205730
申请日：2003-02-04
申请人： BASF AG
发明人： NOE RALF , HENNE ANDREAS , MAASE MATTHIAS
IPC分类号： C07F9/32 , C07F9/36 , C07F9/46 , C07F9/553 , C07F9/655 , C08F2/50 , G03F7/029

9. 发明专利

PT1020455E 未知
公开(公告)号：PT1020455E
公开(公告)日：2003-07-31
申请号：PT99125083
申请日：1999-12-16
申请人： BASF AG
发明人： RIECHERS HARTMUT , SIMON JOACHIM , HENNE ANDREAS , ARTHUR HOHN DR
IPC分类号： C07D295/08 , B01J23/72 , C07D295/088
摘要： 2,2'-Dimorpholinodiethyl ether is produced by reacting diethylene glycol with ammonia under pressure at elevated temperature in the presence of hydrogen. The active hydrogenation catalyst, before reduction with hydrogen, contains 20-85 wt.% alumina, zirconium dioxide, titanium dioxide and/or silica, 1-70 wt.% copper oxide (CuO), less than 20 wt.% nickel oxide with respect to CuO and 0-50 wt.% other metal oxide(s). In the production of 2,2'-dimorpholinodiethyl ether (DMDEE) by reacting diethylene glycol with ammonia under pressure at elevated temperature in the presence of hydrogen and a hydrogenation catalyst, the active catalyst, before reduction with hydrogen, contains 20-85 wt.% aluminum oxide (Al2O3), zirconium dioxide (ZrO2), titanium dioxide (TiO2) and/or silica (SiO2), 1-70 wt.% copper oxide (expressed as CuO), 0-50 wt.% magnesium, chromium, zinc, barium and/or calcium oxide (expressed as MgO, Cr2O3, ZnO, BaO and CaO) and less than 20 wt.% nickel oxide (expressed as NiO) with respect to CuO.

10. 发明专利

DE19722700A1 未知
公开(公告)号：DE19722700A1
公开(公告)日：1998-12-03
申请号：DE19722700
申请日：1997-05-30
申请人： BASF AG
发明人： SIMON JOACHIM , HENNE ANDREAS , LINGK HEINZ
IPC分类号： C07C213/02 , C07C213/10 , C07C217/08 , B01J23/885
摘要： Production of anhydrous 2-amino-1-methoxypropane (I) comprises (a) treating an aqueous reaction mixture (II) containing (I), obtained by reacting 1-methoxy-2-propanol with ammonia (NH3) on a catalyst, with aqueous sodium hydroxide (NaOH) solution to form an aqueous phase containing aqueous NaOH solution and a phase containing (I); (b) separating the phase (III) containing (I) from the aqueous phase; and (c) distilling (III) to separate an azeotrope of water and (I), which is recycled to step (a) or (b), and then anhydrous (I). Also claimed is a method of separating water from (II) in this way.

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